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Synthesis, Characterization, and Supercapacitor Performance of a Mixed-Phase Mn-Doped MoS(2) Nanoflower
The fascinating features of 2D nanomaterials for various applications have prompted increasing research into single and few-layer metal dichalcogenides nanosheets using improved nanofabrication and characterization techniques. MoS(2) has recently been intensively examined among layered metal dichalc...
Autores principales: | , , , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
MDPI
2022
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8839322/ https://www.ncbi.nlm.nih.gov/pubmed/35159835 http://dx.doi.org/10.3390/nano12030490 |
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author | Bello, Ismaila T. Otun, Kabir O. Nyongombe, Gayi Adedokun, Oluwaseun Kabongo, Guy L. Dhlamini, Mokhotjwa S. |
author_facet | Bello, Ismaila T. Otun, Kabir O. Nyongombe, Gayi Adedokun, Oluwaseun Kabongo, Guy L. Dhlamini, Mokhotjwa S. |
author_sort | Bello, Ismaila T. |
collection | PubMed |
description | The fascinating features of 2D nanomaterials for various applications have prompted increasing research into single and few-layer metal dichalcogenides nanosheets using improved nanofabrication and characterization techniques. MoS(2) has recently been intensively examined among layered metal dichalcogenides and other diverse transition metal-based materials, that have previously been studied in various applications. In this research, we report mixed-phase Mn-doped MoS(2) nanoflowers for supercapacitor performance studies. The confirmation of the successfully prepared Mn-doped MoS(2) nanoflowers was characterized by XRD, SEM-EDS, RAMAN, and BET research techniques. The mixed-phase of the as-synthesized electrode material was confirmed by the structural changes observed in the XRD and RAMAN studies. The surface area from the BET measurement was calculated to be 46.0628 m(2)/g, and the adsorption average pore size of the electrode material was 11.26607 nm. The electrochemical performance of the Mn-doped MoS(2) electrode material showed a pseudo-capacitive behavior, with a specific capacitance of 70.37 Fg(−1), and with a corresponding energy density of 3.14 Whkg(−1) and a power density of 4346.35 Wkg(−1). The performance of this metal-doped MoS(2)-based supercapacitor device can be attributed to its mixed phase, which requires further optimization in future works. |
format | Online Article Text |
id | pubmed-8839322 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2022 |
publisher | MDPI |
record_format | MEDLINE/PubMed |
spelling | pubmed-88393222022-02-13 Synthesis, Characterization, and Supercapacitor Performance of a Mixed-Phase Mn-Doped MoS(2) Nanoflower Bello, Ismaila T. Otun, Kabir O. Nyongombe, Gayi Adedokun, Oluwaseun Kabongo, Guy L. Dhlamini, Mokhotjwa S. Nanomaterials (Basel) Article The fascinating features of 2D nanomaterials for various applications have prompted increasing research into single and few-layer metal dichalcogenides nanosheets using improved nanofabrication and characterization techniques. MoS(2) has recently been intensively examined among layered metal dichalcogenides and other diverse transition metal-based materials, that have previously been studied in various applications. In this research, we report mixed-phase Mn-doped MoS(2) nanoflowers for supercapacitor performance studies. The confirmation of the successfully prepared Mn-doped MoS(2) nanoflowers was characterized by XRD, SEM-EDS, RAMAN, and BET research techniques. The mixed-phase of the as-synthesized electrode material was confirmed by the structural changes observed in the XRD and RAMAN studies. The surface area from the BET measurement was calculated to be 46.0628 m(2)/g, and the adsorption average pore size of the electrode material was 11.26607 nm. The electrochemical performance of the Mn-doped MoS(2) electrode material showed a pseudo-capacitive behavior, with a specific capacitance of 70.37 Fg(−1), and with a corresponding energy density of 3.14 Whkg(−1) and a power density of 4346.35 Wkg(−1). The performance of this metal-doped MoS(2)-based supercapacitor device can be attributed to its mixed phase, which requires further optimization in future works. MDPI 2022-01-29 /pmc/articles/PMC8839322/ /pubmed/35159835 http://dx.doi.org/10.3390/nano12030490 Text en © 2022 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/). |
spellingShingle | Article Bello, Ismaila T. Otun, Kabir O. Nyongombe, Gayi Adedokun, Oluwaseun Kabongo, Guy L. Dhlamini, Mokhotjwa S. Synthesis, Characterization, and Supercapacitor Performance of a Mixed-Phase Mn-Doped MoS(2) Nanoflower |
title | Synthesis, Characterization, and Supercapacitor Performance of a Mixed-Phase Mn-Doped MoS(2) Nanoflower |
title_full | Synthesis, Characterization, and Supercapacitor Performance of a Mixed-Phase Mn-Doped MoS(2) Nanoflower |
title_fullStr | Synthesis, Characterization, and Supercapacitor Performance of a Mixed-Phase Mn-Doped MoS(2) Nanoflower |
title_full_unstemmed | Synthesis, Characterization, and Supercapacitor Performance of a Mixed-Phase Mn-Doped MoS(2) Nanoflower |
title_short | Synthesis, Characterization, and Supercapacitor Performance of a Mixed-Phase Mn-Doped MoS(2) Nanoflower |
title_sort | synthesis, characterization, and supercapacitor performance of a mixed-phase mn-doped mos(2) nanoflower |
topic | Article |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8839322/ https://www.ncbi.nlm.nih.gov/pubmed/35159835 http://dx.doi.org/10.3390/nano12030490 |
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