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Fast acquisition protocol for X-ray scattering tensor tomography

Microstructural information over an entire sample is important to understand the macroscopic behaviour of materials. X-ray scattering tensor tomography facilitates the investigation of the microstructural organisation in statistically large sample volumes. However, established acquisition protocols...

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Autores principales: Kim, Jisoo, Kagias, Matias, Marone, Federica, Shi, Zhitian, Stampanoni, Marco
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Nature Publishing Group UK 2021
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8629987/
https://www.ncbi.nlm.nih.gov/pubmed/34845280
http://dx.doi.org/10.1038/s41598-021-02467-w
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author Kim, Jisoo
Kagias, Matias
Marone, Federica
Shi, Zhitian
Stampanoni, Marco
author_facet Kim, Jisoo
Kagias, Matias
Marone, Federica
Shi, Zhitian
Stampanoni, Marco
author_sort Kim, Jisoo
collection PubMed
description Microstructural information over an entire sample is important to understand the macroscopic behaviour of materials. X-ray scattering tensor tomography facilitates the investigation of the microstructural organisation in statistically large sample volumes. However, established acquisition protocols based on scanning small-angle X-ray scattering and X-ray grating interferometry inherently require long scan times even with highly brilliant X-ray sources. Recent developments in X-ray diffractive optics towards circular pattern arrays enable fast single-shot acquisition of the sample scattering properties with 2D omnidirectional sensitivity. X-ray scattering tensor tomography with the use of this circular grating array has been demonstrated. We propose here simple yet inherently rapid acquisition protocols for X-ray scattering tensor tomography leveraging on these new optical elements. Results from both simulation and experimental data, supported by a null space analysis, suggest that the proposed acquisition protocols are not only rapid but also corroborate that sufficient information for the accurate volumetric reconstruction of the scattering properties is provided. The proposed acquisition protocols will build the basis for rapid inspection and/or time-resolved tensor tomography of the microstructural organisation over an extended field of view.
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spelling pubmed-86299872021-12-01 Fast acquisition protocol for X-ray scattering tensor tomography Kim, Jisoo Kagias, Matias Marone, Federica Shi, Zhitian Stampanoni, Marco Sci Rep Article Microstructural information over an entire sample is important to understand the macroscopic behaviour of materials. X-ray scattering tensor tomography facilitates the investigation of the microstructural organisation in statistically large sample volumes. However, established acquisition protocols based on scanning small-angle X-ray scattering and X-ray grating interferometry inherently require long scan times even with highly brilliant X-ray sources. Recent developments in X-ray diffractive optics towards circular pattern arrays enable fast single-shot acquisition of the sample scattering properties with 2D omnidirectional sensitivity. X-ray scattering tensor tomography with the use of this circular grating array has been demonstrated. We propose here simple yet inherently rapid acquisition protocols for X-ray scattering tensor tomography leveraging on these new optical elements. Results from both simulation and experimental data, supported by a null space analysis, suggest that the proposed acquisition protocols are not only rapid but also corroborate that sufficient information for the accurate volumetric reconstruction of the scattering properties is provided. The proposed acquisition protocols will build the basis for rapid inspection and/or time-resolved tensor tomography of the microstructural organisation over an extended field of view. Nature Publishing Group UK 2021-11-29 /pmc/articles/PMC8629987/ /pubmed/34845280 http://dx.doi.org/10.1038/s41598-021-02467-w Text en © The Author(s) 2021, corrected publication 2022 https://creativecommons.org/licenses/by/4.0/Open AccessThis article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons licence, and indicate if changes were made. The images or other third party material in this article are included in the article's Creative Commons licence, unless indicated otherwise in a credit line to the material. If material is not included in the article's Creative Commons licence and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this licence, visit http://creativecommons.org/licenses/by/4.0/ (https://creativecommons.org/licenses/by/4.0/) .
spellingShingle Article
Kim, Jisoo
Kagias, Matias
Marone, Federica
Shi, Zhitian
Stampanoni, Marco
Fast acquisition protocol for X-ray scattering tensor tomography
title Fast acquisition protocol for X-ray scattering tensor tomography
title_full Fast acquisition protocol for X-ray scattering tensor tomography
title_fullStr Fast acquisition protocol for X-ray scattering tensor tomography
title_full_unstemmed Fast acquisition protocol for X-ray scattering tensor tomography
title_short Fast acquisition protocol for X-ray scattering tensor tomography
title_sort fast acquisition protocol for x-ray scattering tensor tomography
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8629987/
https://www.ncbi.nlm.nih.gov/pubmed/34845280
http://dx.doi.org/10.1038/s41598-021-02467-w
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