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Beamline commissioning for microscopic measurements with ultraviolet and soft X-ray beam at the upgraded beamline BL-13B of the Photon Factory

Beamline 13 of the Photon Factory has been in operation since 2010 as a vacuum ultraviolet and soft X-ray undulator beamline for X-ray photoelectron spectroscopy (XPS), X-ray absorption spectroscopy (XAS), and angle-resolved photoelectron spectroscopy (ARPES) experiments. The beamline and the end-st...

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Autores principales: Ozawa, Kenichi, Aiura, Yoshihiro, Wakabayashi, Daisuke, Tanaka, Hirokazu, Kikuchi, Takashi, Toyoshima, Akio, Mase, Kazuhiko
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8900837/
https://www.ncbi.nlm.nih.gov/pubmed/35254303
http://dx.doi.org/10.1107/S160057752200090X
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author Ozawa, Kenichi
Aiura, Yoshihiro
Wakabayashi, Daisuke
Tanaka, Hirokazu
Kikuchi, Takashi
Toyoshima, Akio
Mase, Kazuhiko
author_facet Ozawa, Kenichi
Aiura, Yoshihiro
Wakabayashi, Daisuke
Tanaka, Hirokazu
Kikuchi, Takashi
Toyoshima, Akio
Mase, Kazuhiko
author_sort Ozawa, Kenichi
collection PubMed
description Beamline 13 of the Photon Factory has been in operation since 2010 as a vacuum ultraviolet and soft X-ray undulator beamline for X-ray photoelectron spectroscopy (XPS), X-ray absorption spectroscopy (XAS), and angle-resolved photoelectron spectroscopy (ARPES) experiments. The beamline and the end-station at branch B have been recently upgraded, enabling microscopic XPS, XAS, and ARPES measurements to be performed. In 2015, a planar undulator insertion device was replaced with an APPLE-II (advanced planar polarized light emitter II) undulator. This replacement allows use of linear, circular, and elliptical polarized light between 48 and 2000 eV with photon intensities of 10(9)–10(13) photons s(−1). For microscopic measurements, a toroidal post-mirror was renewed to have more focused beam with profile sizes of 78 µm (horizontal) × 15 µm (vertical) and 84 µm × 11 µm at photon energies of 100 and 400 eV, respectively. A high-precision sample manipulator composed of an XYZ translator, a rotary feedthrough, and a newly developed goniometer, which is essential for microscopic measurements, has been used to control a sample specimen in six degrees of freedom, i.e. translation in the X, Y, and Z directions and rotation in the polar, azimuthal, and tilt directions. To demonstrate the performance of the focused beams, one- and two-dimensional XPS and XAS scan measurements of a copper grid have been performed. It was indicated from analysis of XPS and XAS intensity maps that the actual spatial resolution can be determined by the beam size.
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spelling pubmed-89008372022-03-29 Beamline commissioning for microscopic measurements with ultraviolet and soft X-ray beam at the upgraded beamline BL-13B of the Photon Factory Ozawa, Kenichi Aiura, Yoshihiro Wakabayashi, Daisuke Tanaka, Hirokazu Kikuchi, Takashi Toyoshima, Akio Mase, Kazuhiko J Synchrotron Radiat Research Papers Beamline 13 of the Photon Factory has been in operation since 2010 as a vacuum ultraviolet and soft X-ray undulator beamline for X-ray photoelectron spectroscopy (XPS), X-ray absorption spectroscopy (XAS), and angle-resolved photoelectron spectroscopy (ARPES) experiments. The beamline and the end-station at branch B have been recently upgraded, enabling microscopic XPS, XAS, and ARPES measurements to be performed. In 2015, a planar undulator insertion device was replaced with an APPLE-II (advanced planar polarized light emitter II) undulator. This replacement allows use of linear, circular, and elliptical polarized light between 48 and 2000 eV with photon intensities of 10(9)–10(13) photons s(−1). For microscopic measurements, a toroidal post-mirror was renewed to have more focused beam with profile sizes of 78 µm (horizontal) × 15 µm (vertical) and 84 µm × 11 µm at photon energies of 100 and 400 eV, respectively. A high-precision sample manipulator composed of an XYZ translator, a rotary feedthrough, and a newly developed goniometer, which is essential for microscopic measurements, has been used to control a sample specimen in six degrees of freedom, i.e. translation in the X, Y, and Z directions and rotation in the polar, azimuthal, and tilt directions. To demonstrate the performance of the focused beams, one- and two-dimensional XPS and XAS scan measurements of a copper grid have been performed. It was indicated from analysis of XPS and XAS intensity maps that the actual spatial resolution can be determined by the beam size. International Union of Crystallography 2022-02-16 /pmc/articles/PMC8900837/ /pubmed/35254303 http://dx.doi.org/10.1107/S160057752200090X Text en © Kenichi Ozawa et al. 2022 https://creativecommons.org/licenses/by/4.0/This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Research Papers
Ozawa, Kenichi
Aiura, Yoshihiro
Wakabayashi, Daisuke
Tanaka, Hirokazu
Kikuchi, Takashi
Toyoshima, Akio
Mase, Kazuhiko
Beamline commissioning for microscopic measurements with ultraviolet and soft X-ray beam at the upgraded beamline BL-13B of the Photon Factory
title Beamline commissioning for microscopic measurements with ultraviolet and soft X-ray beam at the upgraded beamline BL-13B of the Photon Factory
title_full Beamline commissioning for microscopic measurements with ultraviolet and soft X-ray beam at the upgraded beamline BL-13B of the Photon Factory
title_fullStr Beamline commissioning for microscopic measurements with ultraviolet and soft X-ray beam at the upgraded beamline BL-13B of the Photon Factory
title_full_unstemmed Beamline commissioning for microscopic measurements with ultraviolet and soft X-ray beam at the upgraded beamline BL-13B of the Photon Factory
title_short Beamline commissioning for microscopic measurements with ultraviolet and soft X-ray beam at the upgraded beamline BL-13B of the Photon Factory
title_sort beamline commissioning for microscopic measurements with ultraviolet and soft x-ray beam at the upgraded beamline bl-13b of the photon factory
topic Research Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8900837/
https://www.ncbi.nlm.nih.gov/pubmed/35254303
http://dx.doi.org/10.1107/S160057752200090X
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