Effects of high mechanical treatment and long-term annealing on crystal structure and thermal stability of Ti(2)O(3) nanocrystals

The effect of high-energy milling and long-term annealing on the stability of Ti(2)O(3) nanocrystals was studied using a magnetic susceptibility method. In situ temperature dependences revealed that the crystal size greatly affects the magnetic susceptibility value. According to XRD, SEM and TEM dat...

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Detalles Bibliográficos
Autores principales: Valeeva, Albina A., Nazarova, Svetlana Z., Schröttner, Hartmuth, Gerasimov, Evgeny Yu., Rempel, Andrey A.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: The Royal Society of Chemistry 2020
Materias:
Chemistry
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9055306/
https://www.ncbi.nlm.nih.gov/pubmed/35518592
http://dx.doi.org/10.1039/d0ra03862h
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author Valeeva, Albina A.
Nazarova, Svetlana Z.
Schröttner, Hartmuth
Gerasimov, Evgeny Yu.
Rempel, Andrey A.
author_facet Valeeva, Albina A.
Nazarova, Svetlana Z.
Schröttner, Hartmuth
Gerasimov, Evgeny Yu.
Rempel, Andrey A.
author_sort Valeeva, Albina A.
collection PubMed
description The effect of high-energy milling and long-term annealing on the stability of Ti(2)O(3) nanocrystals was studied using a magnetic susceptibility method. In situ temperature dependences revealed that the crystal size greatly affects the magnetic susceptibility value. According to XRD, SEM and TEM data, Magnéli phases Ti(9)O(10), Ti(4)O(7), Ti(7)O(19) and Ti(3)O(5) are formed.
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spelling pubmed-90553062022-05-04 Effects of high mechanical treatment and long-term annealing on crystal structure and thermal stability of Ti(2)O(3) nanocrystals Valeeva, Albina A. Nazarova, Svetlana Z. Schröttner, Hartmuth Gerasimov, Evgeny Yu. Rempel, Andrey A. RSC Adv Chemistry The effect of high-energy milling and long-term annealing on the stability of Ti(2)O(3) nanocrystals was studied using a magnetic susceptibility method. In situ temperature dependences revealed that the crystal size greatly affects the magnetic susceptibility value. According to XRD, SEM and TEM data, Magnéli phases Ti(9)O(10), Ti(4)O(7), Ti(7)O(19) and Ti(3)O(5) are formed. The Royal Society of Chemistry 2020-07-07 /pmc/articles/PMC9055306/ /pubmed/35518592 http://dx.doi.org/10.1039/d0ra03862h Text en This journal is © The Royal Society of Chemistry https://creativecommons.org/licenses/by-nc/3.0/
spellingShingle Chemistry
Valeeva, Albina A.
Nazarova, Svetlana Z.
Schröttner, Hartmuth
Gerasimov, Evgeny Yu.
Rempel, Andrey A.
Effects of high mechanical treatment and long-term annealing on crystal structure and thermal stability of Ti(2)O(3) nanocrystals
title Effects of high mechanical treatment and long-term annealing on crystal structure and thermal stability of Ti(2)O(3) nanocrystals
title_full Effects of high mechanical treatment and long-term annealing on crystal structure and thermal stability of Ti(2)O(3) nanocrystals
title_fullStr Effects of high mechanical treatment and long-term annealing on crystal structure and thermal stability of Ti(2)O(3) nanocrystals
title_full_unstemmed Effects of high mechanical treatment and long-term annealing on crystal structure and thermal stability of Ti(2)O(3) nanocrystals
title_short Effects of high mechanical treatment and long-term annealing on crystal structure and thermal stability of Ti(2)O(3) nanocrystals
title_sort effects of high mechanical treatment and long-term annealing on crystal structure and thermal stability of ti(2)o(3) nanocrystals
topic Chemistry
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9055306/
https://www.ncbi.nlm.nih.gov/pubmed/35518592
http://dx.doi.org/10.1039/d0ra03862h
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