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Bergenia ciliate–Mediated Mixed-Phase Synthesis and Characterization of Silver-Copper Oxide Nanocomposite for Environmental and Biological Applications

Bergenia ciliate (B. ciliate) leaf extract was used as a reducing and stabilizing agent for the synthesis of silver-copper oxide nanocomposite (Ag-CuO NC). Scanning and transmission electron microscopies (SEM and TEM) were used to examine the structural morphology, and the average particle size was...

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Autores principales: Rehman, Fazal Ur, Mahmood, Rashid, Ali, Manel Ben, Hedfi, Amor, Almalki, Mohammed, Mezni, Amine, Rehman, Wajid, Haq, Sirajul, Afsar, Humma
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2021
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8549009/
https://www.ncbi.nlm.nih.gov/pubmed/34683677
http://dx.doi.org/10.3390/ma14206085
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author Rehman, Fazal Ur
Mahmood, Rashid
Ali, Manel Ben
Hedfi, Amor
Almalki, Mohammed
Mezni, Amine
Rehman, Wajid
Haq, Sirajul
Afsar, Humma
author_facet Rehman, Fazal Ur
Mahmood, Rashid
Ali, Manel Ben
Hedfi, Amor
Almalki, Mohammed
Mezni, Amine
Rehman, Wajid
Haq, Sirajul
Afsar, Humma
author_sort Rehman, Fazal Ur
collection PubMed
description Bergenia ciliate (B. ciliate) leaf extract was used as a reducing and stabilizing agent for the synthesis of silver-copper oxide nanocomposite (Ag-CuO NC). Scanning and transmission electron microscopies (SEM and TEM) were used to examine the structural morphology, and the average particle size was determined to be 47.65 nm. The phase confirmation and crystalline structure were examined through the X-ray diffraction (XRD) technique, where cubic and monoclinic geometries were assigned to Ag and CuO. The energy dispersive X-ray (EDX), Fourier transform infrared (FTIR) and ultra-violet and visible (UV-Visible) spectroscopies were operated to analyse the elemental composition, functional groups and light absorption phenomena of the Ag-CuO NC. Under the full light spectrum, the photodegradation of Rhodamine 6G was recorded, and 99.42 percent of the dye degraded in 80 min. The Agar well diffusion method was followed to perform antibacterial activity against selected pathogens, and the activity was found to increase with increasing concentration of Ag-CuO NC. The ABTS free radical scavenging activity suggests that the activity of Ag-CuO NC is higher than ascorbic acid.
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spelling pubmed-85490092021-10-28 Bergenia ciliate–Mediated Mixed-Phase Synthesis and Characterization of Silver-Copper Oxide Nanocomposite for Environmental and Biological Applications Rehman, Fazal Ur Mahmood, Rashid Ali, Manel Ben Hedfi, Amor Almalki, Mohammed Mezni, Amine Rehman, Wajid Haq, Sirajul Afsar, Humma Materials (Basel) Article Bergenia ciliate (B. ciliate) leaf extract was used as a reducing and stabilizing agent for the synthesis of silver-copper oxide nanocomposite (Ag-CuO NC). Scanning and transmission electron microscopies (SEM and TEM) were used to examine the structural morphology, and the average particle size was determined to be 47.65 nm. The phase confirmation and crystalline structure were examined through the X-ray diffraction (XRD) technique, where cubic and monoclinic geometries were assigned to Ag and CuO. The energy dispersive X-ray (EDX), Fourier transform infrared (FTIR) and ultra-violet and visible (UV-Visible) spectroscopies were operated to analyse the elemental composition, functional groups and light absorption phenomena of the Ag-CuO NC. Under the full light spectrum, the photodegradation of Rhodamine 6G was recorded, and 99.42 percent of the dye degraded in 80 min. The Agar well diffusion method was followed to perform antibacterial activity against selected pathogens, and the activity was found to increase with increasing concentration of Ag-CuO NC. The ABTS free radical scavenging activity suggests that the activity of Ag-CuO NC is higher than ascorbic acid. MDPI 2021-10-14 /pmc/articles/PMC8549009/ /pubmed/34683677 http://dx.doi.org/10.3390/ma14206085 Text en © 2021 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Rehman, Fazal Ur
Mahmood, Rashid
Ali, Manel Ben
Hedfi, Amor
Almalki, Mohammed
Mezni, Amine
Rehman, Wajid
Haq, Sirajul
Afsar, Humma
Bergenia ciliate–Mediated Mixed-Phase Synthesis and Characterization of Silver-Copper Oxide Nanocomposite for Environmental and Biological Applications
title Bergenia ciliate–Mediated Mixed-Phase Synthesis and Characterization of Silver-Copper Oxide Nanocomposite for Environmental and Biological Applications
title_full Bergenia ciliate–Mediated Mixed-Phase Synthesis and Characterization of Silver-Copper Oxide Nanocomposite for Environmental and Biological Applications
title_fullStr Bergenia ciliate–Mediated Mixed-Phase Synthesis and Characterization of Silver-Copper Oxide Nanocomposite for Environmental and Biological Applications
title_full_unstemmed Bergenia ciliate–Mediated Mixed-Phase Synthesis and Characterization of Silver-Copper Oxide Nanocomposite for Environmental and Biological Applications
title_short Bergenia ciliate–Mediated Mixed-Phase Synthesis and Characterization of Silver-Copper Oxide Nanocomposite for Environmental and Biological Applications
title_sort bergenia ciliate–mediated mixed-phase synthesis and characterization of silver-copper oxide nanocomposite for environmental and biological applications
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8549009/
https://www.ncbi.nlm.nih.gov/pubmed/34683677
http://dx.doi.org/10.3390/ma14206085
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