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Monomer Elution from Three Resin Composites at Two Different Time Interval Using High Performance Liquid Chromatography—An In-Vitro Study
Esthetics, improved colour stability and ease of contour have made photo-activated resin based restorative materials being widely used in routine dental clinical practice. Perhaps improper and inadequate polymerization of resin based composite material might lead to elution of monomer. Thus, the aim...
Autores principales: | , , , , , , , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
MDPI
2021
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8704455/ https://www.ncbi.nlm.nih.gov/pubmed/34960944 http://dx.doi.org/10.3390/polym13244395 |
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author | Janani, Krishnamachari Teja, Kavalipurapu Venkata Sandhya, Raghu Alam, Mohammad Khursheed Al-Qaisi, Ruba K. Shrivastava, Deepti Alnusayri, Mohammed Odhayd Alkhalaf, Zainab Ali Sghaireen, Mohammed G. Srivastava, Kumar Chandan |
author_facet | Janani, Krishnamachari Teja, Kavalipurapu Venkata Sandhya, Raghu Alam, Mohammad Khursheed Al-Qaisi, Ruba K. Shrivastava, Deepti Alnusayri, Mohammed Odhayd Alkhalaf, Zainab Ali Sghaireen, Mohammed G. Srivastava, Kumar Chandan |
author_sort | Janani, Krishnamachari |
collection | PubMed |
description | Esthetics, improved colour stability and ease of contour have made photo-activated resin based restorative materials being widely used in routine dental clinical practice. Perhaps improper and inadequate polymerization of resin based composite material might lead to elution of monomer. Thus, the aim of the current study was to quantify the monomer elution from three resin composites. The intended analysis was made using high performance liquid chromatography (HPLC) at two different time periods. Three different materials that were investigated in the current study included Swiss Tech resin composite (Group A), Ceram X (Group B) and Beautifil Injectable composite (Group C). Ten cylindrical samples were fabricated in each study group. In 75% wt of ethanol, the samples were ingressed immediately and stored at room temperature. A 0.5 mL of the samples was assessed at pre-defined time intervals at 24 h and 7th day. Later, assessment of the samples was performed with HPLC and the data was analyzed using statistical test. Bisphenol A-glycidyl methacrylate (Bis-GMA), Triethylene glycol dimethacrylate (TEGDMA), 2-hydroxyethyl methacrylate (HEMA) and Urethane dimethacrylate (UDMA) were quantified in the samples. When analyzing the release monomer, it was found that at the end of 24 h Bis-GMA was eluted more in the injectable resin composite whereas, TEGDMA was eluted from Swiss Tech and Ceram X resin composites. At the end of the 7th day it was evident that Bis-GMA was eluted maximum in all the three resin composites. Thus, monomer release was found to be evident among all three resin composites and it is of utmost important to be assessed in routine clinical practice. |
format | Online Article Text |
id | pubmed-8704455 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2021 |
publisher | MDPI |
record_format | MEDLINE/PubMed |
spelling | pubmed-87044552021-12-25 Monomer Elution from Three Resin Composites at Two Different Time Interval Using High Performance Liquid Chromatography—An In-Vitro Study Janani, Krishnamachari Teja, Kavalipurapu Venkata Sandhya, Raghu Alam, Mohammad Khursheed Al-Qaisi, Ruba K. Shrivastava, Deepti Alnusayri, Mohammed Odhayd Alkhalaf, Zainab Ali Sghaireen, Mohammed G. Srivastava, Kumar Chandan Polymers (Basel) Article Esthetics, improved colour stability and ease of contour have made photo-activated resin based restorative materials being widely used in routine dental clinical practice. Perhaps improper and inadequate polymerization of resin based composite material might lead to elution of monomer. Thus, the aim of the current study was to quantify the monomer elution from three resin composites. The intended analysis was made using high performance liquid chromatography (HPLC) at two different time periods. Three different materials that were investigated in the current study included Swiss Tech resin composite (Group A), Ceram X (Group B) and Beautifil Injectable composite (Group C). Ten cylindrical samples were fabricated in each study group. In 75% wt of ethanol, the samples were ingressed immediately and stored at room temperature. A 0.5 mL of the samples was assessed at pre-defined time intervals at 24 h and 7th day. Later, assessment of the samples was performed with HPLC and the data was analyzed using statistical test. Bisphenol A-glycidyl methacrylate (Bis-GMA), Triethylene glycol dimethacrylate (TEGDMA), 2-hydroxyethyl methacrylate (HEMA) and Urethane dimethacrylate (UDMA) were quantified in the samples. When analyzing the release monomer, it was found that at the end of 24 h Bis-GMA was eluted more in the injectable resin composite whereas, TEGDMA was eluted from Swiss Tech and Ceram X resin composites. At the end of the 7th day it was evident that Bis-GMA was eluted maximum in all the three resin composites. Thus, monomer release was found to be evident among all three resin composites and it is of utmost important to be assessed in routine clinical practice. MDPI 2021-12-15 /pmc/articles/PMC8704455/ /pubmed/34960944 http://dx.doi.org/10.3390/polym13244395 Text en © 2021 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/). |
spellingShingle | Article Janani, Krishnamachari Teja, Kavalipurapu Venkata Sandhya, Raghu Alam, Mohammad Khursheed Al-Qaisi, Ruba K. Shrivastava, Deepti Alnusayri, Mohammed Odhayd Alkhalaf, Zainab Ali Sghaireen, Mohammed G. Srivastava, Kumar Chandan Monomer Elution from Three Resin Composites at Two Different Time Interval Using High Performance Liquid Chromatography—An In-Vitro Study |
title | Monomer Elution from Three Resin Composites at Two Different Time Interval Using High Performance Liquid Chromatography—An In-Vitro Study |
title_full | Monomer Elution from Three Resin Composites at Two Different Time Interval Using High Performance Liquid Chromatography—An In-Vitro Study |
title_fullStr | Monomer Elution from Three Resin Composites at Two Different Time Interval Using High Performance Liquid Chromatography—An In-Vitro Study |
title_full_unstemmed | Monomer Elution from Three Resin Composites at Two Different Time Interval Using High Performance Liquid Chromatography—An In-Vitro Study |
title_short | Monomer Elution from Three Resin Composites at Two Different Time Interval Using High Performance Liquid Chromatography—An In-Vitro Study |
title_sort | monomer elution from three resin composites at two different time interval using high performance liquid chromatography—an in-vitro study |
topic | Article |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8704455/ https://www.ncbi.nlm.nih.gov/pubmed/34960944 http://dx.doi.org/10.3390/polym13244395 |
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