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A Robust Miniaturized Gas Sensor for H(2) and CO(2) Detection Based on the 3ω Method

Gas concentration monitoring is essential in industrial or life science areas in order to address safety-relevant or process-related questions. Many of the sensors used in this context are based on the principle of thermal conductivity. The [Formula: see text]-method is a very accurate method to det...

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Detalles Bibliográficos
Autores principales: Berndt, Dominik, Muggli, Josef, Heckel, Robert, Rahiman, Mohd Fuad, Lindner, Matthias, Heinrich, Stephan, Plöchinger, Heinz, Schreiner, Rupert
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8780541/
https://www.ncbi.nlm.nih.gov/pubmed/35062446
http://dx.doi.org/10.3390/s22020485
Descripción
Sumario:Gas concentration monitoring is essential in industrial or life science areas in order to address safety-relevant or process-related questions. Many of the sensors used in this context are based on the principle of thermal conductivity. The [Formula: see text]-method is a very accurate method to determine the thermal properties of materials. It has its origin in the thermal characterization of thin solid films. To date, there have been very few scientific investigations using this method to determine the thermal properties of gases and to apply it to gas measurement technology. In this article, we use two exemplary gases ([Formula: see text] and [Formula: see text]) for a systematical investigation of this method in the context of gas analysis. To perform our experiments, we use a robust, reliable sensing element that is already well established in vacuum measurement technology. This helix-shaped thin wire of tungsten exhibits high robustness against chemical and mechanical influences. Our setup features a compact measurement environment, where sensor operation and data acquisition are integrated into a single device. The experimental results show a good agreement with a simplified analytical model and FEM simulations. The sensor exhibits a lower detection limit of 0.62% in the case of [Formula: see text] , and only 0.062% in case the of [Formula: see text] at an excitation frequency of 1 [Formula: see text]. This is one of the lowest values reported in literature for thermal conductivity [Formula: see text] sensors.