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Fabrication and Characterization of Highly Efficient As-Synthesized WO(3)/Graphitic-C(3)N(4) Nanocomposite for Photocatalytic Degradation of Organic Compounds
The incorporation of tungsten trioxide (WO(3)) by various concentrations of graphitic carbon nitride (g-C(3)N(4)) was successfully studied. X-ray diffraction (XRD), Scanning Electron Microscope (SEM), and Diffused Reflectance UV-Vis techniques were applied to investigate morphological and microstruc...
Autores principales: | , , , , , , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
MDPI
2022
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8999551/ https://www.ncbi.nlm.nih.gov/pubmed/35407814 http://dx.doi.org/10.3390/ma15072482 |
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author | Hussien, Mai S. A. Bouzidi, Abdelfatteh Abd-Rabboh, Hisham S. M. Yahia, Ibrahim S. Zahran, Heba Y. Abdel-wahab, Mohamed Sh. Alharbi, Walaa Awwad, Nasser S. Ibrahim, Medhat A. |
author_facet | Hussien, Mai S. A. Bouzidi, Abdelfatteh Abd-Rabboh, Hisham S. M. Yahia, Ibrahim S. Zahran, Heba Y. Abdel-wahab, Mohamed Sh. Alharbi, Walaa Awwad, Nasser S. Ibrahim, Medhat A. |
author_sort | Hussien, Mai S. A. |
collection | PubMed |
description | The incorporation of tungsten trioxide (WO(3)) by various concentrations of graphitic carbon nitride (g-C(3)N(4)) was successfully studied. X-ray diffraction (XRD), Scanning Electron Microscope (SEM), and Diffused Reflectance UV-Vis techniques were applied to investigate morphological and microstructure analysis, diffused reflectance optical properties, and photocatalysis measurements of WO(3)/g-C(3)N(4) photocatalyst composite organic compounds. The photocatalytic activity of incorporating WO3 into g-C(3)N(4) composite organic compounds was evaluated by the photodegradation of both Methylene Blue (MB) dye and phenol under visible-light irradiation. Due to the high purity of the studied heterojunction composite series, no observed diffraction peaks appeared when incorporating WO(3) into g-C(3)N(4) composite organic compounds. The particle size of the prepared composite organic compound photocatalysts revealed no evident influence through the increase in WO(3) atoms from the SEM characteristic. The direct and indirect bandgap were recorded for different mole ratios of WO(3)/g-C(3)N(4,) and indicated no apparent impact on bandgap energy with increasing WO(3) content in the composite photocatalyst. The composite photocatalysts’ properties better understand their photocatalytic activity degradations. The pseudo-first-order reaction constants (K) can be calculated by examining the kinetic photocatalytic activity. |
format | Online Article Text |
id | pubmed-8999551 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2022 |
publisher | MDPI |
record_format | MEDLINE/PubMed |
spelling | pubmed-89995512022-04-12 Fabrication and Characterization of Highly Efficient As-Synthesized WO(3)/Graphitic-C(3)N(4) Nanocomposite for Photocatalytic Degradation of Organic Compounds Hussien, Mai S. A. Bouzidi, Abdelfatteh Abd-Rabboh, Hisham S. M. Yahia, Ibrahim S. Zahran, Heba Y. Abdel-wahab, Mohamed Sh. Alharbi, Walaa Awwad, Nasser S. Ibrahim, Medhat A. Materials (Basel) Article The incorporation of tungsten trioxide (WO(3)) by various concentrations of graphitic carbon nitride (g-C(3)N(4)) was successfully studied. X-ray diffraction (XRD), Scanning Electron Microscope (SEM), and Diffused Reflectance UV-Vis techniques were applied to investigate morphological and microstructure analysis, diffused reflectance optical properties, and photocatalysis measurements of WO(3)/g-C(3)N(4) photocatalyst composite organic compounds. The photocatalytic activity of incorporating WO3 into g-C(3)N(4) composite organic compounds was evaluated by the photodegradation of both Methylene Blue (MB) dye and phenol under visible-light irradiation. Due to the high purity of the studied heterojunction composite series, no observed diffraction peaks appeared when incorporating WO(3) into g-C(3)N(4) composite organic compounds. The particle size of the prepared composite organic compound photocatalysts revealed no evident influence through the increase in WO(3) atoms from the SEM characteristic. The direct and indirect bandgap were recorded for different mole ratios of WO(3)/g-C(3)N(4,) and indicated no apparent impact on bandgap energy with increasing WO(3) content in the composite photocatalyst. The composite photocatalysts’ properties better understand their photocatalytic activity degradations. The pseudo-first-order reaction constants (K) can be calculated by examining the kinetic photocatalytic activity. MDPI 2022-03-28 /pmc/articles/PMC8999551/ /pubmed/35407814 http://dx.doi.org/10.3390/ma15072482 Text en © 2022 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/). |
spellingShingle | Article Hussien, Mai S. A. Bouzidi, Abdelfatteh Abd-Rabboh, Hisham S. M. Yahia, Ibrahim S. Zahran, Heba Y. Abdel-wahab, Mohamed Sh. Alharbi, Walaa Awwad, Nasser S. Ibrahim, Medhat A. Fabrication and Characterization of Highly Efficient As-Synthesized WO(3)/Graphitic-C(3)N(4) Nanocomposite for Photocatalytic Degradation of Organic Compounds |
title | Fabrication and Characterization of Highly Efficient As-Synthesized WO(3)/Graphitic-C(3)N(4) Nanocomposite for Photocatalytic Degradation of Organic Compounds |
title_full | Fabrication and Characterization of Highly Efficient As-Synthesized WO(3)/Graphitic-C(3)N(4) Nanocomposite for Photocatalytic Degradation of Organic Compounds |
title_fullStr | Fabrication and Characterization of Highly Efficient As-Synthesized WO(3)/Graphitic-C(3)N(4) Nanocomposite for Photocatalytic Degradation of Organic Compounds |
title_full_unstemmed | Fabrication and Characterization of Highly Efficient As-Synthesized WO(3)/Graphitic-C(3)N(4) Nanocomposite for Photocatalytic Degradation of Organic Compounds |
title_short | Fabrication and Characterization of Highly Efficient As-Synthesized WO(3)/Graphitic-C(3)N(4) Nanocomposite for Photocatalytic Degradation of Organic Compounds |
title_sort | fabrication and characterization of highly efficient as-synthesized wo(3)/graphitic-c(3)n(4) nanocomposite for photocatalytic degradation of organic compounds |
topic | Article |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8999551/ https://www.ncbi.nlm.nih.gov/pubmed/35407814 http://dx.doi.org/10.3390/ma15072482 |
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