Solvent-free synthesis of symmetric methylene diesters via direct reaction of aromatic carboxylates with 1,n-dihaloalkanes

An efficient methodology for the synthesis of symmetrical methylene diesters was developed through direct reaction of various aromatic carboxylates with 1,n-dihaloalkanes under solvent-free conditions. This strategy offers a high product yield, facile work-up and purification, and an environmentally...

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Detalles Bibliográficos
Autores principales: Bai, Lin, Ding, Shenglong, Ma, Xiaofang
Formato: Online Artículo Texto
Lenguaje:English
Publicado: The Royal Society of Chemistry 2021
Materias:
Chemistry
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9038108/
https://www.ncbi.nlm.nih.gov/pubmed/35478540
http://dx.doi.org/10.1039/d1ra04814g
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author Bai, Lin
Ding, Shenglong
Ma, Xiaofang
author_facet Bai, Lin
Ding, Shenglong
Ma, Xiaofang
author_sort Bai, Lin
collection PubMed
description An efficient methodology for the synthesis of symmetrical methylene diesters was developed through direct reaction of various aromatic carboxylates with 1,n-dihaloalkanes under solvent-free conditions. This strategy offers a high product yield, facile work-up and purification, and an environmentally friendly approach to obtain long-chain methylene carboxylate scaffolds with increased diversity.
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spelling pubmed-90381082022-04-26 Solvent-free synthesis of symmetric methylene diesters via direct reaction of aromatic carboxylates with 1,n-dihaloalkanes Bai, Lin Ding, Shenglong Ma, Xiaofang RSC Adv Chemistry An efficient methodology for the synthesis of symmetrical methylene diesters was developed through direct reaction of various aromatic carboxylates with 1,n-dihaloalkanes under solvent-free conditions. This strategy offers a high product yield, facile work-up and purification, and an environmentally friendly approach to obtain long-chain methylene carboxylate scaffolds with increased diversity. The Royal Society of Chemistry 2021-08-25 /pmc/articles/PMC9038108/ /pubmed/35478540 http://dx.doi.org/10.1039/d1ra04814g Text en This journal is © The Royal Society of Chemistry https://creativecommons.org/licenses/by-nc/3.0/
spellingShingle Chemistry
Bai, Lin
Ding, Shenglong
Ma, Xiaofang
Solvent-free synthesis of symmetric methylene diesters via direct reaction of aromatic carboxylates with 1,n-dihaloalkanes
title Solvent-free synthesis of symmetric methylene diesters via direct reaction of aromatic carboxylates with 1,n-dihaloalkanes
title_full Solvent-free synthesis of symmetric methylene diesters via direct reaction of aromatic carboxylates with 1,n-dihaloalkanes
title_fullStr Solvent-free synthesis of symmetric methylene diesters via direct reaction of aromatic carboxylates with 1,n-dihaloalkanes
title_full_unstemmed Solvent-free synthesis of symmetric methylene diesters via direct reaction of aromatic carboxylates with 1,n-dihaloalkanes
title_short Solvent-free synthesis of symmetric methylene diesters via direct reaction of aromatic carboxylates with 1,n-dihaloalkanes
title_sort solvent-free synthesis of symmetric methylene diesters via direct reaction of aromatic carboxylates with 1,n-dihaloalkanes
topic Chemistry
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9038108/
https://www.ncbi.nlm.nih.gov/pubmed/35478540
http://dx.doi.org/10.1039/d1ra04814g
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AT maxiaofang solventfreesynthesisofsymmetricmethylenediestersviadirectreactionofaromaticcarboxylateswith1ndihaloalkanes

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