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Single-Shot Multicontrast X-ray Imaging for In Situ Visualization of Chemical Reaction Products
We present the application of single-shot multicontrast X-ray imaging with an inverted Hartmann mask to the time-resolved in situ visualization of chemical reaction products. The real-time monitoring of an illustrative chemical reaction indicated the formation of the precipitate by the absorption, d...
Autores principales: | , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
MDPI
2021
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8621068/ https://www.ncbi.nlm.nih.gov/pubmed/34821852 http://dx.doi.org/10.3390/jimaging7110221 |
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author | Zakharova, Margarita Mikhaylov, Andrey Vlnieska, Vitor Kunka, Danays |
author_facet | Zakharova, Margarita Mikhaylov, Andrey Vlnieska, Vitor Kunka, Danays |
author_sort | Zakharova, Margarita |
collection | PubMed |
description | We present the application of single-shot multicontrast X-ray imaging with an inverted Hartmann mask to the time-resolved in situ visualization of chemical reaction products. The real-time monitoring of an illustrative chemical reaction indicated the formation of the precipitate by the absorption, differential phase, and scattering contrast images obtained from a single projection. Through these contrast channels, the formation of the precipitate along the mixing line of the reagents, the border between the solid and the solution, and the presence of the scattering structures of 100–200 nm sizes were observed. The measurements were performed in a flexible and robust setup, which can be tailored to various imaging applications at different time scales. |
format | Online Article Text |
id | pubmed-8621068 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2021 |
publisher | MDPI |
record_format | MEDLINE/PubMed |
spelling | pubmed-86210682021-11-27 Single-Shot Multicontrast X-ray Imaging for In Situ Visualization of Chemical Reaction Products Zakharova, Margarita Mikhaylov, Andrey Vlnieska, Vitor Kunka, Danays J Imaging Article We present the application of single-shot multicontrast X-ray imaging with an inverted Hartmann mask to the time-resolved in situ visualization of chemical reaction products. The real-time monitoring of an illustrative chemical reaction indicated the formation of the precipitate by the absorption, differential phase, and scattering contrast images obtained from a single projection. Through these contrast channels, the formation of the precipitate along the mixing line of the reagents, the border between the solid and the solution, and the presence of the scattering structures of 100–200 nm sizes were observed. The measurements were performed in a flexible and robust setup, which can be tailored to various imaging applications at different time scales. MDPI 2021-10-23 /pmc/articles/PMC8621068/ /pubmed/34821852 http://dx.doi.org/10.3390/jimaging7110221 Text en © 2021 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/). |
spellingShingle | Article Zakharova, Margarita Mikhaylov, Andrey Vlnieska, Vitor Kunka, Danays Single-Shot Multicontrast X-ray Imaging for In Situ Visualization of Chemical Reaction Products |
title | Single-Shot Multicontrast X-ray Imaging for In Situ Visualization of Chemical Reaction Products |
title_full | Single-Shot Multicontrast X-ray Imaging for In Situ Visualization of Chemical Reaction Products |
title_fullStr | Single-Shot Multicontrast X-ray Imaging for In Situ Visualization of Chemical Reaction Products |
title_full_unstemmed | Single-Shot Multicontrast X-ray Imaging for In Situ Visualization of Chemical Reaction Products |
title_short | Single-Shot Multicontrast X-ray Imaging for In Situ Visualization of Chemical Reaction Products |
title_sort | single-shot multicontrast x-ray imaging for in situ visualization of chemical reaction products |
topic | Article |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8621068/ https://www.ncbi.nlm.nih.gov/pubmed/34821852 http://dx.doi.org/10.3390/jimaging7110221 |
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