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Preparation of GO/SiO(2)/PEA as a new solid base catalyst for the green synthesis of some spirooxindole derivatives
Efficient and green one pot multi component synthesis of some spirooxindole derivatives in the presence of graphene oxide functionalized with 2-(1-piperazinyl) ethylamine (GO/SiO(2)/PEA) as a solid base catalyst was studied. GO/SiO(2)/PEA has been obtained through a two step reaction and characteriz...
Autores principales: | , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
The Royal Society of Chemistry
2021
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9034106/ https://www.ncbi.nlm.nih.gov/pubmed/35478825 http://dx.doi.org/10.1039/d1ra02850b |
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author | Toorbaf, Mahla Moradi, Leila |
author_facet | Toorbaf, Mahla Moradi, Leila |
author_sort | Toorbaf, Mahla |
collection | PubMed |
description | Efficient and green one pot multi component synthesis of some spirooxindole derivatives in the presence of graphene oxide functionalized with 2-(1-piperazinyl) ethylamine (GO/SiO(2)/PEA) as a solid base catalyst was studied. GO/SiO(2)/PEA has been obtained through a two step reaction and characterized by Fourier transform infrared spectroscopy (FTIR), field emission scanning electron microscopy (FE-SEM), energy-dispersive X-ray spectroscopy (EDX), thermo gravimetric analysis (TGA), Raman spectroscopy and X-ray diffraction (XRD). Green reaction conditions, short reaction times, reusable catalyst and a high to excellent yield of products are some of the advantageous of the presented method. |
format | Online Article Text |
id | pubmed-9034106 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2021 |
publisher | The Royal Society of Chemistry |
record_format | MEDLINE/PubMed |
spelling | pubmed-90341062022-04-26 Preparation of GO/SiO(2)/PEA as a new solid base catalyst for the green synthesis of some spirooxindole derivatives Toorbaf, Mahla Moradi, Leila RSC Adv Chemistry Efficient and green one pot multi component synthesis of some spirooxindole derivatives in the presence of graphene oxide functionalized with 2-(1-piperazinyl) ethylamine (GO/SiO(2)/PEA) as a solid base catalyst was studied. GO/SiO(2)/PEA has been obtained through a two step reaction and characterized by Fourier transform infrared spectroscopy (FTIR), field emission scanning electron microscopy (FE-SEM), energy-dispersive X-ray spectroscopy (EDX), thermo gravimetric analysis (TGA), Raman spectroscopy and X-ray diffraction (XRD). Green reaction conditions, short reaction times, reusable catalyst and a high to excellent yield of products are some of the advantageous of the presented method. The Royal Society of Chemistry 2021-06-21 /pmc/articles/PMC9034106/ /pubmed/35478825 http://dx.doi.org/10.1039/d1ra02850b Text en This journal is © The Royal Society of Chemistry https://creativecommons.org/licenses/by/3.0/ |
spellingShingle | Chemistry Toorbaf, Mahla Moradi, Leila Preparation of GO/SiO(2)/PEA as a new solid base catalyst for the green synthesis of some spirooxindole derivatives |
title | Preparation of GO/SiO(2)/PEA as a new solid base catalyst for the green synthesis of some spirooxindole derivatives |
title_full | Preparation of GO/SiO(2)/PEA as a new solid base catalyst for the green synthesis of some spirooxindole derivatives |
title_fullStr | Preparation of GO/SiO(2)/PEA as a new solid base catalyst for the green synthesis of some spirooxindole derivatives |
title_full_unstemmed | Preparation of GO/SiO(2)/PEA as a new solid base catalyst for the green synthesis of some spirooxindole derivatives |
title_short | Preparation of GO/SiO(2)/PEA as a new solid base catalyst for the green synthesis of some spirooxindole derivatives |
title_sort | preparation of go/sio(2)/pea as a new solid base catalyst for the green synthesis of some spirooxindole derivatives |
topic | Chemistry |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9034106/ https://www.ncbi.nlm.nih.gov/pubmed/35478825 http://dx.doi.org/10.1039/d1ra02850b |
work_keys_str_mv | AT toorbafmahla preparationofgosio2peaasanewsolidbasecatalystforthegreensynthesisofsomespirooxindolederivatives AT moradileila preparationofgosio2peaasanewsolidbasecatalystforthegreensynthesisofsomespirooxindolederivatives |