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Nano-[Fe(3)O(4)@SiO(2)/N-propyl-1-(thiophen-2-yl)ethanimine][ZnCl(2)] as a nano magnetite Schiff base complex and heterogeneous catalyst for the synthesis of pyrimido[4,5-b]quinolones

Nano-[Fe(3)O(4)@SiO(2)/N-propyl-1-(thiophen-2-yl)ethanimine][ZnCl(2)] as a nano magnetite Schiff base complex was designed and fully characterized by various analyses such as Fourier transform infrared spectroscopy (FT-IR), energy-dispersive X-ray spectroscopy (EDX), X-ray diffraction (XRD), thermal...

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Autores principales: Esmaili, Soheila, Moosavi-Zare, Ahmad Reza, Khazaei, Ardeshir
Formato: Online Artículo Texto
Lenguaje:English
Publicado: The Royal Society of Chemistry 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8981359/
https://www.ncbi.nlm.nih.gov/pubmed/35425540
http://dx.doi.org/10.1039/d2ra00213b
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author Esmaili, Soheila
Moosavi-Zare, Ahmad Reza
Khazaei, Ardeshir
author_facet Esmaili, Soheila
Moosavi-Zare, Ahmad Reza
Khazaei, Ardeshir
author_sort Esmaili, Soheila
collection PubMed
description Nano-[Fe(3)O(4)@SiO(2)/N-propyl-1-(thiophen-2-yl)ethanimine][ZnCl(2)] as a nano magnetite Schiff base complex was designed and fully characterized by various analyses such as Fourier transform infrared spectroscopy (FT-IR), energy-dispersive X-ray spectroscopy (EDX), X-ray diffraction (XRD), thermal gravimetric analysis (TGA), differential thermal gravimetric analysis (DTA), vibrating sample magnetometry (VSM), scanning electron microscopy (SEM), and transmission electron micrographs (TEM). The presented nano magnetite Schiff base complex was used as a heterogeneous catalyst for the synthesis of pyrimido[4,5-b]quinolones by the reaction of aryl aldehyde, dimedone and 6-amino-1,3-dimethyluracil in EtOH : H(2)O (7 : 3) as a solvent at 60 °C.
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spelling pubmed-89813592022-04-13 Nano-[Fe(3)O(4)@SiO(2)/N-propyl-1-(thiophen-2-yl)ethanimine][ZnCl(2)] as a nano magnetite Schiff base complex and heterogeneous catalyst for the synthesis of pyrimido[4,5-b]quinolones Esmaili, Soheila Moosavi-Zare, Ahmad Reza Khazaei, Ardeshir RSC Adv Chemistry Nano-[Fe(3)O(4)@SiO(2)/N-propyl-1-(thiophen-2-yl)ethanimine][ZnCl(2)] as a nano magnetite Schiff base complex was designed and fully characterized by various analyses such as Fourier transform infrared spectroscopy (FT-IR), energy-dispersive X-ray spectroscopy (EDX), X-ray diffraction (XRD), thermal gravimetric analysis (TGA), differential thermal gravimetric analysis (DTA), vibrating sample magnetometry (VSM), scanning electron microscopy (SEM), and transmission electron micrographs (TEM). The presented nano magnetite Schiff base complex was used as a heterogeneous catalyst for the synthesis of pyrimido[4,5-b]quinolones by the reaction of aryl aldehyde, dimedone and 6-amino-1,3-dimethyluracil in EtOH : H(2)O (7 : 3) as a solvent at 60 °C. The Royal Society of Chemistry 2022-02-14 /pmc/articles/PMC8981359/ /pubmed/35425540 http://dx.doi.org/10.1039/d2ra00213b Text en This journal is © The Royal Society of Chemistry https://creativecommons.org/licenses/by-nc/3.0/
spellingShingle Chemistry
Esmaili, Soheila
Moosavi-Zare, Ahmad Reza
Khazaei, Ardeshir
Nano-[Fe(3)O(4)@SiO(2)/N-propyl-1-(thiophen-2-yl)ethanimine][ZnCl(2)] as a nano magnetite Schiff base complex and heterogeneous catalyst for the synthesis of pyrimido[4,5-b]quinolones
title Nano-[Fe(3)O(4)@SiO(2)/N-propyl-1-(thiophen-2-yl)ethanimine][ZnCl(2)] as a nano magnetite Schiff base complex and heterogeneous catalyst for the synthesis of pyrimido[4,5-b]quinolones
title_full Nano-[Fe(3)O(4)@SiO(2)/N-propyl-1-(thiophen-2-yl)ethanimine][ZnCl(2)] as a nano magnetite Schiff base complex and heterogeneous catalyst for the synthesis of pyrimido[4,5-b]quinolones
title_fullStr Nano-[Fe(3)O(4)@SiO(2)/N-propyl-1-(thiophen-2-yl)ethanimine][ZnCl(2)] as a nano magnetite Schiff base complex and heterogeneous catalyst for the synthesis of pyrimido[4,5-b]quinolones
title_full_unstemmed Nano-[Fe(3)O(4)@SiO(2)/N-propyl-1-(thiophen-2-yl)ethanimine][ZnCl(2)] as a nano magnetite Schiff base complex and heterogeneous catalyst for the synthesis of pyrimido[4,5-b]quinolones
title_short Nano-[Fe(3)O(4)@SiO(2)/N-propyl-1-(thiophen-2-yl)ethanimine][ZnCl(2)] as a nano magnetite Schiff base complex and heterogeneous catalyst for the synthesis of pyrimido[4,5-b]quinolones
title_sort nano-[fe(3)o(4)@sio(2)/n-propyl-1-(thiophen-2-yl)ethanimine][zncl(2)] as a nano magnetite schiff base complex and heterogeneous catalyst for the synthesis of pyrimido[4,5-b]quinolones
topic Chemistry
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8981359/
https://www.ncbi.nlm.nih.gov/pubmed/35425540
http://dx.doi.org/10.1039/d2ra00213b
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