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In situ tracking and characterisation of scorpionate ligands via(11)B-NMR spectroscopy
Herein, we exemplify the use of (11)B-NMR spectroscopy as a new means of tracking the synthesis of scorpionate ligands in situ and ascertaining their purity upon isolation. We have demonstrated the use of the characterisation technique on five well known scorpionate ligands as their potassium salts.
| Autores principales: | , |
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| Formato: | Online Artículo Texto |
| Lenguaje: | English |
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The Royal Society of Chemistry
2021
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| Materias: | |
| Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9030394/ https://www.ncbi.nlm.nih.gov/pubmed/35479172 http://dx.doi.org/10.1039/d0ra10826j |
| _version_ | 1784692128394248192 |
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| author | Thomas, Jarrod R. Sulway, Scott A. |
| author_facet | Thomas, Jarrod R. Sulway, Scott A. |
| author_sort | Thomas, Jarrod R. |
| collection | PubMed |
| description | Herein, we exemplify the use of (11)B-NMR spectroscopy as a new means of tracking the synthesis of scorpionate ligands in situ and ascertaining their purity upon isolation. We have demonstrated the use of the characterisation technique on five well known scorpionate ligands as their potassium salts. |
| format | Online Article Text |
| id | pubmed-9030394 |
| institution | National Center for Biotechnology Information |
| language | English |
| publishDate | 2021 |
| publisher | The Royal Society of Chemistry |
| record_format | MEDLINE/PubMed |
| spelling | pubmed-90303942022-04-26 In situ tracking and characterisation of scorpionate ligands via(11)B-NMR spectroscopy Thomas, Jarrod R. Sulway, Scott A. RSC Adv Chemistry Herein, we exemplify the use of (11)B-NMR spectroscopy as a new means of tracking the synthesis of scorpionate ligands in situ and ascertaining their purity upon isolation. We have demonstrated the use of the characterisation technique on five well known scorpionate ligands as their potassium salts. The Royal Society of Chemistry 2021-04-30 /pmc/articles/PMC9030394/ /pubmed/35479172 http://dx.doi.org/10.1039/d0ra10826j Text en This journal is © The Royal Society of Chemistry https://creativecommons.org/licenses/by/3.0/ |
| spellingShingle | Chemistry Thomas, Jarrod R. Sulway, Scott A. In situ tracking and characterisation of scorpionate ligands via(11)B-NMR spectroscopy |
| title |
In situ tracking and characterisation of scorpionate ligands via(11)B-NMR spectroscopy |
| title_full |
In situ tracking and characterisation of scorpionate ligands via(11)B-NMR spectroscopy |
| title_fullStr |
In situ tracking and characterisation of scorpionate ligands via(11)B-NMR spectroscopy |
| title_full_unstemmed |
In situ tracking and characterisation of scorpionate ligands via(11)B-NMR spectroscopy |
| title_short |
In situ tracking and characterisation of scorpionate ligands via(11)B-NMR spectroscopy |
| title_sort | in situ tracking and characterisation of scorpionate ligands via(11)b-nmr spectroscopy |
| topic | Chemistry |
| url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9030394/ https://www.ncbi.nlm.nih.gov/pubmed/35479172 http://dx.doi.org/10.1039/d0ra10826j |
| work_keys_str_mv | AT thomasjarrodr insitutrackingandcharacterisationofscorpionateligandsvia11bnmrspectroscopy AT sulwayscotta insitutrackingandcharacterisationofscorpionateligandsvia11bnmrspectroscopy |