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Enhancing the Mechanical Properties of Biodegradable Mg Alloys Processed by Warm HPT and Thermal Treatments

In this study, several biodegradable Mg alloys (Mg5Zn, Mg5Zn0.3Ca, Mg5Zn0.15Ca, and Mg5Zn0.15Ca0.15Zr, numbers in wt%) were investigated after thermomechanical processing via high-pressure torsion (HPT) at elevated temperature as well as after additional heat treatments. Indirect and direct analyses...

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Autores principales: Mizelli-Ojdanic, Andrea, Horky, Jelena, Mingler, Bernhard, Fanetti, Mattia, Gardonio, Sandra, Valant, Matjaz, Sulkowski, Bartosz, Schafler, Erhard, Orlov, Dmytro, Zehetbauer, Michael J.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2021
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8585245/
https://www.ncbi.nlm.nih.gov/pubmed/34771925
http://dx.doi.org/10.3390/ma14216399
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author Mizelli-Ojdanic, Andrea
Horky, Jelena
Mingler, Bernhard
Fanetti, Mattia
Gardonio, Sandra
Valant, Matjaz
Sulkowski, Bartosz
Schafler, Erhard
Orlov, Dmytro
Zehetbauer, Michael J.
author_facet Mizelli-Ojdanic, Andrea
Horky, Jelena
Mingler, Bernhard
Fanetti, Mattia
Gardonio, Sandra
Valant, Matjaz
Sulkowski, Bartosz
Schafler, Erhard
Orlov, Dmytro
Zehetbauer, Michael J.
author_sort Mizelli-Ojdanic, Andrea
collection PubMed
description In this study, several biodegradable Mg alloys (Mg5Zn, Mg5Zn0.3Ca, Mg5Zn0.15Ca, and Mg5Zn0.15Ca0.15Zr, numbers in wt%) were investigated after thermomechanical processing via high-pressure torsion (HPT) at elevated temperature as well as after additional heat treatments. Indirect and direct analyses of microstructure revealed that the significant strength increases arise not only from dislocations and precipitates but also from vacancy agglomerates. By contrast with former low-temperature processing routes applied by the authors, a significant ductility was obtained because of temperature-induced dynamic recovery. The low initial values of Young’s modulus were not significantly affected by warm HPT-processing. nor by heat treatments afterwards. Also, corrosion resistance did not change or even increase during those treatments. Altogether, the study reveals a viable processing route for the optimization of Mg alloys to provide enhanced mechanical properties while leaving the corrosion properties unaffected, suggesting it for the use as biodegradable implant material.
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spelling pubmed-85852452021-11-12 Enhancing the Mechanical Properties of Biodegradable Mg Alloys Processed by Warm HPT and Thermal Treatments Mizelli-Ojdanic, Andrea Horky, Jelena Mingler, Bernhard Fanetti, Mattia Gardonio, Sandra Valant, Matjaz Sulkowski, Bartosz Schafler, Erhard Orlov, Dmytro Zehetbauer, Michael J. Materials (Basel) Article In this study, several biodegradable Mg alloys (Mg5Zn, Mg5Zn0.3Ca, Mg5Zn0.15Ca, and Mg5Zn0.15Ca0.15Zr, numbers in wt%) were investigated after thermomechanical processing via high-pressure torsion (HPT) at elevated temperature as well as after additional heat treatments. Indirect and direct analyses of microstructure revealed that the significant strength increases arise not only from dislocations and precipitates but also from vacancy agglomerates. By contrast with former low-temperature processing routes applied by the authors, a significant ductility was obtained because of temperature-induced dynamic recovery. The low initial values of Young’s modulus were not significantly affected by warm HPT-processing. nor by heat treatments afterwards. Also, corrosion resistance did not change or even increase during those treatments. Altogether, the study reveals a viable processing route for the optimization of Mg alloys to provide enhanced mechanical properties while leaving the corrosion properties unaffected, suggesting it for the use as biodegradable implant material. MDPI 2021-10-25 /pmc/articles/PMC8585245/ /pubmed/34771925 http://dx.doi.org/10.3390/ma14216399 Text en © 2021 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Mizelli-Ojdanic, Andrea
Horky, Jelena
Mingler, Bernhard
Fanetti, Mattia
Gardonio, Sandra
Valant, Matjaz
Sulkowski, Bartosz
Schafler, Erhard
Orlov, Dmytro
Zehetbauer, Michael J.
Enhancing the Mechanical Properties of Biodegradable Mg Alloys Processed by Warm HPT and Thermal Treatments
title Enhancing the Mechanical Properties of Biodegradable Mg Alloys Processed by Warm HPT and Thermal Treatments
title_full Enhancing the Mechanical Properties of Biodegradable Mg Alloys Processed by Warm HPT and Thermal Treatments
title_fullStr Enhancing the Mechanical Properties of Biodegradable Mg Alloys Processed by Warm HPT and Thermal Treatments
title_full_unstemmed Enhancing the Mechanical Properties of Biodegradable Mg Alloys Processed by Warm HPT and Thermal Treatments
title_short Enhancing the Mechanical Properties of Biodegradable Mg Alloys Processed by Warm HPT and Thermal Treatments
title_sort enhancing the mechanical properties of biodegradable mg alloys processed by warm hpt and thermal treatments
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8585245/
https://www.ncbi.nlm.nih.gov/pubmed/34771925
http://dx.doi.org/10.3390/ma14216399
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