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Morphology of subsurface cracks in glass-ceramics induced by Vickers indentation observed by synchrotron X-ray multiscale tomography
The characterization of subsurface cracks induced by indentation is a challenge for understanding contact damage, impact, wear, erosion, and abrasion of brittle materials, because the crack pattern observable on the surface is only a part of the total crack system. Here we applied synchrotron X-ray...
Autores principales: | , , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
Nature Publishing Group UK
2022
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9050884/ https://www.ncbi.nlm.nih.gov/pubmed/35484320 http://dx.doi.org/10.1038/s41598-022-11084-0 |
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author | Okuma, Gaku Maeda, Kei Yoshida, Satoshi Takeuchi, Akihisa Wakai, Fumihiro |
author_facet | Okuma, Gaku Maeda, Kei Yoshida, Satoshi Takeuchi, Akihisa Wakai, Fumihiro |
author_sort | Okuma, Gaku |
collection | PubMed |
description | The characterization of subsurface cracks induced by indentation is a challenge for understanding contact damage, impact, wear, erosion, and abrasion of brittle materials, because the crack pattern observable on the surface is only a part of the total crack system. Here we applied synchrotron X-ray multiscale tomography to observe the morphology of subsurface cracks produced by Vickers indentation in a novel CaO–Al(2)O(3)–SiO(2) glass-ceramic with plate-like crystals forming a house-of-cards microstructure. It revealed a diverse type of crack systems around the semispherical microcrack zone beneath the indent, including a new mode II inclined lateral crack driven by the maximum shear stress. Tomography images provided knowledge on how the heterogeneous microstructure affected the toughening processes such as crack deflection, crack bridging, and microcracking. |
format | Online Article Text |
id | pubmed-9050884 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2022 |
publisher | Nature Publishing Group UK |
record_format | MEDLINE/PubMed |
spelling | pubmed-90508842022-04-30 Morphology of subsurface cracks in glass-ceramics induced by Vickers indentation observed by synchrotron X-ray multiscale tomography Okuma, Gaku Maeda, Kei Yoshida, Satoshi Takeuchi, Akihisa Wakai, Fumihiro Sci Rep Article The characterization of subsurface cracks induced by indentation is a challenge for understanding contact damage, impact, wear, erosion, and abrasion of brittle materials, because the crack pattern observable on the surface is only a part of the total crack system. Here we applied synchrotron X-ray multiscale tomography to observe the morphology of subsurface cracks produced by Vickers indentation in a novel CaO–Al(2)O(3)–SiO(2) glass-ceramic with plate-like crystals forming a house-of-cards microstructure. It revealed a diverse type of crack systems around the semispherical microcrack zone beneath the indent, including a new mode II inclined lateral crack driven by the maximum shear stress. Tomography images provided knowledge on how the heterogeneous microstructure affected the toughening processes such as crack deflection, crack bridging, and microcracking. Nature Publishing Group UK 2022-04-28 /pmc/articles/PMC9050884/ /pubmed/35484320 http://dx.doi.org/10.1038/s41598-022-11084-0 Text en © The Author(s) 2022 https://creativecommons.org/licenses/by/4.0/Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons licence, and indicate if changes were made. The images or other third party material in this article are included in the article's Creative Commons licence, unless indicated otherwise in a credit line to the material. If material is not included in the article's Creative Commons licence and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this licence, visit http://creativecommons.org/licenses/by/4.0/ (https://creativecommons.org/licenses/by/4.0/) . |
spellingShingle | Article Okuma, Gaku Maeda, Kei Yoshida, Satoshi Takeuchi, Akihisa Wakai, Fumihiro Morphology of subsurface cracks in glass-ceramics induced by Vickers indentation observed by synchrotron X-ray multiscale tomography |
title | Morphology of subsurface cracks in glass-ceramics induced by Vickers indentation observed by synchrotron X-ray multiscale tomography |
title_full | Morphology of subsurface cracks in glass-ceramics induced by Vickers indentation observed by synchrotron X-ray multiscale tomography |
title_fullStr | Morphology of subsurface cracks in glass-ceramics induced by Vickers indentation observed by synchrotron X-ray multiscale tomography |
title_full_unstemmed | Morphology of subsurface cracks in glass-ceramics induced by Vickers indentation observed by synchrotron X-ray multiscale tomography |
title_short | Morphology of subsurface cracks in glass-ceramics induced by Vickers indentation observed by synchrotron X-ray multiscale tomography |
title_sort | morphology of subsurface cracks in glass-ceramics induced by vickers indentation observed by synchrotron x-ray multiscale tomography |
topic | Article |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9050884/ https://www.ncbi.nlm.nih.gov/pubmed/35484320 http://dx.doi.org/10.1038/s41598-022-11084-0 |
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