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Single-Shot Multicontrast X-ray Imaging for In Situ Visualization of Chemical Reaction Products

We present the application of single-shot multicontrast X-ray imaging with an inverted Hartmann mask to the time-resolved in situ visualization of chemical reaction products. The real-time monitoring of an illustrative chemical reaction indicated the formation of the precipitate by the absorption, d...

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Detalles Bibliográficos
Autores principales: Zakharova, Margarita, Mikhaylov, Andrey, Vlnieska, Vitor, Kunka, Danays
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2021
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8621068/
https://www.ncbi.nlm.nih.gov/pubmed/34821852
http://dx.doi.org/10.3390/jimaging7110221
Descripción
Sumario:We present the application of single-shot multicontrast X-ray imaging with an inverted Hartmann mask to the time-resolved in situ visualization of chemical reaction products. The real-time monitoring of an illustrative chemical reaction indicated the formation of the precipitate by the absorption, differential phase, and scattering contrast images obtained from a single projection. Through these contrast channels, the formation of the precipitate along the mixing line of the reagents, the border between the solid and the solution, and the presence of the scattering structures of 100–200 nm sizes were observed. The measurements were performed in a flexible and robust setup, which can be tailored to various imaging applications at different time scales.