The Synthesis and Characterization of h-BN Nanosheets with High Yield and Crystallinity

[Image: see text] Nowadays, boron nitride (BN) has attracted a great deal of attention due to its physical and chemical properties, such as high-temperature resistance, oxidation resistance, heat conduction, electrical insulation, and neutron absorption. The unique lamellar, reticular, and tubular morphologies and physicochemical properties of BN make it attractive in the fields of adsorption, catalysis, hydrogen storage, thermal conduction, insulation, dielectric substrate of electronic devices, radiation protection, polymer composites, medicine, etc. Based on this, we propose a novel method to produce boron nitride nanosheets (BNNSs) by a two-step method. The structure and morphology of the prepared BNNSs were characterized by scanning electron microscopy, transmission electron microscopy, atomic force microscopy, XRD, FTIR, etc. The results showed that the prepared BNNSs had high crystallinity and the stripping efficiency of h-BN as well as the performance and yield of BNNSs had been improved, and the cost and environmental pollution of BNNS preparation had been reduced accordingly.