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Analysis of the Electroconsolidation Process of Fine-Dispersed Structures Out of Hot Pressed Al(2)O(3)–WC Nanopowders

Fabrication of alumina–tungsten carbide nanocomposite was investigated. Characteristics of the densification and sintering were analyzed considering both the nano-size particle starting powders and the processing stages. Different heating rates were generated during densification and consolidation w...

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Autores principales: Gevorkyan, Edwin, Rucki, Mirosław, Krzysiak, Zbigniew, Chishkala, Volodymyr, Zurowski, Wojciech, Kucharczyk, Wojciech, Barsamyan, Voskan, Nerubatskyi, Volodymyr, Mazur, Tomasz, Morozow, Dmitrij, Siemiątkowski, Zbigniew, Caban, Jacek
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2021
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8585290/
https://www.ncbi.nlm.nih.gov/pubmed/34772030
http://dx.doi.org/10.3390/ma14216503
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author Gevorkyan, Edwin
Rucki, Mirosław
Krzysiak, Zbigniew
Chishkala, Volodymyr
Zurowski, Wojciech
Kucharczyk, Wojciech
Barsamyan, Voskan
Nerubatskyi, Volodymyr
Mazur, Tomasz
Morozow, Dmitrij
Siemiątkowski, Zbigniew
Caban, Jacek
author_facet Gevorkyan, Edwin
Rucki, Mirosław
Krzysiak, Zbigniew
Chishkala, Volodymyr
Zurowski, Wojciech
Kucharczyk, Wojciech
Barsamyan, Voskan
Nerubatskyi, Volodymyr
Mazur, Tomasz
Morozow, Dmitrij
Siemiątkowski, Zbigniew
Caban, Jacek
author_sort Gevorkyan, Edwin
collection PubMed
description Fabrication of alumina–tungsten carbide nanocomposite was investigated. Characteristics of the densification and sintering were analyzed considering both the nano-size particle starting powders and the processing stages. Different heating rates were generated during densification and consolidation with a maximal load was applied only after a temperature of 1000 °C was reached. Due to the varying dominance of different physical processes affecting the grains, appropriate heating rates and pressure at different stages ensured that a structure with submicron grains was obtained. With directly applied alternating current, it was found that the proportion Al(2)O(3) (50 wt.%)–WC provided the highest fracture toughness, and a sintering temperature above 1600 °C was found to be disadvantageous. High heating rates and a short sintering time enabled the process to be completed in 12 min, saving energy and time.
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spelling pubmed-85852902021-11-12 Analysis of the Electroconsolidation Process of Fine-Dispersed Structures Out of Hot Pressed Al(2)O(3)–WC Nanopowders Gevorkyan, Edwin Rucki, Mirosław Krzysiak, Zbigniew Chishkala, Volodymyr Zurowski, Wojciech Kucharczyk, Wojciech Barsamyan, Voskan Nerubatskyi, Volodymyr Mazur, Tomasz Morozow, Dmitrij Siemiątkowski, Zbigniew Caban, Jacek Materials (Basel) Article Fabrication of alumina–tungsten carbide nanocomposite was investigated. Characteristics of the densification and sintering were analyzed considering both the nano-size particle starting powders and the processing stages. Different heating rates were generated during densification and consolidation with a maximal load was applied only after a temperature of 1000 °C was reached. Due to the varying dominance of different physical processes affecting the grains, appropriate heating rates and pressure at different stages ensured that a structure with submicron grains was obtained. With directly applied alternating current, it was found that the proportion Al(2)O(3) (50 wt.%)–WC provided the highest fracture toughness, and a sintering temperature above 1600 °C was found to be disadvantageous. High heating rates and a short sintering time enabled the process to be completed in 12 min, saving energy and time. MDPI 2021-10-29 /pmc/articles/PMC8585290/ /pubmed/34772030 http://dx.doi.org/10.3390/ma14216503 Text en © 2021 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Gevorkyan, Edwin
Rucki, Mirosław
Krzysiak, Zbigniew
Chishkala, Volodymyr
Zurowski, Wojciech
Kucharczyk, Wojciech
Barsamyan, Voskan
Nerubatskyi, Volodymyr
Mazur, Tomasz
Morozow, Dmitrij
Siemiątkowski, Zbigniew
Caban, Jacek
Analysis of the Electroconsolidation Process of Fine-Dispersed Structures Out of Hot Pressed Al(2)O(3)–WC Nanopowders
title Analysis of the Electroconsolidation Process of Fine-Dispersed Structures Out of Hot Pressed Al(2)O(3)–WC Nanopowders
title_full Analysis of the Electroconsolidation Process of Fine-Dispersed Structures Out of Hot Pressed Al(2)O(3)–WC Nanopowders
title_fullStr Analysis of the Electroconsolidation Process of Fine-Dispersed Structures Out of Hot Pressed Al(2)O(3)–WC Nanopowders
title_full_unstemmed Analysis of the Electroconsolidation Process of Fine-Dispersed Structures Out of Hot Pressed Al(2)O(3)–WC Nanopowders
title_short Analysis of the Electroconsolidation Process of Fine-Dispersed Structures Out of Hot Pressed Al(2)O(3)–WC Nanopowders
title_sort analysis of the electroconsolidation process of fine-dispersed structures out of hot pressed al(2)o(3)–wc nanopowders
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8585290/
https://www.ncbi.nlm.nih.gov/pubmed/34772030
http://dx.doi.org/10.3390/ma14216503
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