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Synthesis, Characterization, and Supercapacitor Performance of a Mixed-Phase Mn-Doped MoS(2) Nanoflower

The fascinating features of 2D nanomaterials for various applications have prompted increasing research into single and few-layer metal dichalcogenides nanosheets using improved nanofabrication and characterization techniques. MoS(2) has recently been intensively examined among layered metal dichalc...

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Detalles Bibliográficos
Autores principales: Bello, Ismaila T., Otun, Kabir O., Nyongombe, Gayi, Adedokun, Oluwaseun, Kabongo, Guy L., Dhlamini, Mokhotjwa S.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8839322/
https://www.ncbi.nlm.nih.gov/pubmed/35159835
http://dx.doi.org/10.3390/nano12030490
Descripción
Sumario:The fascinating features of 2D nanomaterials for various applications have prompted increasing research into single and few-layer metal dichalcogenides nanosheets using improved nanofabrication and characterization techniques. MoS(2) has recently been intensively examined among layered metal dichalcogenides and other diverse transition metal-based materials, that have previously been studied in various applications. In this research, we report mixed-phase Mn-doped MoS(2) nanoflowers for supercapacitor performance studies. The confirmation of the successfully prepared Mn-doped MoS(2) nanoflowers was characterized by XRD, SEM-EDS, RAMAN, and BET research techniques. The mixed-phase of the as-synthesized electrode material was confirmed by the structural changes observed in the XRD and RAMAN studies. The surface area from the BET measurement was calculated to be 46.0628 m(2)/g, and the adsorption average pore size of the electrode material was 11.26607 nm. The electrochemical performance of the Mn-doped MoS(2) electrode material showed a pseudo-capacitive behavior, with a specific capacitance of 70.37 Fg(−1), and with a corresponding energy density of 3.14 Whkg(−1) and a power density of 4346.35 Wkg(−1). The performance of this metal-doped MoS(2)-based supercapacitor device can be attributed to its mixed phase, which requires further optimization in future works.