Cargando…

Synthesis, Characterization, and Supercapacitor Performance of a Mixed-Phase Mn-Doped MoS(2) Nanoflower

The fascinating features of 2D nanomaterials for various applications have prompted increasing research into single and few-layer metal dichalcogenides nanosheets using improved nanofabrication and characterization techniques. MoS(2) has recently been intensively examined among layered metal dichalc...

Descripción completa

Detalles Bibliográficos
Autores principales: Bello, Ismaila T., Otun, Kabir O., Nyongombe, Gayi, Adedokun, Oluwaseun, Kabongo, Guy L., Dhlamini, Mokhotjwa S.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8839322/
https://www.ncbi.nlm.nih.gov/pubmed/35159835
http://dx.doi.org/10.3390/nano12030490
_version_ 1784650341556420608
author Bello, Ismaila T.
Otun, Kabir O.
Nyongombe, Gayi
Adedokun, Oluwaseun
Kabongo, Guy L.
Dhlamini, Mokhotjwa S.
author_facet Bello, Ismaila T.
Otun, Kabir O.
Nyongombe, Gayi
Adedokun, Oluwaseun
Kabongo, Guy L.
Dhlamini, Mokhotjwa S.
author_sort Bello, Ismaila T.
collection PubMed
description The fascinating features of 2D nanomaterials for various applications have prompted increasing research into single and few-layer metal dichalcogenides nanosheets using improved nanofabrication and characterization techniques. MoS(2) has recently been intensively examined among layered metal dichalcogenides and other diverse transition metal-based materials, that have previously been studied in various applications. In this research, we report mixed-phase Mn-doped MoS(2) nanoflowers for supercapacitor performance studies. The confirmation of the successfully prepared Mn-doped MoS(2) nanoflowers was characterized by XRD, SEM-EDS, RAMAN, and BET research techniques. The mixed-phase of the as-synthesized electrode material was confirmed by the structural changes observed in the XRD and RAMAN studies. The surface area from the BET measurement was calculated to be 46.0628 m(2)/g, and the adsorption average pore size of the electrode material was 11.26607 nm. The electrochemical performance of the Mn-doped MoS(2) electrode material showed a pseudo-capacitive behavior, with a specific capacitance of 70.37 Fg(−1), and with a corresponding energy density of 3.14 Whkg(−1) and a power density of 4346.35 Wkg(−1). The performance of this metal-doped MoS(2)-based supercapacitor device can be attributed to its mixed phase, which requires further optimization in future works.
format Online
Article
Text
id pubmed-8839322
institution National Center for Biotechnology Information
language English
publishDate 2022
publisher MDPI
record_format MEDLINE/PubMed
spelling pubmed-88393222022-02-13 Synthesis, Characterization, and Supercapacitor Performance of a Mixed-Phase Mn-Doped MoS(2) Nanoflower Bello, Ismaila T. Otun, Kabir O. Nyongombe, Gayi Adedokun, Oluwaseun Kabongo, Guy L. Dhlamini, Mokhotjwa S. Nanomaterials (Basel) Article The fascinating features of 2D nanomaterials for various applications have prompted increasing research into single and few-layer metal dichalcogenides nanosheets using improved nanofabrication and characterization techniques. MoS(2) has recently been intensively examined among layered metal dichalcogenides and other diverse transition metal-based materials, that have previously been studied in various applications. In this research, we report mixed-phase Mn-doped MoS(2) nanoflowers for supercapacitor performance studies. The confirmation of the successfully prepared Mn-doped MoS(2) nanoflowers was characterized by XRD, SEM-EDS, RAMAN, and BET research techniques. The mixed-phase of the as-synthesized electrode material was confirmed by the structural changes observed in the XRD and RAMAN studies. The surface area from the BET measurement was calculated to be 46.0628 m(2)/g, and the adsorption average pore size of the electrode material was 11.26607 nm. The electrochemical performance of the Mn-doped MoS(2) electrode material showed a pseudo-capacitive behavior, with a specific capacitance of 70.37 Fg(−1), and with a corresponding energy density of 3.14 Whkg(−1) and a power density of 4346.35 Wkg(−1). The performance of this metal-doped MoS(2)-based supercapacitor device can be attributed to its mixed phase, which requires further optimization in future works. MDPI 2022-01-29 /pmc/articles/PMC8839322/ /pubmed/35159835 http://dx.doi.org/10.3390/nano12030490 Text en © 2022 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Bello, Ismaila T.
Otun, Kabir O.
Nyongombe, Gayi
Adedokun, Oluwaseun
Kabongo, Guy L.
Dhlamini, Mokhotjwa S.
Synthesis, Characterization, and Supercapacitor Performance of a Mixed-Phase Mn-Doped MoS(2) Nanoflower
title Synthesis, Characterization, and Supercapacitor Performance of a Mixed-Phase Mn-Doped MoS(2) Nanoflower
title_full Synthesis, Characterization, and Supercapacitor Performance of a Mixed-Phase Mn-Doped MoS(2) Nanoflower
title_fullStr Synthesis, Characterization, and Supercapacitor Performance of a Mixed-Phase Mn-Doped MoS(2) Nanoflower
title_full_unstemmed Synthesis, Characterization, and Supercapacitor Performance of a Mixed-Phase Mn-Doped MoS(2) Nanoflower
title_short Synthesis, Characterization, and Supercapacitor Performance of a Mixed-Phase Mn-Doped MoS(2) Nanoflower
title_sort synthesis, characterization, and supercapacitor performance of a mixed-phase mn-doped mos(2) nanoflower
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8839322/
https://www.ncbi.nlm.nih.gov/pubmed/35159835
http://dx.doi.org/10.3390/nano12030490
work_keys_str_mv AT belloismailat synthesischaracterizationandsupercapacitorperformanceofamixedphasemndopedmos2nanoflower
AT otunkabiro synthesischaracterizationandsupercapacitorperformanceofamixedphasemndopedmos2nanoflower
AT nyongombegayi synthesischaracterizationandsupercapacitorperformanceofamixedphasemndopedmos2nanoflower
AT adedokunoluwaseun synthesischaracterizationandsupercapacitorperformanceofamixedphasemndopedmos2nanoflower
AT kabongoguyl synthesischaracterizationandsupercapacitorperformanceofamixedphasemndopedmos2nanoflower
AT dhlaminimokhotjwas synthesischaracterizationandsupercapacitorperformanceofamixedphasemndopedmos2nanoflower