Cargando…
Fast acquisition protocol for X-ray scattering tensor tomography
Microstructural information over an entire sample is important to understand the macroscopic behaviour of materials. X-ray scattering tensor tomography facilitates the investigation of the microstructural organisation in statistically large sample volumes. However, established acquisition protocols...
Autores principales: | , , , , |
---|---|
Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
Nature Publishing Group UK
2021
|
Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8629987/ https://www.ncbi.nlm.nih.gov/pubmed/34845280 http://dx.doi.org/10.1038/s41598-021-02467-w |
_version_ | 1784607314413617152 |
---|---|
author | Kim, Jisoo Kagias, Matias Marone, Federica Shi, Zhitian Stampanoni, Marco |
author_facet | Kim, Jisoo Kagias, Matias Marone, Federica Shi, Zhitian Stampanoni, Marco |
author_sort | Kim, Jisoo |
collection | PubMed |
description | Microstructural information over an entire sample is important to understand the macroscopic behaviour of materials. X-ray scattering tensor tomography facilitates the investigation of the microstructural organisation in statistically large sample volumes. However, established acquisition protocols based on scanning small-angle X-ray scattering and X-ray grating interferometry inherently require long scan times even with highly brilliant X-ray sources. Recent developments in X-ray diffractive optics towards circular pattern arrays enable fast single-shot acquisition of the sample scattering properties with 2D omnidirectional sensitivity. X-ray scattering tensor tomography with the use of this circular grating array has been demonstrated. We propose here simple yet inherently rapid acquisition protocols for X-ray scattering tensor tomography leveraging on these new optical elements. Results from both simulation and experimental data, supported by a null space analysis, suggest that the proposed acquisition protocols are not only rapid but also corroborate that sufficient information for the accurate volumetric reconstruction of the scattering properties is provided. The proposed acquisition protocols will build the basis for rapid inspection and/or time-resolved tensor tomography of the microstructural organisation over an extended field of view. |
format | Online Article Text |
id | pubmed-8629987 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2021 |
publisher | Nature Publishing Group UK |
record_format | MEDLINE/PubMed |
spelling | pubmed-86299872021-12-01 Fast acquisition protocol for X-ray scattering tensor tomography Kim, Jisoo Kagias, Matias Marone, Federica Shi, Zhitian Stampanoni, Marco Sci Rep Article Microstructural information over an entire sample is important to understand the macroscopic behaviour of materials. X-ray scattering tensor tomography facilitates the investigation of the microstructural organisation in statistically large sample volumes. However, established acquisition protocols based on scanning small-angle X-ray scattering and X-ray grating interferometry inherently require long scan times even with highly brilliant X-ray sources. Recent developments in X-ray diffractive optics towards circular pattern arrays enable fast single-shot acquisition of the sample scattering properties with 2D omnidirectional sensitivity. X-ray scattering tensor tomography with the use of this circular grating array has been demonstrated. We propose here simple yet inherently rapid acquisition protocols for X-ray scattering tensor tomography leveraging on these new optical elements. Results from both simulation and experimental data, supported by a null space analysis, suggest that the proposed acquisition protocols are not only rapid but also corroborate that sufficient information for the accurate volumetric reconstruction of the scattering properties is provided. The proposed acquisition protocols will build the basis for rapid inspection and/or time-resolved tensor tomography of the microstructural organisation over an extended field of view. Nature Publishing Group UK 2021-11-29 /pmc/articles/PMC8629987/ /pubmed/34845280 http://dx.doi.org/10.1038/s41598-021-02467-w Text en © The Author(s) 2021, corrected publication 2022 https://creativecommons.org/licenses/by/4.0/Open AccessThis article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons licence, and indicate if changes were made. The images or other third party material in this article are included in the article's Creative Commons licence, unless indicated otherwise in a credit line to the material. If material is not included in the article's Creative Commons licence and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this licence, visit http://creativecommons.org/licenses/by/4.0/ (https://creativecommons.org/licenses/by/4.0/) . |
spellingShingle | Article Kim, Jisoo Kagias, Matias Marone, Federica Shi, Zhitian Stampanoni, Marco Fast acquisition protocol for X-ray scattering tensor tomography |
title | Fast acquisition protocol for X-ray scattering tensor tomography |
title_full | Fast acquisition protocol for X-ray scattering tensor tomography |
title_fullStr | Fast acquisition protocol for X-ray scattering tensor tomography |
title_full_unstemmed | Fast acquisition protocol for X-ray scattering tensor tomography |
title_short | Fast acquisition protocol for X-ray scattering tensor tomography |
title_sort | fast acquisition protocol for x-ray scattering tensor tomography |
topic | Article |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8629987/ https://www.ncbi.nlm.nih.gov/pubmed/34845280 http://dx.doi.org/10.1038/s41598-021-02467-w |
work_keys_str_mv | AT kimjisoo fastacquisitionprotocolforxrayscatteringtensortomography AT kagiasmatias fastacquisitionprotocolforxrayscatteringtensortomography AT maronefederica fastacquisitionprotocolforxrayscatteringtensortomography AT shizhitian fastacquisitionprotocolforxrayscatteringtensortomography AT stampanonimarco fastacquisitionprotocolforxrayscatteringtensortomography |