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Corrosion and Microstructural Investigation on Additively Manufactured 316L Stainless Steel: Experimental and Statistical Approach

The use of metal additive manufacturing (AM) has strongly increased in the industry during the last years. More specifically, selective laser melting (SLM) is one of the most used techniques due to its numerous advantages compared to conventional processing methods. The purpose of this study is to i...

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Autores principales: Maicas-Esteve, Héctor, Taji, Iman, Wilms, Marc, Gonzalez-Garcia, Yaiza, Johnsen, Roy
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8877025/
https://www.ncbi.nlm.nih.gov/pubmed/35208144
http://dx.doi.org/10.3390/ma15041605
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author Maicas-Esteve, Héctor
Taji, Iman
Wilms, Marc
Gonzalez-Garcia, Yaiza
Johnsen, Roy
author_facet Maicas-Esteve, Héctor
Taji, Iman
Wilms, Marc
Gonzalez-Garcia, Yaiza
Johnsen, Roy
author_sort Maicas-Esteve, Héctor
collection PubMed
description The use of metal additive manufacturing (AM) has strongly increased in the industry during the last years. More specifically, selective laser melting (SLM) is one of the most used techniques due to its numerous advantages compared to conventional processing methods. The purpose of this study is to investigate the effects of process parameters on the microstructural and corrosion properties of the additively manufactured AISI 316L stainless steel. Porosity, surface roughness, hardness, and grain size were studied for specimens produced with energy densities ranging from 51.17 to 173.91 J/mm(3) that resulted from different combinations of processing parameters. Using experimental results and applying the Taguchi model, 99.38 J/mm(3) was determined as the optimal energy density needed to produce samples with almost no porosity. The following analysis of variance ANOVA confirmed the scanning speed as the most influential factor in reducing the porosity percentage, which had a 74.9% contribution, followed by the position along the building direction with 22.8%, and finally, the laser energy with 2.3%. The influence on corrosion resistance was obtained by performing cyclic potentiodynamic polarization tests (CPP) in a 3.5 wt % NaCl solution at room temperature for different energy densities and positions (Z axis). The corrosion properties of the AM samples were studied and compared to those obtained from the traditionally manufactured samples. The corrosion resistance of the samples worsened with the increase in the percentage of porosity. The process parameters have consequently been optimized and the database has been extended to improve the quality of the AM-produced parts in which microstructural heterogeneities were observed along the building direction.
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spelling pubmed-88770252022-02-26 Corrosion and Microstructural Investigation on Additively Manufactured 316L Stainless Steel: Experimental and Statistical Approach Maicas-Esteve, Héctor Taji, Iman Wilms, Marc Gonzalez-Garcia, Yaiza Johnsen, Roy Materials (Basel) Article The use of metal additive manufacturing (AM) has strongly increased in the industry during the last years. More specifically, selective laser melting (SLM) is one of the most used techniques due to its numerous advantages compared to conventional processing methods. The purpose of this study is to investigate the effects of process parameters on the microstructural and corrosion properties of the additively manufactured AISI 316L stainless steel. Porosity, surface roughness, hardness, and grain size were studied for specimens produced with energy densities ranging from 51.17 to 173.91 J/mm(3) that resulted from different combinations of processing parameters. Using experimental results and applying the Taguchi model, 99.38 J/mm(3) was determined as the optimal energy density needed to produce samples with almost no porosity. The following analysis of variance ANOVA confirmed the scanning speed as the most influential factor in reducing the porosity percentage, which had a 74.9% contribution, followed by the position along the building direction with 22.8%, and finally, the laser energy with 2.3%. The influence on corrosion resistance was obtained by performing cyclic potentiodynamic polarization tests (CPP) in a 3.5 wt % NaCl solution at room temperature for different energy densities and positions (Z axis). The corrosion properties of the AM samples were studied and compared to those obtained from the traditionally manufactured samples. The corrosion resistance of the samples worsened with the increase in the percentage of porosity. The process parameters have consequently been optimized and the database has been extended to improve the quality of the AM-produced parts in which microstructural heterogeneities were observed along the building direction. MDPI 2022-02-21 /pmc/articles/PMC8877025/ /pubmed/35208144 http://dx.doi.org/10.3390/ma15041605 Text en © 2022 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Maicas-Esteve, Héctor
Taji, Iman
Wilms, Marc
Gonzalez-Garcia, Yaiza
Johnsen, Roy
Corrosion and Microstructural Investigation on Additively Manufactured 316L Stainless Steel: Experimental and Statistical Approach
title Corrosion and Microstructural Investigation on Additively Manufactured 316L Stainless Steel: Experimental and Statistical Approach
title_full Corrosion and Microstructural Investigation on Additively Manufactured 316L Stainless Steel: Experimental and Statistical Approach
title_fullStr Corrosion and Microstructural Investigation on Additively Manufactured 316L Stainless Steel: Experimental and Statistical Approach
title_full_unstemmed Corrosion and Microstructural Investigation on Additively Manufactured 316L Stainless Steel: Experimental and Statistical Approach
title_short Corrosion and Microstructural Investigation on Additively Manufactured 316L Stainless Steel: Experimental and Statistical Approach
title_sort corrosion and microstructural investigation on additively manufactured 316l stainless steel: experimental and statistical approach
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8877025/
https://www.ncbi.nlm.nih.gov/pubmed/35208144
http://dx.doi.org/10.3390/ma15041605
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