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Increase of Solid Polymer Electrolyte Ionic Conductivity Using Nano-SiO(2) Synthesized from Sugarcane Bagasse as Filler

The synthesize of solid polymer electrolyte (SPE) based on polyethylene oxide (PEO), NaClO(4) and nano-SiO(2) was carried out by solution cast technique. Nano-SiO(2) was synthesized from sugarcane bagasse using sol-gel method. FTIR analysis was carried out to investigate the bonding between nano-SiO...

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Autores principales: Ni’mah, Yatim Lailun, Muhaiminah, Zakkiyyah Hidayatul, Suprapto, Suprapto
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2021
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8659504/
https://www.ncbi.nlm.nih.gov/pubmed/34883743
http://dx.doi.org/10.3390/polym13234240
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author Ni’mah, Yatim Lailun
Muhaiminah, Zakkiyyah Hidayatul
Suprapto, Suprapto
author_facet Ni’mah, Yatim Lailun
Muhaiminah, Zakkiyyah Hidayatul
Suprapto, Suprapto
author_sort Ni’mah, Yatim Lailun
collection PubMed
description The synthesize of solid polymer electrolyte (SPE) based on polyethylene oxide (PEO), NaClO(4) and nano-SiO(2) was carried out by solution cast technique. Nano-SiO(2) was synthesized from sugarcane bagasse using sol-gel method. FTIR analysis was carried out to investigate the bonding between nano-SiO(2) and PEO/NaClO(4). The morphology of the SPE was characterized using SEM. XRD and DSC analysis showed that SPE crystallinity decreased as nano-SiO(2) concentration was increased. Mechanical analyses were conducted to characterize the SPE tensile strength and elongation at break. EIS analysis was conducted to measure SPE ionic conductivity. The PEO/NaClO(4) SPE with the addition of 5% nano-SiO(2) from sugarcane bagasse at 60 °C produced SPE with the highest ionic conductivity, 1.18 × 10(−6) S/cm. It was concluded that the addition of nano-SiO(2) increased ionic conductivity and interface stability at the solid polymer electrolyte-PEO/NaClO(4).
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spelling pubmed-86595042021-12-10 Increase of Solid Polymer Electrolyte Ionic Conductivity Using Nano-SiO(2) Synthesized from Sugarcane Bagasse as Filler Ni’mah, Yatim Lailun Muhaiminah, Zakkiyyah Hidayatul Suprapto, Suprapto Polymers (Basel) Article The synthesize of solid polymer electrolyte (SPE) based on polyethylene oxide (PEO), NaClO(4) and nano-SiO(2) was carried out by solution cast technique. Nano-SiO(2) was synthesized from sugarcane bagasse using sol-gel method. FTIR analysis was carried out to investigate the bonding between nano-SiO(2) and PEO/NaClO(4). The morphology of the SPE was characterized using SEM. XRD and DSC analysis showed that SPE crystallinity decreased as nano-SiO(2) concentration was increased. Mechanical analyses were conducted to characterize the SPE tensile strength and elongation at break. EIS analysis was conducted to measure SPE ionic conductivity. The PEO/NaClO(4) SPE with the addition of 5% nano-SiO(2) from sugarcane bagasse at 60 °C produced SPE with the highest ionic conductivity, 1.18 × 10(−6) S/cm. It was concluded that the addition of nano-SiO(2) increased ionic conductivity and interface stability at the solid polymer electrolyte-PEO/NaClO(4). MDPI 2021-12-03 /pmc/articles/PMC8659504/ /pubmed/34883743 http://dx.doi.org/10.3390/polym13234240 Text en © 2021 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Ni’mah, Yatim Lailun
Muhaiminah, Zakkiyyah Hidayatul
Suprapto, Suprapto
Increase of Solid Polymer Electrolyte Ionic Conductivity Using Nano-SiO(2) Synthesized from Sugarcane Bagasse as Filler
title Increase of Solid Polymer Electrolyte Ionic Conductivity Using Nano-SiO(2) Synthesized from Sugarcane Bagasse as Filler
title_full Increase of Solid Polymer Electrolyte Ionic Conductivity Using Nano-SiO(2) Synthesized from Sugarcane Bagasse as Filler
title_fullStr Increase of Solid Polymer Electrolyte Ionic Conductivity Using Nano-SiO(2) Synthesized from Sugarcane Bagasse as Filler
title_full_unstemmed Increase of Solid Polymer Electrolyte Ionic Conductivity Using Nano-SiO(2) Synthesized from Sugarcane Bagasse as Filler
title_short Increase of Solid Polymer Electrolyte Ionic Conductivity Using Nano-SiO(2) Synthesized from Sugarcane Bagasse as Filler
title_sort increase of solid polymer electrolyte ionic conductivity using nano-sio(2) synthesized from sugarcane bagasse as filler
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8659504/
https://www.ncbi.nlm.nih.gov/pubmed/34883743
http://dx.doi.org/10.3390/polym13234240
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