Efficient Synthesis of Various Substituted (Thio)Ureas, Semicarbazides, Thiosemicarbazides, Thiazolidones, and Oxadiazole Derived from [2.2]Paracyclophane

[Image: see text] The strategies of the syntheses of various (thio)ureas, semicarbazides, thiosemicarbazides, thiazolidones, and oxadiazole derived from the [2.2]paracyclophane molecule are achieved starting with 4-(2.2]paracyclophanyl)isocyanate. The structures of the obtained products were elucida...

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Autores principales: Alshammari, Mohammed B., Aly, Ashraf A., Bräse, Stefan, Nieger, Martin, Abd El-Haleem, Lamiaa E.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: American Chemical Society 2022
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9026011/
https://www.ncbi.nlm.nih.gov/pubmed/35474844
http://dx.doi.org/10.1021/acsomega.2c00141
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author Alshammari, Mohammed B.
Aly, Ashraf A.
Bräse, Stefan
Nieger, Martin
Abd El-Haleem, Lamiaa E.
author_facet Alshammari, Mohammed B.
Aly, Ashraf A.
Bräse, Stefan
Nieger, Martin
Abd El-Haleem, Lamiaa E.
author_sort Alshammari, Mohammed B.
collection PubMed
description [Image: see text] The strategies of the syntheses of various (thio)ureas, semicarbazides, thiosemicarbazides, thiazolidones, and oxadiazole derived from the [2.2]paracyclophane molecule are achieved starting with 4-(2.2]paracyclophanyl)isocyanate. The structures of the obtained products were elucidated by NMR, mass spectrometry, and infrared (IR) spectroscopy in addition to high-resolution mass spectrometry (HRMS). X-ray structure analysis was also used to prove the assigned structure.
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spelling pubmed-90260112022-04-25 Efficient Synthesis of Various Substituted (Thio)Ureas, Semicarbazides, Thiosemicarbazides, Thiazolidones, and Oxadiazole Derived from [2.2]Paracyclophane Alshammari, Mohammed B. Aly, Ashraf A. Bräse, Stefan Nieger, Martin Abd El-Haleem, Lamiaa E. ACS Omega [Image: see text] The strategies of the syntheses of various (thio)ureas, semicarbazides, thiosemicarbazides, thiazolidones, and oxadiazole derived from the [2.2]paracyclophane molecule are achieved starting with 4-(2.2]paracyclophanyl)isocyanate. The structures of the obtained products were elucidated by NMR, mass spectrometry, and infrared (IR) spectroscopy in addition to high-resolution mass spectrometry (HRMS). X-ray structure analysis was also used to prove the assigned structure. American Chemical Society 2022-04-06 /pmc/articles/PMC9026011/ /pubmed/35474844 http://dx.doi.org/10.1021/acsomega.2c00141 Text en © 2022 The Authors. Published by American Chemical Society https://creativecommons.org/licenses/by/4.0/Permits the broadest form of re-use including for commercial purposes, provided that author attribution and integrity are maintained (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Alshammari, Mohammed B.
Aly, Ashraf A.
Bräse, Stefan
Nieger, Martin
Abd El-Haleem, Lamiaa E.
Efficient Synthesis of Various Substituted (Thio)Ureas, Semicarbazides, Thiosemicarbazides, Thiazolidones, and Oxadiazole Derived from [2.2]Paracyclophane
title Efficient Synthesis of Various Substituted (Thio)Ureas, Semicarbazides, Thiosemicarbazides, Thiazolidones, and Oxadiazole Derived from [2.2]Paracyclophane
title_full Efficient Synthesis of Various Substituted (Thio)Ureas, Semicarbazides, Thiosemicarbazides, Thiazolidones, and Oxadiazole Derived from [2.2]Paracyclophane
title_fullStr Efficient Synthesis of Various Substituted (Thio)Ureas, Semicarbazides, Thiosemicarbazides, Thiazolidones, and Oxadiazole Derived from [2.2]Paracyclophane
title_full_unstemmed Efficient Synthesis of Various Substituted (Thio)Ureas, Semicarbazides, Thiosemicarbazides, Thiazolidones, and Oxadiazole Derived from [2.2]Paracyclophane
title_short Efficient Synthesis of Various Substituted (Thio)Ureas, Semicarbazides, Thiosemicarbazides, Thiazolidones, and Oxadiazole Derived from [2.2]Paracyclophane
title_sort efficient synthesis of various substituted (thio)ureas, semicarbazides, thiosemicarbazides, thiazolidones, and oxadiazole derived from [2.2]paracyclophane
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9026011/
https://www.ncbi.nlm.nih.gov/pubmed/35474844
http://dx.doi.org/10.1021/acsomega.2c00141
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