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A Fabrication of Multichannel Graphite Electrode Using Low-Cost Stencil-Printing Technique

Multichannel graphite electrodes (MGrEs) have been designed and fabricated in this study. A template was cut from an adhesive plastic sheet using a desktop cutting device. The template was placed on a polypropylene substrate, and carbon graphite ink was applied with a squeegee to the template. The s...

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Autores principales: Kongkaew, Supatinee, Tubtimtong, Suowarot, Thavarungkul, Panote, Kanatharana, Proespichaya, Chang, Kah Haw, Abdullah, Ahmad Fahmi Lim, Limbut, Warakorn
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9032575/
https://www.ncbi.nlm.nih.gov/pubmed/35459019
http://dx.doi.org/10.3390/s22083034
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author Kongkaew, Supatinee
Tubtimtong, Suowarot
Thavarungkul, Panote
Kanatharana, Proespichaya
Chang, Kah Haw
Abdullah, Ahmad Fahmi Lim
Limbut, Warakorn
author_facet Kongkaew, Supatinee
Tubtimtong, Suowarot
Thavarungkul, Panote
Kanatharana, Proespichaya
Chang, Kah Haw
Abdullah, Ahmad Fahmi Lim
Limbut, Warakorn
author_sort Kongkaew, Supatinee
collection PubMed
description Multichannel graphite electrodes (MGrEs) have been designed and fabricated in this study. A template was cut from an adhesive plastic sheet using a desktop cutting device. The template was placed on a polypropylene substrate, and carbon graphite ink was applied with a squeegee to the template. The size of the auxiliary electrode (AE) as well as the location of the reference electrode (RE) of MGrEs design were investigated. Scanning electron microscopy was used to determine the thickness of the ink on the four working electrodes (WEs), which was 21.9 ± 1.8 µm. Cyclic voltammetry with a redox probe solution was used to assess the precision of the four WEs. The intra-electrode repeatability and inter-electrode reproducibility of the MGrEs production were satisfied by low RSD (<6%). Therefore, the MGrEs is reliable and capable of detecting four replicates of the target analyte in a single analysis. The electrochemical performance of four WEs was investigated and compared to one WE. The sensitivity of the MGrEs was comparable to the sensitivity of a single WE. The MGrEs’ potential applications were investigated by analyzing the nitrite in milk and tap water samples (recoveries values of 97.6 ± 0.4 to 110 ± 2%).
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spelling pubmed-90325752022-04-23 A Fabrication of Multichannel Graphite Electrode Using Low-Cost Stencil-Printing Technique Kongkaew, Supatinee Tubtimtong, Suowarot Thavarungkul, Panote Kanatharana, Proespichaya Chang, Kah Haw Abdullah, Ahmad Fahmi Lim Limbut, Warakorn Sensors (Basel) Article Multichannel graphite electrodes (MGrEs) have been designed and fabricated in this study. A template was cut from an adhesive plastic sheet using a desktop cutting device. The template was placed on a polypropylene substrate, and carbon graphite ink was applied with a squeegee to the template. The size of the auxiliary electrode (AE) as well as the location of the reference electrode (RE) of MGrEs design were investigated. Scanning electron microscopy was used to determine the thickness of the ink on the four working electrodes (WEs), which was 21.9 ± 1.8 µm. Cyclic voltammetry with a redox probe solution was used to assess the precision of the four WEs. The intra-electrode repeatability and inter-electrode reproducibility of the MGrEs production were satisfied by low RSD (<6%). Therefore, the MGrEs is reliable and capable of detecting four replicates of the target analyte in a single analysis. The electrochemical performance of four WEs was investigated and compared to one WE. The sensitivity of the MGrEs was comparable to the sensitivity of a single WE. The MGrEs’ potential applications were investigated by analyzing the nitrite in milk and tap water samples (recoveries values of 97.6 ± 0.4 to 110 ± 2%). MDPI 2022-04-15 /pmc/articles/PMC9032575/ /pubmed/35459019 http://dx.doi.org/10.3390/s22083034 Text en © 2022 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Kongkaew, Supatinee
Tubtimtong, Suowarot
Thavarungkul, Panote
Kanatharana, Proespichaya
Chang, Kah Haw
Abdullah, Ahmad Fahmi Lim
Limbut, Warakorn
A Fabrication of Multichannel Graphite Electrode Using Low-Cost Stencil-Printing Technique
title A Fabrication of Multichannel Graphite Electrode Using Low-Cost Stencil-Printing Technique
title_full A Fabrication of Multichannel Graphite Electrode Using Low-Cost Stencil-Printing Technique
title_fullStr A Fabrication of Multichannel Graphite Electrode Using Low-Cost Stencil-Printing Technique
title_full_unstemmed A Fabrication of Multichannel Graphite Electrode Using Low-Cost Stencil-Printing Technique
title_short A Fabrication of Multichannel Graphite Electrode Using Low-Cost Stencil-Printing Technique
title_sort fabrication of multichannel graphite electrode using low-cost stencil-printing technique
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9032575/
https://www.ncbi.nlm.nih.gov/pubmed/35459019
http://dx.doi.org/10.3390/s22083034
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