Application of novel metal–organic framework [Zr-UiO-66-PDC-SO(3)H]FeCl(4) in the synthesis of dihydrobenzo[g]pyrimido[4,5-b]quinoline derivatives

In the current paper, we produce a new metal–organic framework (MOF) based on Zr metal, [Zr-UiO-66-PDC-SO(3)H]FeCl(4), via an anion exchange method, which is fully characterized by FT-IR, SEM with elemental mapping and EDX, FE-SEM and TEM. Furthermore, the use of [Zr-UiO-66-PDC-SO(3)H]FeCl(4) as a p...

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Detalles Bibliográficos
Autores principales: Jalili, Fatemeh, Zarei, Mahmoud, Zolfigol, Mohammad Ali, Khazaei, Ardeshir
Formato: Online Artículo Texto
Lenguaje:English
Publicado: The Royal Society of Chemistry 2022
Materias:
Chemistry
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8985156/
https://www.ncbi.nlm.nih.gov/pubmed/35424891
http://dx.doi.org/10.1039/d1ra08710j
Descripción
Sumario:In the current paper, we produce a new metal–organic framework (MOF) based on Zr metal, [Zr-UiO-66-PDC-SO(3)H]FeCl(4), via an anion exchange method, which is fully characterized by FT-IR, SEM with elemental mapping and EDX, FE-SEM and TEM. Furthermore, the use of [Zr-UiO-66-PDC-SO(3)H]FeCl(4) as a porous catalyst was examined for the one-pot synthesis of novel dihydrobenzo[g]pyrimido[4,5-b]quinoline derivatives by reaction of 6-amino-1,3-dimethylpyrimidine-2,4(1H,3H)-dione, 2-hydroxynaphthalene-1,4-dione and various aldehydes at 100 °C with good to excellent yields.

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