Cargando…

Accessing new polymorphs and solvates through solvothermal recrystallization

In high-pressure structural chemistry, recrystallization techniques have been shown to be a powerful way of generating new polymorphs and solvates. A recent study by Olejniczak et al. [ IUCrJ (2022), 9, 49–54] on the pyridazine-based compound 6-chloro-1,2,3,4-tetrazolo[1,5-b]pyridazine (C(4)H(2)N(5)...

Descripción completa

Detalles Bibliográficos
Autor principal: Allan, David R.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2021
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8733882/
https://www.ncbi.nlm.nih.gov/pubmed/35059203
http://dx.doi.org/10.1107/S2052252521012835
_version_ 1784627895637901312
author Allan, David R.
author_facet Allan, David R.
author_sort Allan, David R.
collection PubMed
description In high-pressure structural chemistry, recrystallization techniques have been shown to be a powerful way of generating new polymorphs and solvates. A recent study by Olejniczak et al. [ IUCrJ (2022), 9, 49–54] on the pyridazine-based compound 6-chloro-1,2,3,4-tetrazolo[1,5-b]pyridazine (C(4)H(2)N(5)Cl or CTP) uses these solvothermal techniques to establish the phase behaviour of CTP and the effects of partial hydration.
format Online
Article
Text
id pubmed-8733882
institution National Center for Biotechnology Information
language English
publishDate 2021
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-87338822022-01-19 Accessing new polymorphs and solvates through solvothermal recrystallization Allan, David R. IUCrJ Scientific Commentaries In high-pressure structural chemistry, recrystallization techniques have been shown to be a powerful way of generating new polymorphs and solvates. A recent study by Olejniczak et al. [ IUCrJ (2022), 9, 49–54] on the pyridazine-based compound 6-chloro-1,2,3,4-tetrazolo[1,5-b]pyridazine (C(4)H(2)N(5)Cl or CTP) uses these solvothermal techniques to establish the phase behaviour of CTP and the effects of partial hydration. International Union of Crystallography 2021-12-16 /pmc/articles/PMC8733882/ /pubmed/35059203 http://dx.doi.org/10.1107/S2052252521012835 Text en © David R. Allan 2022 https://creativecommons.org/licenses/by/4.0/This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Scientific Commentaries
Allan, David R.
Accessing new polymorphs and solvates through solvothermal recrystallization
title Accessing new polymorphs and solvates through solvothermal recrystallization
title_full Accessing new polymorphs and solvates through solvothermal recrystallization
title_fullStr Accessing new polymorphs and solvates through solvothermal recrystallization
title_full_unstemmed Accessing new polymorphs and solvates through solvothermal recrystallization
title_short Accessing new polymorphs and solvates through solvothermal recrystallization
title_sort accessing new polymorphs and solvates through solvothermal recrystallization
topic Scientific Commentaries
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8733882/
https://www.ncbi.nlm.nih.gov/pubmed/35059203
http://dx.doi.org/10.1107/S2052252521012835
work_keys_str_mv AT allandavidr accessingnewpolymorphsandsolvatesthroughsolvothermalrecrystallization