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Fabrication and Characterization of Highly Efficient As-Synthesized WO(3)/Graphitic-C(3)N(4) Nanocomposite for Photocatalytic Degradation of Organic Compounds

The incorporation of tungsten trioxide (WO(3)) by various concentrations of graphitic carbon nitride (g-C(3)N(4)) was successfully studied. X-ray diffraction (XRD), Scanning Electron Microscope (SEM), and Diffused Reflectance UV-Vis techniques were applied to investigate morphological and microstruc...

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Autores principales: Hussien, Mai S. A., Bouzidi, Abdelfatteh, Abd-Rabboh, Hisham S. M., Yahia, Ibrahim S., Zahran, Heba Y., Abdel-wahab, Mohamed Sh., Alharbi, Walaa, Awwad, Nasser S., Ibrahim, Medhat A.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8999551/
https://www.ncbi.nlm.nih.gov/pubmed/35407814
http://dx.doi.org/10.3390/ma15072482
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author Hussien, Mai S. A.
Bouzidi, Abdelfatteh
Abd-Rabboh, Hisham S. M.
Yahia, Ibrahim S.
Zahran, Heba Y.
Abdel-wahab, Mohamed Sh.
Alharbi, Walaa
Awwad, Nasser S.
Ibrahim, Medhat A.
author_facet Hussien, Mai S. A.
Bouzidi, Abdelfatteh
Abd-Rabboh, Hisham S. M.
Yahia, Ibrahim S.
Zahran, Heba Y.
Abdel-wahab, Mohamed Sh.
Alharbi, Walaa
Awwad, Nasser S.
Ibrahim, Medhat A.
author_sort Hussien, Mai S. A.
collection PubMed
description The incorporation of tungsten trioxide (WO(3)) by various concentrations of graphitic carbon nitride (g-C(3)N(4)) was successfully studied. X-ray diffraction (XRD), Scanning Electron Microscope (SEM), and Diffused Reflectance UV-Vis techniques were applied to investigate morphological and microstructure analysis, diffused reflectance optical properties, and photocatalysis measurements of WO(3)/g-C(3)N(4) photocatalyst composite organic compounds. The photocatalytic activity of incorporating WO3 into g-C(3)N(4) composite organic compounds was evaluated by the photodegradation of both Methylene Blue (MB) dye and phenol under visible-light irradiation. Due to the high purity of the studied heterojunction composite series, no observed diffraction peaks appeared when incorporating WO(3) into g-C(3)N(4) composite organic compounds. The particle size of the prepared composite organic compound photocatalysts revealed no evident influence through the increase in WO(3) atoms from the SEM characteristic. The direct and indirect bandgap were recorded for different mole ratios of WO(3)/g-C(3)N(4,) and indicated no apparent impact on bandgap energy with increasing WO(3) content in the composite photocatalyst. The composite photocatalysts’ properties better understand their photocatalytic activity degradations. The pseudo-first-order reaction constants (K) can be calculated by examining the kinetic photocatalytic activity.
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spelling pubmed-89995512022-04-12 Fabrication and Characterization of Highly Efficient As-Synthesized WO(3)/Graphitic-C(3)N(4) Nanocomposite for Photocatalytic Degradation of Organic Compounds Hussien, Mai S. A. Bouzidi, Abdelfatteh Abd-Rabboh, Hisham S. M. Yahia, Ibrahim S. Zahran, Heba Y. Abdel-wahab, Mohamed Sh. Alharbi, Walaa Awwad, Nasser S. Ibrahim, Medhat A. Materials (Basel) Article The incorporation of tungsten trioxide (WO(3)) by various concentrations of graphitic carbon nitride (g-C(3)N(4)) was successfully studied. X-ray diffraction (XRD), Scanning Electron Microscope (SEM), and Diffused Reflectance UV-Vis techniques were applied to investigate morphological and microstructure analysis, diffused reflectance optical properties, and photocatalysis measurements of WO(3)/g-C(3)N(4) photocatalyst composite organic compounds. The photocatalytic activity of incorporating WO3 into g-C(3)N(4) composite organic compounds was evaluated by the photodegradation of both Methylene Blue (MB) dye and phenol under visible-light irradiation. Due to the high purity of the studied heterojunction composite series, no observed diffraction peaks appeared when incorporating WO(3) into g-C(3)N(4) composite organic compounds. The particle size of the prepared composite organic compound photocatalysts revealed no evident influence through the increase in WO(3) atoms from the SEM characteristic. The direct and indirect bandgap were recorded for different mole ratios of WO(3)/g-C(3)N(4,) and indicated no apparent impact on bandgap energy with increasing WO(3) content in the composite photocatalyst. The composite photocatalysts’ properties better understand their photocatalytic activity degradations. The pseudo-first-order reaction constants (K) can be calculated by examining the kinetic photocatalytic activity. MDPI 2022-03-28 /pmc/articles/PMC8999551/ /pubmed/35407814 http://dx.doi.org/10.3390/ma15072482 Text en © 2022 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Hussien, Mai S. A.
Bouzidi, Abdelfatteh
Abd-Rabboh, Hisham S. M.
Yahia, Ibrahim S.
Zahran, Heba Y.
Abdel-wahab, Mohamed Sh.
Alharbi, Walaa
Awwad, Nasser S.
Ibrahim, Medhat A.
Fabrication and Characterization of Highly Efficient As-Synthesized WO(3)/Graphitic-C(3)N(4) Nanocomposite for Photocatalytic Degradation of Organic Compounds
title Fabrication and Characterization of Highly Efficient As-Synthesized WO(3)/Graphitic-C(3)N(4) Nanocomposite for Photocatalytic Degradation of Organic Compounds
title_full Fabrication and Characterization of Highly Efficient As-Synthesized WO(3)/Graphitic-C(3)N(4) Nanocomposite for Photocatalytic Degradation of Organic Compounds
title_fullStr Fabrication and Characterization of Highly Efficient As-Synthesized WO(3)/Graphitic-C(3)N(4) Nanocomposite for Photocatalytic Degradation of Organic Compounds
title_full_unstemmed Fabrication and Characterization of Highly Efficient As-Synthesized WO(3)/Graphitic-C(3)N(4) Nanocomposite for Photocatalytic Degradation of Organic Compounds
title_short Fabrication and Characterization of Highly Efficient As-Synthesized WO(3)/Graphitic-C(3)N(4) Nanocomposite for Photocatalytic Degradation of Organic Compounds
title_sort fabrication and characterization of highly efficient as-synthesized wo(3)/graphitic-c(3)n(4) nanocomposite for photocatalytic degradation of organic compounds
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8999551/
https://www.ncbi.nlm.nih.gov/pubmed/35407814
http://dx.doi.org/10.3390/ma15072482
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