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Effects of Ti Target Purity and Microstructure on Deposition Rate, Microstructure and Properties of Ti Films

Three titanium (Ti) targets with different purities were used to prepare Ti films on polyimide substrates by DC magnetron sputtering. The microstructures of Ti films were characterized by a metallographic microscope, X-ray diffractometer, field emission scanning electron microscope and three-dimensi...

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Detalles Bibliográficos
Autores principales: Liu, Liming, Li, Wuhui, Sun, Haoliang, Wang, Guangxin
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9000231/
https://www.ncbi.nlm.nih.gov/pubmed/35407993
http://dx.doi.org/10.3390/ma15072661
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author Liu, Liming
Li, Wuhui
Sun, Haoliang
Wang, Guangxin
author_facet Liu, Liming
Li, Wuhui
Sun, Haoliang
Wang, Guangxin
author_sort Liu, Liming
collection PubMed
description Three titanium (Ti) targets with different purities were used to prepare Ti films on polyimide substrates by DC magnetron sputtering. The microstructures of Ti films were characterized by a metallographic microscope, X-ray diffractometer, field emission scanning electron microscope and three-dimensional surface topography instrument. In this study, we investigated the effects of Ti target purity and microstructure on film deposition rate, surface roughness, microstructure and resistivity. The results show that the deposition rate increased with increasing Ti target purity. Ti film deposited by the high-purity (99.999%) Ti target has fewer surface particles with smaller size, lower surface roughness and lower resistivity when compared to that prepared by the Ti target of low purity (99.7%). The surface roughness of Ti film prepared by the high-purity Ti target was Sa = 121 nm, the deposition rate was 16.3 nm/min and the resistivity was 6.9 × 10(−6) Ω·m. For Ti targets of the same purity, the performance of Ti film prepared by a target with equiaxed α-phase grains is better than that of Ti film prepared by a target with twins and β-phase grains.
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spelling pubmed-90002312022-04-12 Effects of Ti Target Purity and Microstructure on Deposition Rate, Microstructure and Properties of Ti Films Liu, Liming Li, Wuhui Sun, Haoliang Wang, Guangxin Materials (Basel) Article Three titanium (Ti) targets with different purities were used to prepare Ti films on polyimide substrates by DC magnetron sputtering. The microstructures of Ti films were characterized by a metallographic microscope, X-ray diffractometer, field emission scanning electron microscope and three-dimensional surface topography instrument. In this study, we investigated the effects of Ti target purity and microstructure on film deposition rate, surface roughness, microstructure and resistivity. The results show that the deposition rate increased with increasing Ti target purity. Ti film deposited by the high-purity (99.999%) Ti target has fewer surface particles with smaller size, lower surface roughness and lower resistivity when compared to that prepared by the Ti target of low purity (99.7%). The surface roughness of Ti film prepared by the high-purity Ti target was Sa = 121 nm, the deposition rate was 16.3 nm/min and the resistivity was 6.9 × 10(−6) Ω·m. For Ti targets of the same purity, the performance of Ti film prepared by a target with equiaxed α-phase grains is better than that of Ti film prepared by a target with twins and β-phase grains. MDPI 2022-04-05 /pmc/articles/PMC9000231/ /pubmed/35407993 http://dx.doi.org/10.3390/ma15072661 Text en © 2022 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Liu, Liming
Li, Wuhui
Sun, Haoliang
Wang, Guangxin
Effects of Ti Target Purity and Microstructure on Deposition Rate, Microstructure and Properties of Ti Films
title Effects of Ti Target Purity and Microstructure on Deposition Rate, Microstructure and Properties of Ti Films
title_full Effects of Ti Target Purity and Microstructure on Deposition Rate, Microstructure and Properties of Ti Films
title_fullStr Effects of Ti Target Purity and Microstructure on Deposition Rate, Microstructure and Properties of Ti Films
title_full_unstemmed Effects of Ti Target Purity and Microstructure on Deposition Rate, Microstructure and Properties of Ti Films
title_short Effects of Ti Target Purity and Microstructure on Deposition Rate, Microstructure and Properties of Ti Films
title_sort effects of ti target purity and microstructure on deposition rate, microstructure and properties of ti films
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9000231/
https://www.ncbi.nlm.nih.gov/pubmed/35407993
http://dx.doi.org/10.3390/ma15072661
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