Cargando…

Alumina Manufactured by Fused Filament Fabrication: A Comprehensive Study of Mechanical Properties and Porosity

This article deals with a comprehensive study of the processing and mechanical properties of the ceramic material Al [Formula: see text] O [Formula: see text] on Fused Filament Fabrication technology (FFF). It describes the basic input analyses of the material, such as TGA, FTIR, and MVR. These anal...

Descripción completa

Detalles Bibliográficos
Autores principales: Truxová, Veronika, Šafka, Jiří, Sobotka, Jiří, Macháček, Jakub, Ackermann, Michal
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8912858/
https://www.ncbi.nlm.nih.gov/pubmed/35267814
http://dx.doi.org/10.3390/polym14050991
_version_ 1784667266833448960
author Truxová, Veronika
Šafka, Jiří
Sobotka, Jiří
Macháček, Jakub
Ackermann, Michal
author_facet Truxová, Veronika
Šafka, Jiří
Sobotka, Jiří
Macháček, Jakub
Ackermann, Michal
author_sort Truxová, Veronika
collection PubMed
description This article deals with a comprehensive study of the processing and mechanical properties of the ceramic material Al [Formula: see text] O [Formula: see text] on Fused Filament Fabrication technology (FFF). It describes the basic input analyses of the material, such as TGA, FTIR, and MVR. These analyses enabled the design and testing of process parameters for the 3D printing of parts. The article also presents the post-processes, including the technological parameters required to finalize parts made from this material, i.e., chemical debinding in acetone at elevated temperatures + thermal debinding and sintering. The microhardness was measured on the processed samples, depending on the density of the inner filling. The resulting hardness had an almost linear relationship between the percentage of filler (20–40–60–80–100%) and the resulting microhardness (1382–2428 HV10). Flexural strength was also measured on the test specimens with different degrees of internal filling (80–90–100%). However, inner filling do not affect the flexural strength (316.12–327.84–331.61 MPa). The relative density of the final parts was measured on a ZEISS METROTOM 1500 CT machine and reached 99.54%.
format Online
Article
Text
id pubmed-8912858
institution National Center for Biotechnology Information
language English
publishDate 2022
publisher MDPI
record_format MEDLINE/PubMed
spelling pubmed-89128582022-03-11 Alumina Manufactured by Fused Filament Fabrication: A Comprehensive Study of Mechanical Properties and Porosity Truxová, Veronika Šafka, Jiří Sobotka, Jiří Macháček, Jakub Ackermann, Michal Polymers (Basel) Article This article deals with a comprehensive study of the processing and mechanical properties of the ceramic material Al [Formula: see text] O [Formula: see text] on Fused Filament Fabrication technology (FFF). It describes the basic input analyses of the material, such as TGA, FTIR, and MVR. These analyses enabled the design and testing of process parameters for the 3D printing of parts. The article also presents the post-processes, including the technological parameters required to finalize parts made from this material, i.e., chemical debinding in acetone at elevated temperatures + thermal debinding and sintering. The microhardness was measured on the processed samples, depending on the density of the inner filling. The resulting hardness had an almost linear relationship between the percentage of filler (20–40–60–80–100%) and the resulting microhardness (1382–2428 HV10). Flexural strength was also measured on the test specimens with different degrees of internal filling (80–90–100%). However, inner filling do not affect the flexural strength (316.12–327.84–331.61 MPa). The relative density of the final parts was measured on a ZEISS METROTOM 1500 CT machine and reached 99.54%. MDPI 2022-02-28 /pmc/articles/PMC8912858/ /pubmed/35267814 http://dx.doi.org/10.3390/polym14050991 Text en © 2022 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Truxová, Veronika
Šafka, Jiří
Sobotka, Jiří
Macháček, Jakub
Ackermann, Michal
Alumina Manufactured by Fused Filament Fabrication: A Comprehensive Study of Mechanical Properties and Porosity
title Alumina Manufactured by Fused Filament Fabrication: A Comprehensive Study of Mechanical Properties and Porosity
title_full Alumina Manufactured by Fused Filament Fabrication: A Comprehensive Study of Mechanical Properties and Porosity
title_fullStr Alumina Manufactured by Fused Filament Fabrication: A Comprehensive Study of Mechanical Properties and Porosity
title_full_unstemmed Alumina Manufactured by Fused Filament Fabrication: A Comprehensive Study of Mechanical Properties and Porosity
title_short Alumina Manufactured by Fused Filament Fabrication: A Comprehensive Study of Mechanical Properties and Porosity
title_sort alumina manufactured by fused filament fabrication: a comprehensive study of mechanical properties and porosity
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8912858/
https://www.ncbi.nlm.nih.gov/pubmed/35267814
http://dx.doi.org/10.3390/polym14050991
work_keys_str_mv AT truxovaveronika aluminamanufacturedbyfusedfilamentfabricationacomprehensivestudyofmechanicalpropertiesandporosity
AT safkajiri aluminamanufacturedbyfusedfilamentfabricationacomprehensivestudyofmechanicalpropertiesandporosity
AT sobotkajiri aluminamanufacturedbyfusedfilamentfabricationacomprehensivestudyofmechanicalpropertiesandporosity
AT machacekjakub aluminamanufacturedbyfusedfilamentfabricationacomprehensivestudyofmechanicalpropertiesandporosity
AT ackermannmichal aluminamanufacturedbyfusedfilamentfabricationacomprehensivestudyofmechanicalpropertiesandporosity