Laser synthesis: a solvent-free approach for the preparation of phenylthiazolo[5,4-b]pyridine derivatives

We describe here a rapid and straightforward solvent-free method to access phenylthiazolo[5,4-b]pyridines using a Nd-YAG laser NANO-NY81-10 (λ = 355 nm, 10 Hz pulse frequency; 8 ns pulse duration). This newly presented method successfully brings several improvements to the laser assisted synthesis o...

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Detalles Bibliográficos
Autores principales: Jemili, Rihab, Campos, Joana F., Dumuis, Nicolas, Rabat, Hervé, Semmar, Nadjib, Berteina-Raboin, Sabine
Formato: Online Artículo Texto
Lenguaje:English
Publicado: The Royal Society of Chemistry 2021
Materias:
Chemistry
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8694535/
https://www.ncbi.nlm.nih.gov/pubmed/35424455
http://dx.doi.org/10.1039/d0ra10094c
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author Jemili, Rihab
Campos, Joana F.
Dumuis, Nicolas
Rabat, Hervé
Semmar, Nadjib
Berteina-Raboin, Sabine
author_facet Jemili, Rihab
Campos, Joana F.
Dumuis, Nicolas
Rabat, Hervé
Semmar, Nadjib
Berteina-Raboin, Sabine
author_sort Jemili, Rihab
collection PubMed
description We describe here a rapid and straightforward solvent-free method to access phenylthiazolo[5,4-b]pyridines using a Nd-YAG laser NANO-NY81-10 (λ = 355 nm, 10 Hz pulse frequency; 8 ns pulse duration). This newly presented method successfully brings several improvements to the laser assisted synthesis of N,S-heterocycles. We are able to provide a solvent-, metal- and base-free method with good yield and a substantial reduction in reaction time.
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spelling pubmed-86945352022-04-13 Laser synthesis: a solvent-free approach for the preparation of phenylthiazolo[5,4-b]pyridine derivatives Jemili, Rihab Campos, Joana F. Dumuis, Nicolas Rabat, Hervé Semmar, Nadjib Berteina-Raboin, Sabine RSC Adv Chemistry We describe here a rapid and straightforward solvent-free method to access phenylthiazolo[5,4-b]pyridines using a Nd-YAG laser NANO-NY81-10 (λ = 355 nm, 10 Hz pulse frequency; 8 ns pulse duration). This newly presented method successfully brings several improvements to the laser assisted synthesis of N,S-heterocycles. We are able to provide a solvent-, metal- and base-free method with good yield and a substantial reduction in reaction time. The Royal Society of Chemistry 2021-01-27 /pmc/articles/PMC8694535/ /pubmed/35424455 http://dx.doi.org/10.1039/d0ra10094c Text en This journal is © The Royal Society of Chemistry https://creativecommons.org/licenses/by-nc/3.0/
spellingShingle Chemistry
Jemili, Rihab
Campos, Joana F.
Dumuis, Nicolas
Rabat, Hervé
Semmar, Nadjib
Berteina-Raboin, Sabine
Laser synthesis: a solvent-free approach for the preparation of phenylthiazolo[5,4-b]pyridine derivatives
title Laser synthesis: a solvent-free approach for the preparation of phenylthiazolo[5,4-b]pyridine derivatives
title_full Laser synthesis: a solvent-free approach for the preparation of phenylthiazolo[5,4-b]pyridine derivatives
title_fullStr Laser synthesis: a solvent-free approach for the preparation of phenylthiazolo[5,4-b]pyridine derivatives
title_full_unstemmed Laser synthesis: a solvent-free approach for the preparation of phenylthiazolo[5,4-b]pyridine derivatives
title_short Laser synthesis: a solvent-free approach for the preparation of phenylthiazolo[5,4-b]pyridine derivatives
title_sort laser synthesis: a solvent-free approach for the preparation of phenylthiazolo[5,4-b]pyridine derivatives
topic Chemistry
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8694535/
https://www.ncbi.nlm.nih.gov/pubmed/35424455
http://dx.doi.org/10.1039/d0ra10094c
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