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Single-Shot Multicontrast X-ray Imaging for In Situ Visualization of Chemical Reaction Products

We present the application of single-shot multicontrast X-ray imaging with an inverted Hartmann mask to the time-resolved in situ visualization of chemical reaction products. The real-time monitoring of an illustrative chemical reaction indicated the formation of the precipitate by the absorption, d...

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Detalles Bibliográficos
Autores principales: Zakharova, Margarita, Mikhaylov, Andrey, Vlnieska, Vitor, Kunka, Danays
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2021
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8621068/
https://www.ncbi.nlm.nih.gov/pubmed/34821852
http://dx.doi.org/10.3390/jimaging7110221
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author Zakharova, Margarita
Mikhaylov, Andrey
Vlnieska, Vitor
Kunka, Danays
author_facet Zakharova, Margarita
Mikhaylov, Andrey
Vlnieska, Vitor
Kunka, Danays
author_sort Zakharova, Margarita
collection PubMed
description We present the application of single-shot multicontrast X-ray imaging with an inverted Hartmann mask to the time-resolved in situ visualization of chemical reaction products. The real-time monitoring of an illustrative chemical reaction indicated the formation of the precipitate by the absorption, differential phase, and scattering contrast images obtained from a single projection. Through these contrast channels, the formation of the precipitate along the mixing line of the reagents, the border between the solid and the solution, and the presence of the scattering structures of 100–200 nm sizes were observed. The measurements were performed in a flexible and robust setup, which can be tailored to various imaging applications at different time scales.
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spelling pubmed-86210682021-11-27 Single-Shot Multicontrast X-ray Imaging for In Situ Visualization of Chemical Reaction Products Zakharova, Margarita Mikhaylov, Andrey Vlnieska, Vitor Kunka, Danays J Imaging Article We present the application of single-shot multicontrast X-ray imaging with an inverted Hartmann mask to the time-resolved in situ visualization of chemical reaction products. The real-time monitoring of an illustrative chemical reaction indicated the formation of the precipitate by the absorption, differential phase, and scattering contrast images obtained from a single projection. Through these contrast channels, the formation of the precipitate along the mixing line of the reagents, the border between the solid and the solution, and the presence of the scattering structures of 100–200 nm sizes were observed. The measurements were performed in a flexible and robust setup, which can be tailored to various imaging applications at different time scales. MDPI 2021-10-23 /pmc/articles/PMC8621068/ /pubmed/34821852 http://dx.doi.org/10.3390/jimaging7110221 Text en © 2021 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Zakharova, Margarita
Mikhaylov, Andrey
Vlnieska, Vitor
Kunka, Danays
Single-Shot Multicontrast X-ray Imaging for In Situ Visualization of Chemical Reaction Products
title Single-Shot Multicontrast X-ray Imaging for In Situ Visualization of Chemical Reaction Products
title_full Single-Shot Multicontrast X-ray Imaging for In Situ Visualization of Chemical Reaction Products
title_fullStr Single-Shot Multicontrast X-ray Imaging for In Situ Visualization of Chemical Reaction Products
title_full_unstemmed Single-Shot Multicontrast X-ray Imaging for In Situ Visualization of Chemical Reaction Products
title_short Single-Shot Multicontrast X-ray Imaging for In Situ Visualization of Chemical Reaction Products
title_sort single-shot multicontrast x-ray imaging for in situ visualization of chemical reaction products
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8621068/
https://www.ncbi.nlm.nih.gov/pubmed/34821852
http://dx.doi.org/10.3390/jimaging7110221
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