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Performance of the time-resolved ultra-small-angle X-ray scattering beamline with the Extremely Brilliant Source
The new technical features and enhanced performance of the ID02 beamline with the Extremely Brilliant Source (EBS) at the ESRF are described. The beamline enables static and kinetic investigations of a broad range of systems from ångström to micrometre size scales and down to the sub-millisecond tim...
Autores principales: | , , , , , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
International Union of Crystallography
2022
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8805168/ https://www.ncbi.nlm.nih.gov/pubmed/35145357 http://dx.doi.org/10.1107/S1600576721012693 |
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author | Narayanan, Theyencheri Sztucki, Michael Zinn, Thomas Kieffer, Jérôme Homs-Puron, Alejandro Gorini, Jacques Van Vaerenbergh, Pierre Boesecke, Peter |
author_facet | Narayanan, Theyencheri Sztucki, Michael Zinn, Thomas Kieffer, Jérôme Homs-Puron, Alejandro Gorini, Jacques Van Vaerenbergh, Pierre Boesecke, Peter |
author_sort | Narayanan, Theyencheri |
collection | PubMed |
description | The new technical features and enhanced performance of the ID02 beamline with the Extremely Brilliant Source (EBS) at the ESRF are described. The beamline enables static and kinetic investigations of a broad range of systems from ångström to micrometre size scales and down to the sub-millisecond time range by combining different small-angle X-ray scattering techniques in a single instrument. In addition, a nearly coherent beam obtained in the high-resolution mode allows multispeckle X-ray photon correlation spectroscopy measurements down to the microsecond range over the ultra-small- and small-angle regions. While the scattering vector (of magnitude q) range covered is the same as before, 0.001 ≤ q ≤ 50 nm(−1) for an X-ray wavelength of 1 Å, the EBS permits relaxation of the collimation conditions, thereby obtaining a higher flux throughput and lower background. In particular, a coherent photon flux in excess of 10(12) photons s(−1) can be routinely obtained, allowing dynamic studies of relatively dilute samples. The enhanced beam properties are complemented by advanced pixel-array detectors and high-throughput data reduction pipelines. All these developments together open new opportunities for structural, dynamic and kinetic investigations of out-of-equilibrium soft matter and biophysical systems. |
format | Online Article Text |
id | pubmed-8805168 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2022 |
publisher | International Union of Crystallography |
record_format | MEDLINE/PubMed |
spelling | pubmed-88051682022-02-09 Performance of the time-resolved ultra-small-angle X-ray scattering beamline with the Extremely Brilliant Source Narayanan, Theyencheri Sztucki, Michael Zinn, Thomas Kieffer, Jérôme Homs-Puron, Alejandro Gorini, Jacques Van Vaerenbergh, Pierre Boesecke, Peter J Appl Crystallogr Research Papers The new technical features and enhanced performance of the ID02 beamline with the Extremely Brilliant Source (EBS) at the ESRF are described. The beamline enables static and kinetic investigations of a broad range of systems from ångström to micrometre size scales and down to the sub-millisecond time range by combining different small-angle X-ray scattering techniques in a single instrument. In addition, a nearly coherent beam obtained in the high-resolution mode allows multispeckle X-ray photon correlation spectroscopy measurements down to the microsecond range over the ultra-small- and small-angle regions. While the scattering vector (of magnitude q) range covered is the same as before, 0.001 ≤ q ≤ 50 nm(−1) for an X-ray wavelength of 1 Å, the EBS permits relaxation of the collimation conditions, thereby obtaining a higher flux throughput and lower background. In particular, a coherent photon flux in excess of 10(12) photons s(−1) can be routinely obtained, allowing dynamic studies of relatively dilute samples. The enhanced beam properties are complemented by advanced pixel-array detectors and high-throughput data reduction pipelines. All these developments together open new opportunities for structural, dynamic and kinetic investigations of out-of-equilibrium soft matter and biophysical systems. International Union of Crystallography 2022-02-01 /pmc/articles/PMC8805168/ /pubmed/35145357 http://dx.doi.org/10.1107/S1600576721012693 Text en © Theyencheri Narayanan et al. 2022 https://creativecommons.org/licenses/by/4.0/This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
spellingShingle | Research Papers Narayanan, Theyencheri Sztucki, Michael Zinn, Thomas Kieffer, Jérôme Homs-Puron, Alejandro Gorini, Jacques Van Vaerenbergh, Pierre Boesecke, Peter Performance of the time-resolved ultra-small-angle X-ray scattering beamline with the Extremely Brilliant Source |
title | Performance of the time-resolved ultra-small-angle X-ray scattering beamline with the Extremely Brilliant Source |
title_full | Performance of the time-resolved ultra-small-angle X-ray scattering beamline with the Extremely Brilliant Source |
title_fullStr | Performance of the time-resolved ultra-small-angle X-ray scattering beamline with the Extremely Brilliant Source |
title_full_unstemmed | Performance of the time-resolved ultra-small-angle X-ray scattering beamline with the Extremely Brilliant Source |
title_short | Performance of the time-resolved ultra-small-angle X-ray scattering beamline with the Extremely Brilliant Source |
title_sort | performance of the time-resolved ultra-small-angle x-ray scattering beamline with the extremely brilliant source |
topic | Research Papers |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8805168/ https://www.ncbi.nlm.nih.gov/pubmed/35145357 http://dx.doi.org/10.1107/S1600576721012693 |
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