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High-speed free-run ptychography at the Australian Synchrotron

Over the last decade ptychography has progressed rapidly from a specialist ultramicroscopy technique into a mature method accessible to non-expert users. However, to improve scientific value ptychography data must reconstruct reliably, with high image quality and at no cost to other correlative meth...

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Autores principales: Jones, Michael W. M., van Riessen, Grant A., Phillips, Nicholas W., Schrank, Christoph E., Hinsley, Gerard N., Afshar, Nader, Reinhardt, Juliane, de Jonge, Martin D., Kewish, Cameron M.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8900864/
https://www.ncbi.nlm.nih.gov/pubmed/35254312
http://dx.doi.org/10.1107/S1600577521012856
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author Jones, Michael W. M.
van Riessen, Grant A.
Phillips, Nicholas W.
Schrank, Christoph E.
Hinsley, Gerard N.
Afshar, Nader
Reinhardt, Juliane
de Jonge, Martin D.
Kewish, Cameron M.
author_facet Jones, Michael W. M.
van Riessen, Grant A.
Phillips, Nicholas W.
Schrank, Christoph E.
Hinsley, Gerard N.
Afshar, Nader
Reinhardt, Juliane
de Jonge, Martin D.
Kewish, Cameron M.
author_sort Jones, Michael W. M.
collection PubMed
description Over the last decade ptychography has progressed rapidly from a specialist ultramicroscopy technique into a mature method accessible to non-expert users. However, to improve scientific value ptychography data must reconstruct reliably, with high image quality and at no cost to other correlative methods. Presented here is the implementation of high-speed ptychography used at the Australian Synchrotron on the XFM beamline, which includes a free-run data collection mode where dead time is eliminated and the scan time is optimized. It is shown that free-run data collection is viable for fast and high-quality ptychography by demonstrating extremely high data rate acquisition covering areas up to 352 000 µm(2) at up to 140 µm(2) s(−1), with 13× spatial resolution enhancement compared with the beam size. With these improvements, ptychography at velocities up to 250 µm s(−1) is approaching speeds compatible with fast-scanning X-ray fluorescence microscopy. The combination of these methods provides morphological context for elemental and chemical information, enabling unique scientific outcomes.
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spelling pubmed-89008642022-03-29 High-speed free-run ptychography at the Australian Synchrotron Jones, Michael W. M. van Riessen, Grant A. Phillips, Nicholas W. Schrank, Christoph E. Hinsley, Gerard N. Afshar, Nader Reinhardt, Juliane de Jonge, Martin D. Kewish, Cameron M. J Synchrotron Radiat Research Papers Over the last decade ptychography has progressed rapidly from a specialist ultramicroscopy technique into a mature method accessible to non-expert users. However, to improve scientific value ptychography data must reconstruct reliably, with high image quality and at no cost to other correlative methods. Presented here is the implementation of high-speed ptychography used at the Australian Synchrotron on the XFM beamline, which includes a free-run data collection mode where dead time is eliminated and the scan time is optimized. It is shown that free-run data collection is viable for fast and high-quality ptychography by demonstrating extremely high data rate acquisition covering areas up to 352 000 µm(2) at up to 140 µm(2) s(−1), with 13× spatial resolution enhancement compared with the beam size. With these improvements, ptychography at velocities up to 250 µm s(−1) is approaching speeds compatible with fast-scanning X-ray fluorescence microscopy. The combination of these methods provides morphological context for elemental and chemical information, enabling unique scientific outcomes. International Union of Crystallography 2022-01-17 /pmc/articles/PMC8900864/ /pubmed/35254312 http://dx.doi.org/10.1107/S1600577521012856 Text en © Michael W. M. Jones et al. 2022 https://creativecommons.org/licenses/by/4.0/This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Research Papers
Jones, Michael W. M.
van Riessen, Grant A.
Phillips, Nicholas W.
Schrank, Christoph E.
Hinsley, Gerard N.
Afshar, Nader
Reinhardt, Juliane
de Jonge, Martin D.
Kewish, Cameron M.
High-speed free-run ptychography at the Australian Synchrotron
title High-speed free-run ptychography at the Australian Synchrotron
title_full High-speed free-run ptychography at the Australian Synchrotron
title_fullStr High-speed free-run ptychography at the Australian Synchrotron
title_full_unstemmed High-speed free-run ptychography at the Australian Synchrotron
title_short High-speed free-run ptychography at the Australian Synchrotron
title_sort high-speed free-run ptychography at the australian synchrotron
topic Research Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8900864/
https://www.ncbi.nlm.nih.gov/pubmed/35254312
http://dx.doi.org/10.1107/S1600577521012856
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