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Growth of crystalline WO(3)-ZnSe nanocomposites: an approach to optical, electrochemical, and catalytic properties

In this study, novel growth of WO(3)-ZnSe nanocomposites was carried out by a simple, low-cost hydrothermal process under subcritical conditions and is reported for the first time in just 5 h. The products were characterized in detail by multiform techniques: X-ray diffraction, scanning electron mic...

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Autores principales: Assadullah, Insaaf, Malik, Javied Hamid, Shafi, Adil, Tomar, Radha
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Nature Publishing Group UK 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8913615/
https://www.ncbi.nlm.nih.gov/pubmed/35273263
http://dx.doi.org/10.1038/s41598-022-07951-5
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author Assadullah, Insaaf
Malik, Javied Hamid
Shafi, Adil
Tomar, Radha
author_facet Assadullah, Insaaf
Malik, Javied Hamid
Shafi, Adil
Tomar, Radha
author_sort Assadullah, Insaaf
collection PubMed
description In this study, novel growth of WO(3)-ZnSe nanocomposites was carried out by a simple, low-cost hydrothermal process under subcritical conditions and is reported for the first time in just 5 h. The products were characterized in detail by multiform techniques: X-ray diffraction, scanning electron microscopy (SEM), optical studies, and Fourier transform analysis. The influence of ZnSe on the structural, morphological, compositional, optical, and catalytic properties of WO(3) is demonstrated. The WO(3) metal oxide material is grown in a hexagonal crystal structure with wide-band-gap and has been modified by ZnSe to form a composite nanostructures in the nanoscale range. The electrochemical properties of the prepared materials were studied by cyclic voltammetry, which revealed that the synthesized material exhibited remarkable electrochemical supercapacitive activity. Moreover, the composite nanostructures showed excellent photocatalytic activity for degradation of phenol and almost 93% of phenol was degraded with good recyclability and stability. According to The International Commission on Illumination (CIE), the synthesized nanomaterial shows blue emission and is suitable for blue LEDs.
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spelling pubmed-89136152022-03-11 Growth of crystalline WO(3)-ZnSe nanocomposites: an approach to optical, electrochemical, and catalytic properties Assadullah, Insaaf Malik, Javied Hamid Shafi, Adil Tomar, Radha Sci Rep Article In this study, novel growth of WO(3)-ZnSe nanocomposites was carried out by a simple, low-cost hydrothermal process under subcritical conditions and is reported for the first time in just 5 h. The products were characterized in detail by multiform techniques: X-ray diffraction, scanning electron microscopy (SEM), optical studies, and Fourier transform analysis. The influence of ZnSe on the structural, morphological, compositional, optical, and catalytic properties of WO(3) is demonstrated. The WO(3) metal oxide material is grown in a hexagonal crystal structure with wide-band-gap and has been modified by ZnSe to form a composite nanostructures in the nanoscale range. The electrochemical properties of the prepared materials were studied by cyclic voltammetry, which revealed that the synthesized material exhibited remarkable electrochemical supercapacitive activity. Moreover, the composite nanostructures showed excellent photocatalytic activity for degradation of phenol and almost 93% of phenol was degraded with good recyclability and stability. According to The International Commission on Illumination (CIE), the synthesized nanomaterial shows blue emission and is suitable for blue LEDs. Nature Publishing Group UK 2022-03-10 /pmc/articles/PMC8913615/ /pubmed/35273263 http://dx.doi.org/10.1038/s41598-022-07951-5 Text en © The Author(s) 2022 https://creativecommons.org/licenses/by/4.0/Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons licence, and indicate if changes were made. The images or other third party material in this article are included in the article's Creative Commons licence, unless indicated otherwise in a credit line to the material. If material is not included in the article's Creative Commons licence and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this licence, visit http://creativecommons.org/licenses/by/4.0/ (https://creativecommons.org/licenses/by/4.0/) .
spellingShingle Article
Assadullah, Insaaf
Malik, Javied Hamid
Shafi, Adil
Tomar, Radha
Growth of crystalline WO(3)-ZnSe nanocomposites: an approach to optical, electrochemical, and catalytic properties
title Growth of crystalline WO(3)-ZnSe nanocomposites: an approach to optical, electrochemical, and catalytic properties
title_full Growth of crystalline WO(3)-ZnSe nanocomposites: an approach to optical, electrochemical, and catalytic properties
title_fullStr Growth of crystalline WO(3)-ZnSe nanocomposites: an approach to optical, electrochemical, and catalytic properties
title_full_unstemmed Growth of crystalline WO(3)-ZnSe nanocomposites: an approach to optical, electrochemical, and catalytic properties
title_short Growth of crystalline WO(3)-ZnSe nanocomposites: an approach to optical, electrochemical, and catalytic properties
title_sort growth of crystalline wo(3)-znse nanocomposites: an approach to optical, electrochemical, and catalytic properties
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8913615/
https://www.ncbi.nlm.nih.gov/pubmed/35273263
http://dx.doi.org/10.1038/s41598-022-07951-5
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