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Study on the Hot Deformation Characterization of Borated Stainless Steel by Hot Isostatic Pressing

Borated stainless steel (BSS) specimens have a boron content of 1.86 wt%, and are prepared by hot isostatic pressing (HIP) conducted at different temperatures, ranging from 1000 to 1100 °C and a constant true strain rate (0.01, 0.1, 1 and 10 s(−1)). These tests, with observations and microstructural...

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Autores principales: Pei, Yanbin, Qu, Xuanhui, Ge, Qilu, Wang, Tiejun
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2021
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8658134/
https://www.ncbi.nlm.nih.gov/pubmed/34885265
http://dx.doi.org/10.3390/ma14237110
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author Pei, Yanbin
Qu, Xuanhui
Ge, Qilu
Wang, Tiejun
author_facet Pei, Yanbin
Qu, Xuanhui
Ge, Qilu
Wang, Tiejun
author_sort Pei, Yanbin
collection PubMed
description Borated stainless steel (BSS) specimens have a boron content of 1.86 wt%, and are prepared by hot isostatic pressing (HIP) conducted at different temperatures, ranging from 1000 to 1100 °C and a constant true strain rate (0.01, 0.1, 1 and 10 s(−1)). These tests, with observations and microstructural analysis, have achieved the hot deformation characteristics and mechanisms of BSS. In this research, the activation energy (Q) and Zener–Hollomon parameter (Z) were contrasted against the flow curves: Q = 442.35 kJ/mol. The critical conditions associated with the initiation of dynamic recrystallization (DRX) for BSS were precisely calculated based on the function between the strain hardening rate with the flow stress: at different temperatures from 1000 to 1100 °C: the critical stresses were 146.69–254.77 MPa and the critical strains were 0.022–0.044. The facts show that the boron-containing phase of BSS prevented the onset of DRX, despite the saturated boron in the austenite initiated DRX. The microstructural analysis showed that hot deformation promoted the generation of borides, which differed from the initial microstructure of HIP. The inhomogeneous distribution of elements in the boron-containing phase was caused by hot compression.
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spelling pubmed-86581342021-12-10 Study on the Hot Deformation Characterization of Borated Stainless Steel by Hot Isostatic Pressing Pei, Yanbin Qu, Xuanhui Ge, Qilu Wang, Tiejun Materials (Basel) Article Borated stainless steel (BSS) specimens have a boron content of 1.86 wt%, and are prepared by hot isostatic pressing (HIP) conducted at different temperatures, ranging from 1000 to 1100 °C and a constant true strain rate (0.01, 0.1, 1 and 10 s(−1)). These tests, with observations and microstructural analysis, have achieved the hot deformation characteristics and mechanisms of BSS. In this research, the activation energy (Q) and Zener–Hollomon parameter (Z) were contrasted against the flow curves: Q = 442.35 kJ/mol. The critical conditions associated with the initiation of dynamic recrystallization (DRX) for BSS were precisely calculated based on the function between the strain hardening rate with the flow stress: at different temperatures from 1000 to 1100 °C: the critical stresses were 146.69–254.77 MPa and the critical strains were 0.022–0.044. The facts show that the boron-containing phase of BSS prevented the onset of DRX, despite the saturated boron in the austenite initiated DRX. The microstructural analysis showed that hot deformation promoted the generation of borides, which differed from the initial microstructure of HIP. The inhomogeneous distribution of elements in the boron-containing phase was caused by hot compression. MDPI 2021-11-23 /pmc/articles/PMC8658134/ /pubmed/34885265 http://dx.doi.org/10.3390/ma14237110 Text en © 2021 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Pei, Yanbin
Qu, Xuanhui
Ge, Qilu
Wang, Tiejun
Study on the Hot Deformation Characterization of Borated Stainless Steel by Hot Isostatic Pressing
title Study on the Hot Deformation Characterization of Borated Stainless Steel by Hot Isostatic Pressing
title_full Study on the Hot Deformation Characterization of Borated Stainless Steel by Hot Isostatic Pressing
title_fullStr Study on the Hot Deformation Characterization of Borated Stainless Steel by Hot Isostatic Pressing
title_full_unstemmed Study on the Hot Deformation Characterization of Borated Stainless Steel by Hot Isostatic Pressing
title_short Study on the Hot Deformation Characterization of Borated Stainless Steel by Hot Isostatic Pressing
title_sort study on the hot deformation characterization of borated stainless steel by hot isostatic pressing
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8658134/
https://www.ncbi.nlm.nih.gov/pubmed/34885265
http://dx.doi.org/10.3390/ma14237110
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