Cargando…

Ionic Liquid-Based Low-Temperature Synthesis of Crystalline Ti(OH)OF·0.66H(2)O: Elucidating the Molecular Reaction Steps by NMR Spectroscopy and Theoretical Studies

[Image: see text] We present an in-depth mechanistic study of the first steps of the solution-based synthesis of the peculiar hexagonal tungsten bronze-type Ti(OH)OF·0.66H(2)O solid, using NMR analyses ((1)H, (13)C, (19)F, and (11)B) as well as modeling based on density functional theory (DFT) and a...

Descripción completa

Detalles Bibliográficos
Autores principales: Sieland, Melanie, Schenker, Manuel, Esser, Lars, Kirchner, Barbara, Smarsly, Bernd M.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: American Chemical Society 2022
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8851441/
https://www.ncbi.nlm.nih.gov/pubmed/35187350
http://dx.doi.org/10.1021/acsomega.1c06534

Ejemplares similares