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Bioinspired triangular ZnO nanoclusters synthesized by Argyreia nervosa nascent leaf extract for the efficient electrochemical determination of vitamin C
This work deals with the synthesis of bioinspired triangular ZnO nanoclusters (bT-ZnO NCs) from Argyreia nervosa nascent leaf extract for their effective antibacterial activity and further utilization as a platform for the electrocatalytic determination of ascorbic acid (AA; vitamin C) for applicati...
Autores principales: | , , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
The Royal Society of Chemistry
2021
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9037078/ https://www.ncbi.nlm.nih.gov/pubmed/35478888 http://dx.doi.org/10.1039/d1ra04704c |
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author | Singh, Pooja Singh, Kshitij RB Singh, Jay Prasad, Priyanka Singh, Ravindra Pratap |
author_facet | Singh, Pooja Singh, Kshitij RB Singh, Jay Prasad, Priyanka Singh, Ravindra Pratap |
author_sort | Singh, Pooja |
collection | PubMed |
description | This work deals with the synthesis of bioinspired triangular ZnO nanoclusters (bT-ZnO NCs) from Argyreia nervosa nascent leaf extract for their effective antibacterial activity and further utilization as a platform for the electrocatalytic determination of ascorbic acid (AA; vitamin C) for applications in the agricultural domain. The structural, optical, and morphological characteristics of the synthesized bT-ZnO NCs were analyzed by UV-vis, FT-IR, XRD, AFM, SEM, TEM, HR-TEM, and EDX techniques. After this, bT-ZnO NCs were electrophoretically deposited onto an indium-tin-oxide (ITO) glass substrate and assessed for the electro-oxidation of AA by cyclic voltammetry (CV), and from this it was proven that bT-ZnO NCs had a very high electrochemical sensitivity of 29.88 μA cm(−2) toward AA and a low limit of detection of 0.5321 mM under the optimized experimental conditions. Thus, it provides a potential sensing platform for electrochemical studies to detect AA. Moreover, bT-ZnO NCs were preliminarily investigated for their antibacterial activity, and the obtained results showed that the bT-ZnO NCs have potency as an antibacterial agent. |
format | Online Article Text |
id | pubmed-9037078 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2021 |
publisher | The Royal Society of Chemistry |
record_format | MEDLINE/PubMed |
spelling | pubmed-90370782022-04-26 Bioinspired triangular ZnO nanoclusters synthesized by Argyreia nervosa nascent leaf extract for the efficient electrochemical determination of vitamin C Singh, Pooja Singh, Kshitij RB Singh, Jay Prasad, Priyanka Singh, Ravindra Pratap RSC Adv Chemistry This work deals with the synthesis of bioinspired triangular ZnO nanoclusters (bT-ZnO NCs) from Argyreia nervosa nascent leaf extract for their effective antibacterial activity and further utilization as a platform for the electrocatalytic determination of ascorbic acid (AA; vitamin C) for applications in the agricultural domain. The structural, optical, and morphological characteristics of the synthesized bT-ZnO NCs were analyzed by UV-vis, FT-IR, XRD, AFM, SEM, TEM, HR-TEM, and EDX techniques. After this, bT-ZnO NCs were electrophoretically deposited onto an indium-tin-oxide (ITO) glass substrate and assessed for the electro-oxidation of AA by cyclic voltammetry (CV), and from this it was proven that bT-ZnO NCs had a very high electrochemical sensitivity of 29.88 μA cm(−2) toward AA and a low limit of detection of 0.5321 mM under the optimized experimental conditions. Thus, it provides a potential sensing platform for electrochemical studies to detect AA. Moreover, bT-ZnO NCs were preliminarily investigated for their antibacterial activity, and the obtained results showed that the bT-ZnO NCs have potency as an antibacterial agent. The Royal Society of Chemistry 2021-07-27 /pmc/articles/PMC9037078/ /pubmed/35478888 http://dx.doi.org/10.1039/d1ra04704c Text en This journal is © The Royal Society of Chemistry https://creativecommons.org/licenses/by-nc/3.0/ |
spellingShingle | Chemistry Singh, Pooja Singh, Kshitij RB Singh, Jay Prasad, Priyanka Singh, Ravindra Pratap Bioinspired triangular ZnO nanoclusters synthesized by Argyreia nervosa nascent leaf extract for the efficient electrochemical determination of vitamin C |
title | Bioinspired triangular ZnO nanoclusters synthesized by Argyreia nervosa nascent leaf extract for the efficient electrochemical determination of vitamin C |
title_full | Bioinspired triangular ZnO nanoclusters synthesized by Argyreia nervosa nascent leaf extract for the efficient electrochemical determination of vitamin C |
title_fullStr | Bioinspired triangular ZnO nanoclusters synthesized by Argyreia nervosa nascent leaf extract for the efficient electrochemical determination of vitamin C |
title_full_unstemmed | Bioinspired triangular ZnO nanoclusters synthesized by Argyreia nervosa nascent leaf extract for the efficient electrochemical determination of vitamin C |
title_short | Bioinspired triangular ZnO nanoclusters synthesized by Argyreia nervosa nascent leaf extract for the efficient electrochemical determination of vitamin C |
title_sort | bioinspired triangular zno nanoclusters synthesized by argyreia nervosa nascent leaf extract for the efficient electrochemical determination of vitamin c |
topic | Chemistry |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9037078/ https://www.ncbi.nlm.nih.gov/pubmed/35478888 http://dx.doi.org/10.1039/d1ra04704c |
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