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Fast automated energy changes at synchrotron radiation beamlines equipped with transfocator or focusing mirrors

Algorithms and procedures to fully automate retuning of synchrotron radiation beamlines over wide energy ranges are discussed. The discussion is based on the implementation at the National Institute of General Medical Sciences and the National Cancer Institute Structural Biology Facility at the Adva...

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Autores principales: Stepanov, Sergey, Kissick, David, Makarov, Oleg, Hilgart, Mark, Becker, Michael, Venugopalan, Nagarajan, Xu, Shenglan, Smith, Janet L., Fischetti, Robert F.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8900858/
https://www.ncbi.nlm.nih.gov/pubmed/35254302
http://dx.doi.org/10.1107/S1600577522001084
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author Stepanov, Sergey
Kissick, David
Makarov, Oleg
Hilgart, Mark
Becker, Michael
Venugopalan, Nagarajan
Xu, Shenglan
Smith, Janet L.
Fischetti, Robert F.
author_facet Stepanov, Sergey
Kissick, David
Makarov, Oleg
Hilgart, Mark
Becker, Michael
Venugopalan, Nagarajan
Xu, Shenglan
Smith, Janet L.
Fischetti, Robert F.
author_sort Stepanov, Sergey
collection PubMed
description Algorithms and procedures to fully automate retuning of synchrotron radiation beamlines over wide energy ranges are discussed. The discussion is based on the implementation at the National Institute of General Medical Sciences and the National Cancer Institute Structural Biology Facility at the Advanced Photon Source. When a user selects a new beamline energy, software synchronously controls the beamline monochromator and undulator to maintain the X-ray beam flux after the monochromator, preserves beam attenuation by determining a new set of attenuator foils, changes, as needed, mirror reflecting stripes and the undulator harmonic, preserves beam focal distance of compound refractive lens focusing by changing the In/Out combination of lenses in the transfocator, and, finally, restores beam position at the sample by on-the-fly scanning of either the Kirkpatrick–Baez mirror angles or the transfocator up/down and inboard/outboard positions. The sample is protected from radiation damage by automatically moving it out of the beam during the energy change and optimization.
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spelling pubmed-89008582022-03-29 Fast automated energy changes at synchrotron radiation beamlines equipped with transfocator or focusing mirrors Stepanov, Sergey Kissick, David Makarov, Oleg Hilgart, Mark Becker, Michael Venugopalan, Nagarajan Xu, Shenglan Smith, Janet L. Fischetti, Robert F. J Synchrotron Radiat Research Papers Algorithms and procedures to fully automate retuning of synchrotron radiation beamlines over wide energy ranges are discussed. The discussion is based on the implementation at the National Institute of General Medical Sciences and the National Cancer Institute Structural Biology Facility at the Advanced Photon Source. When a user selects a new beamline energy, software synchronously controls the beamline monochromator and undulator to maintain the X-ray beam flux after the monochromator, preserves beam attenuation by determining a new set of attenuator foils, changes, as needed, mirror reflecting stripes and the undulator harmonic, preserves beam focal distance of compound refractive lens focusing by changing the In/Out combination of lenses in the transfocator, and, finally, restores beam position at the sample by on-the-fly scanning of either the Kirkpatrick–Baez mirror angles or the transfocator up/down and inboard/outboard positions. The sample is protected from radiation damage by automatically moving it out of the beam during the energy change and optimization. International Union of Crystallography 2022-02-15 /pmc/articles/PMC8900858/ /pubmed/35254302 http://dx.doi.org/10.1107/S1600577522001084 Text en © Sergey Stepanov et al. 2022 https://creativecommons.org/licenses/by/4.0/This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Research Papers
Stepanov, Sergey
Kissick, David
Makarov, Oleg
Hilgart, Mark
Becker, Michael
Venugopalan, Nagarajan
Xu, Shenglan
Smith, Janet L.
Fischetti, Robert F.
Fast automated energy changes at synchrotron radiation beamlines equipped with transfocator or focusing mirrors
title Fast automated energy changes at synchrotron radiation beamlines equipped with transfocator or focusing mirrors
title_full Fast automated energy changes at synchrotron radiation beamlines equipped with transfocator or focusing mirrors
title_fullStr Fast automated energy changes at synchrotron radiation beamlines equipped with transfocator or focusing mirrors
title_full_unstemmed Fast automated energy changes at synchrotron radiation beamlines equipped with transfocator or focusing mirrors
title_short Fast automated energy changes at synchrotron radiation beamlines equipped with transfocator or focusing mirrors
title_sort fast automated energy changes at synchrotron radiation beamlines equipped with transfocator or focusing mirrors
topic Research Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8900858/
https://www.ncbi.nlm.nih.gov/pubmed/35254302
http://dx.doi.org/10.1107/S1600577522001084
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