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Preparation of GO/SiO(2)/PEA as a new solid base catalyst for the green synthesis of some spirooxindole derivatives

Efficient and green one pot multi component synthesis of some spirooxindole derivatives in the presence of graphene oxide functionalized with 2-(1-piperazinyl) ethylamine (GO/SiO(2)/PEA) as a solid base catalyst was studied. GO/SiO(2)/PEA has been obtained through a two step reaction and characteriz...

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Detalles Bibliográficos
Autores principales: Toorbaf, Mahla, Moradi, Leila
Formato: Online Artículo Texto
Lenguaje:English
Publicado: The Royal Society of Chemistry 2021
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9034106/
https://www.ncbi.nlm.nih.gov/pubmed/35478825
http://dx.doi.org/10.1039/d1ra02850b
Descripción
Sumario:Efficient and green one pot multi component synthesis of some spirooxindole derivatives in the presence of graphene oxide functionalized with 2-(1-piperazinyl) ethylamine (GO/SiO(2)/PEA) as a solid base catalyst was studied. GO/SiO(2)/PEA has been obtained through a two step reaction and characterized by Fourier transform infrared spectroscopy (FTIR), field emission scanning electron microscopy (FE-SEM), energy-dispersive X-ray spectroscopy (EDX), thermo gravimetric analysis (TGA), Raman spectroscopy and X-ray diffraction (XRD). Green reaction conditions, short reaction times, reusable catalyst and a high to excellent yield of products are some of the advantageous of the presented method.