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Measurement of the coherent beam properties at the CoSAXS beamline

The CoSAXS beamline at the MAX IV Laboratory is a modern multi-purpose (coherent) small-angle X-ray scattering (CoSAXS) instrument, designed to provide intense and optionally coherent illumination at the sample position, enabling coherent imaging and speckle contrast techniques. X-ray tracing simula...

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Autores principales: Kahnt, Maik, Klementiev, Konstantin, Haghighat, Vahid, Weninger, Clemens, Plivelic, Tomás S., Terry, Ann E., Björling, Alexander
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2021
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8570205/
https://www.ncbi.nlm.nih.gov/pubmed/34738950
http://dx.doi.org/10.1107/S1600577521009140
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author Kahnt, Maik
Klementiev, Konstantin
Haghighat, Vahid
Weninger, Clemens
Plivelic, Tomás S.
Terry, Ann E.
Björling, Alexander
author_facet Kahnt, Maik
Klementiev, Konstantin
Haghighat, Vahid
Weninger, Clemens
Plivelic, Tomás S.
Terry, Ann E.
Björling, Alexander
author_sort Kahnt, Maik
collection PubMed
description The CoSAXS beamline at the MAX IV Laboratory is a modern multi-purpose (coherent) small-angle X-ray scattering (CoSAXS) instrument, designed to provide intense and optionally coherent illumination at the sample position, enabling coherent imaging and speckle contrast techniques. X-ray tracing simulations used to design the beamline optics have predicted a total photon flux of 10(12)–10(13) photons s(−1) and a degree of coherence of up to 10% at 7.1 keV. The normalized degree of coherence and the coherent flux of this instrument were experimentally determined using the separability of a ptychographic reconstruction into multiple mutually incoherent modes and thus the Coherence in the name CoSAXS was verified. How the beamline can be used both for coherent imaging and XPCS measurements, which both heavily rely on the degree of coherence of the beam, was demonstrated. These results are the first experimental quantification of coherence properties in a SAXS instrument at a fourth-generation synchrotron light source.
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spelling pubmed-85702052021-11-18 Measurement of the coherent beam properties at the CoSAXS beamline Kahnt, Maik Klementiev, Konstantin Haghighat, Vahid Weninger, Clemens Plivelic, Tomás S. Terry, Ann E. Björling, Alexander J Synchrotron Radiat Beamlines The CoSAXS beamline at the MAX IV Laboratory is a modern multi-purpose (coherent) small-angle X-ray scattering (CoSAXS) instrument, designed to provide intense and optionally coherent illumination at the sample position, enabling coherent imaging and speckle contrast techniques. X-ray tracing simulations used to design the beamline optics have predicted a total photon flux of 10(12)–10(13) photons s(−1) and a degree of coherence of up to 10% at 7.1 keV. The normalized degree of coherence and the coherent flux of this instrument were experimentally determined using the separability of a ptychographic reconstruction into multiple mutually incoherent modes and thus the Coherence in the name CoSAXS was verified. How the beamline can be used both for coherent imaging and XPCS measurements, which both heavily rely on the degree of coherence of the beam, was demonstrated. These results are the first experimental quantification of coherence properties in a SAXS instrument at a fourth-generation synchrotron light source. International Union of Crystallography 2021-10-05 /pmc/articles/PMC8570205/ /pubmed/34738950 http://dx.doi.org/10.1107/S1600577521009140 Text en © Maik Kahnt et al. 2021 https://creativecommons.org/licenses/by/4.0/This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Beamlines
Kahnt, Maik
Klementiev, Konstantin
Haghighat, Vahid
Weninger, Clemens
Plivelic, Tomás S.
Terry, Ann E.
Björling, Alexander
Measurement of the coherent beam properties at the CoSAXS beamline
title Measurement of the coherent beam properties at the CoSAXS beamline
title_full Measurement of the coherent beam properties at the CoSAXS beamline
title_fullStr Measurement of the coherent beam properties at the CoSAXS beamline
title_full_unstemmed Measurement of the coherent beam properties at the CoSAXS beamline
title_short Measurement of the coherent beam properties at the CoSAXS beamline
title_sort measurement of the coherent beam properties at the cosaxs beamline
topic Beamlines
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8570205/
https://www.ncbi.nlm.nih.gov/pubmed/34738950
http://dx.doi.org/10.1107/S1600577521009140
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