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Creating a Material Spectral Library for Plaster and Mortar Material Determination

Historic object analysis and the knowledge of composition play an important role in restoration processes. Based on this information, restoration works are conducted. This paper introduces a non-invasive technique of plaster and mortar material decomposition using reflectance spectroscopy. For this...

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Detalles Bibliográficos
Autores principales: Matoušková, Eva, Pavelka, Karel, Ibrahim, Saleem
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2021
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8621938/
https://www.ncbi.nlm.nih.gov/pubmed/34832427
http://dx.doi.org/10.3390/ma14227030
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author Matoušková, Eva
Pavelka, Karel
Ibrahim, Saleem
author_facet Matoušková, Eva
Pavelka, Karel
Ibrahim, Saleem
author_sort Matoušková, Eva
collection PubMed
description Historic object analysis and the knowledge of composition play an important role in restoration processes. Based on this information, restoration works are conducted. This paper introduces a non-invasive technique of plaster and mortar material decomposition using reflectance spectroscopy. For this purpose, a NIRQuest512-2,5 from Ocean Optics(®)/Ocean Insight(®), is used to create a unique spectral library consisting of various materials. They were carefully selected to include those that were and still are commonly used for a plaster and mortar production. Each material of the spectral library was mapped in detail, verified using scanning electronic microscope (SEM) data, and the results were compared to a previously determined spectral signature. The new spectral library was then tested on 11 unknown plaster and mortar samples and verified using a scanning electronic microscope. It was found that reflectance spectroscopy provides a powerful tool for plaster and mortar material decomposition, although at the moment it cannot fully replace invasive techniques like chemical analyses or other invasive techniques. It provides relevant information that can be used for restoration works.
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spelling pubmed-86219382021-11-27 Creating a Material Spectral Library for Plaster and Mortar Material Determination Matoušková, Eva Pavelka, Karel Ibrahim, Saleem Materials (Basel) Article Historic object analysis and the knowledge of composition play an important role in restoration processes. Based on this information, restoration works are conducted. This paper introduces a non-invasive technique of plaster and mortar material decomposition using reflectance spectroscopy. For this purpose, a NIRQuest512-2,5 from Ocean Optics(®)/Ocean Insight(®), is used to create a unique spectral library consisting of various materials. They were carefully selected to include those that were and still are commonly used for a plaster and mortar production. Each material of the spectral library was mapped in detail, verified using scanning electronic microscope (SEM) data, and the results were compared to a previously determined spectral signature. The new spectral library was then tested on 11 unknown plaster and mortar samples and verified using a scanning electronic microscope. It was found that reflectance spectroscopy provides a powerful tool for plaster and mortar material decomposition, although at the moment it cannot fully replace invasive techniques like chemical analyses or other invasive techniques. It provides relevant information that can be used for restoration works. MDPI 2021-11-19 /pmc/articles/PMC8621938/ /pubmed/34832427 http://dx.doi.org/10.3390/ma14227030 Text en © 2021 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Matoušková, Eva
Pavelka, Karel
Ibrahim, Saleem
Creating a Material Spectral Library for Plaster and Mortar Material Determination
title Creating a Material Spectral Library for Plaster and Mortar Material Determination
title_full Creating a Material Spectral Library for Plaster and Mortar Material Determination
title_fullStr Creating a Material Spectral Library for Plaster and Mortar Material Determination
title_full_unstemmed Creating a Material Spectral Library for Plaster and Mortar Material Determination
title_short Creating a Material Spectral Library for Plaster and Mortar Material Determination
title_sort creating a material spectral library for plaster and mortar material determination
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8621938/
https://www.ncbi.nlm.nih.gov/pubmed/34832427
http://dx.doi.org/10.3390/ma14227030
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