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Increase of Solid Polymer Electrolyte Ionic Conductivity Using Nano-SiO(2) Synthesized from Sugarcane Bagasse as Filler
The synthesize of solid polymer electrolyte (SPE) based on polyethylene oxide (PEO), NaClO(4) and nano-SiO(2) was carried out by solution cast technique. Nano-SiO(2) was synthesized from sugarcane bagasse using sol-gel method. FTIR analysis was carried out to investigate the bonding between nano-SiO...
Autores principales: | , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
MDPI
2021
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8659504/ https://www.ncbi.nlm.nih.gov/pubmed/34883743 http://dx.doi.org/10.3390/polym13234240 |
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author | Ni’mah, Yatim Lailun Muhaiminah, Zakkiyyah Hidayatul Suprapto, Suprapto |
author_facet | Ni’mah, Yatim Lailun Muhaiminah, Zakkiyyah Hidayatul Suprapto, Suprapto |
author_sort | Ni’mah, Yatim Lailun |
collection | PubMed |
description | The synthesize of solid polymer electrolyte (SPE) based on polyethylene oxide (PEO), NaClO(4) and nano-SiO(2) was carried out by solution cast technique. Nano-SiO(2) was synthesized from sugarcane bagasse using sol-gel method. FTIR analysis was carried out to investigate the bonding between nano-SiO(2) and PEO/NaClO(4). The morphology of the SPE was characterized using SEM. XRD and DSC analysis showed that SPE crystallinity decreased as nano-SiO(2) concentration was increased. Mechanical analyses were conducted to characterize the SPE tensile strength and elongation at break. EIS analysis was conducted to measure SPE ionic conductivity. The PEO/NaClO(4) SPE with the addition of 5% nano-SiO(2) from sugarcane bagasse at 60 °C produced SPE with the highest ionic conductivity, 1.18 × 10(−6) S/cm. It was concluded that the addition of nano-SiO(2) increased ionic conductivity and interface stability at the solid polymer electrolyte-PEO/NaClO(4). |
format | Online Article Text |
id | pubmed-8659504 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2021 |
publisher | MDPI |
record_format | MEDLINE/PubMed |
spelling | pubmed-86595042021-12-10 Increase of Solid Polymer Electrolyte Ionic Conductivity Using Nano-SiO(2) Synthesized from Sugarcane Bagasse as Filler Ni’mah, Yatim Lailun Muhaiminah, Zakkiyyah Hidayatul Suprapto, Suprapto Polymers (Basel) Article The synthesize of solid polymer electrolyte (SPE) based on polyethylene oxide (PEO), NaClO(4) and nano-SiO(2) was carried out by solution cast technique. Nano-SiO(2) was synthesized from sugarcane bagasse using sol-gel method. FTIR analysis was carried out to investigate the bonding between nano-SiO(2) and PEO/NaClO(4). The morphology of the SPE was characterized using SEM. XRD and DSC analysis showed that SPE crystallinity decreased as nano-SiO(2) concentration was increased. Mechanical analyses were conducted to characterize the SPE tensile strength and elongation at break. EIS analysis was conducted to measure SPE ionic conductivity. The PEO/NaClO(4) SPE with the addition of 5% nano-SiO(2) from sugarcane bagasse at 60 °C produced SPE with the highest ionic conductivity, 1.18 × 10(−6) S/cm. It was concluded that the addition of nano-SiO(2) increased ionic conductivity and interface stability at the solid polymer electrolyte-PEO/NaClO(4). MDPI 2021-12-03 /pmc/articles/PMC8659504/ /pubmed/34883743 http://dx.doi.org/10.3390/polym13234240 Text en © 2021 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/). |
spellingShingle | Article Ni’mah, Yatim Lailun Muhaiminah, Zakkiyyah Hidayatul Suprapto, Suprapto Increase of Solid Polymer Electrolyte Ionic Conductivity Using Nano-SiO(2) Synthesized from Sugarcane Bagasse as Filler |
title | Increase of Solid Polymer Electrolyte Ionic Conductivity Using Nano-SiO(2) Synthesized from Sugarcane Bagasse as Filler |
title_full | Increase of Solid Polymer Electrolyte Ionic Conductivity Using Nano-SiO(2) Synthesized from Sugarcane Bagasse as Filler |
title_fullStr | Increase of Solid Polymer Electrolyte Ionic Conductivity Using Nano-SiO(2) Synthesized from Sugarcane Bagasse as Filler |
title_full_unstemmed | Increase of Solid Polymer Electrolyte Ionic Conductivity Using Nano-SiO(2) Synthesized from Sugarcane Bagasse as Filler |
title_short | Increase of Solid Polymer Electrolyte Ionic Conductivity Using Nano-SiO(2) Synthesized from Sugarcane Bagasse as Filler |
title_sort | increase of solid polymer electrolyte ionic conductivity using nano-sio(2) synthesized from sugarcane bagasse as filler |
topic | Article |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8659504/ https://www.ncbi.nlm.nih.gov/pubmed/34883743 http://dx.doi.org/10.3390/polym13234240 |
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