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A Robust Miniaturized Gas Sensor for H(2) and CO(2) Detection Based on the 3ω Method

Gas concentration monitoring is essential in industrial or life science areas in order to address safety-relevant or process-related questions. Many of the sensors used in this context are based on the principle of thermal conductivity. The [Formula: see text]-method is a very accurate method to det...

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Autores principales: Berndt, Dominik, Muggli, Josef, Heckel, Robert, Rahiman, Mohd Fuad, Lindner, Matthias, Heinrich, Stephan, Plöchinger, Heinz, Schreiner, Rupert
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8780541/
https://www.ncbi.nlm.nih.gov/pubmed/35062446
http://dx.doi.org/10.3390/s22020485
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author Berndt, Dominik
Muggli, Josef
Heckel, Robert
Rahiman, Mohd Fuad
Lindner, Matthias
Heinrich, Stephan
Plöchinger, Heinz
Schreiner, Rupert
author_facet Berndt, Dominik
Muggli, Josef
Heckel, Robert
Rahiman, Mohd Fuad
Lindner, Matthias
Heinrich, Stephan
Plöchinger, Heinz
Schreiner, Rupert
author_sort Berndt, Dominik
collection PubMed
description Gas concentration monitoring is essential in industrial or life science areas in order to address safety-relevant or process-related questions. Many of the sensors used in this context are based on the principle of thermal conductivity. The [Formula: see text]-method is a very accurate method to determine the thermal properties of materials. It has its origin in the thermal characterization of thin solid films. To date, there have been very few scientific investigations using this method to determine the thermal properties of gases and to apply it to gas measurement technology. In this article, we use two exemplary gases ([Formula: see text] and [Formula: see text]) for a systematical investigation of this method in the context of gas analysis. To perform our experiments, we use a robust, reliable sensing element that is already well established in vacuum measurement technology. This helix-shaped thin wire of tungsten exhibits high robustness against chemical and mechanical influences. Our setup features a compact measurement environment, where sensor operation and data acquisition are integrated into a single device. The experimental results show a good agreement with a simplified analytical model and FEM simulations. The sensor exhibits a lower detection limit of 0.62% in the case of [Formula: see text] , and only 0.062% in case the of [Formula: see text] at an excitation frequency of 1 [Formula: see text]. This is one of the lowest values reported in literature for thermal conductivity [Formula: see text] sensors.
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spelling pubmed-87805412022-01-22 A Robust Miniaturized Gas Sensor for H(2) and CO(2) Detection Based on the 3ω Method Berndt, Dominik Muggli, Josef Heckel, Robert Rahiman, Mohd Fuad Lindner, Matthias Heinrich, Stephan Plöchinger, Heinz Schreiner, Rupert Sensors (Basel) Article Gas concentration monitoring is essential in industrial or life science areas in order to address safety-relevant or process-related questions. Many of the sensors used in this context are based on the principle of thermal conductivity. The [Formula: see text]-method is a very accurate method to determine the thermal properties of materials. It has its origin in the thermal characterization of thin solid films. To date, there have been very few scientific investigations using this method to determine the thermal properties of gases and to apply it to gas measurement technology. In this article, we use two exemplary gases ([Formula: see text] and [Formula: see text]) for a systematical investigation of this method in the context of gas analysis. To perform our experiments, we use a robust, reliable sensing element that is already well established in vacuum measurement technology. This helix-shaped thin wire of tungsten exhibits high robustness against chemical and mechanical influences. Our setup features a compact measurement environment, where sensor operation and data acquisition are integrated into a single device. The experimental results show a good agreement with a simplified analytical model and FEM simulations. The sensor exhibits a lower detection limit of 0.62% in the case of [Formula: see text] , and only 0.062% in case the of [Formula: see text] at an excitation frequency of 1 [Formula: see text]. This is one of the lowest values reported in literature for thermal conductivity [Formula: see text] sensors. MDPI 2022-01-09 /pmc/articles/PMC8780541/ /pubmed/35062446 http://dx.doi.org/10.3390/s22020485 Text en © 2022 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Berndt, Dominik
Muggli, Josef
Heckel, Robert
Rahiman, Mohd Fuad
Lindner, Matthias
Heinrich, Stephan
Plöchinger, Heinz
Schreiner, Rupert
A Robust Miniaturized Gas Sensor for H(2) and CO(2) Detection Based on the 3ω Method
title A Robust Miniaturized Gas Sensor for H(2) and CO(2) Detection Based on the 3ω Method
title_full A Robust Miniaturized Gas Sensor for H(2) and CO(2) Detection Based on the 3ω Method
title_fullStr A Robust Miniaturized Gas Sensor for H(2) and CO(2) Detection Based on the 3ω Method
title_full_unstemmed A Robust Miniaturized Gas Sensor for H(2) and CO(2) Detection Based on the 3ω Method
title_short A Robust Miniaturized Gas Sensor for H(2) and CO(2) Detection Based on the 3ω Method
title_sort robust miniaturized gas sensor for h(2) and co(2) detection based on the 3ω method
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8780541/
https://www.ncbi.nlm.nih.gov/pubmed/35062446
http://dx.doi.org/10.3390/s22020485
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