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Synthesis of benzimidazolones by immobilized gold nanoparticles on chitosan extracted from shrimp shells supported on fibrous phosphosilicate
Here we demonstrate the synthesis of benzimidazolones from o-phenylenediamines and carbon dioxide in the presence of gold nanoparticles supported on a composite material based on microcrystalline chitosan from shrimp shells and fibrous phosphosilicate (CS–FPS/Au). The results showed that the gold na...
Autores principales: | , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
The Royal Society of Chemistry
2019
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9060964/ https://www.ncbi.nlm.nih.gov/pubmed/35518508 http://dx.doi.org/10.1039/c9ra00481e |
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author | Zahedifar, Mahboobeh Es-haghi, Ali Zhiani, Rahele Sadeghzadeh, Seyed Mohsen |
author_facet | Zahedifar, Mahboobeh Es-haghi, Ali Zhiani, Rahele Sadeghzadeh, Seyed Mohsen |
author_sort | Zahedifar, Mahboobeh |
collection | PubMed |
description | Here we demonstrate the synthesis of benzimidazolones from o-phenylenediamines and carbon dioxide in the presence of gold nanoparticles supported on a composite material based on microcrystalline chitosan from shrimp shells and fibrous phosphosilicate (CS–FPS/Au). The results showed that the gold nanoparticles were stable with the P, N and O atoms of CS–FPS. The morphology and structure of FPS leads to a higher catalytic activity. The CS–FPS/Au NPs were thoroughly characterized using TEM, FESEM, TGA, FTIR, and BET. |
format | Online Article Text |
id | pubmed-9060964 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2019 |
publisher | The Royal Society of Chemistry |
record_format | MEDLINE/PubMed |
spelling | pubmed-90609642022-05-04 Synthesis of benzimidazolones by immobilized gold nanoparticles on chitosan extracted from shrimp shells supported on fibrous phosphosilicate Zahedifar, Mahboobeh Es-haghi, Ali Zhiani, Rahele Sadeghzadeh, Seyed Mohsen RSC Adv Chemistry Here we demonstrate the synthesis of benzimidazolones from o-phenylenediamines and carbon dioxide in the presence of gold nanoparticles supported on a composite material based on microcrystalline chitosan from shrimp shells and fibrous phosphosilicate (CS–FPS/Au). The results showed that the gold nanoparticles were stable with the P, N and O atoms of CS–FPS. The morphology and structure of FPS leads to a higher catalytic activity. The CS–FPS/Au NPs were thoroughly characterized using TEM, FESEM, TGA, FTIR, and BET. The Royal Society of Chemistry 2019-02-25 /pmc/articles/PMC9060964/ /pubmed/35518508 http://dx.doi.org/10.1039/c9ra00481e Text en This journal is © The Royal Society of Chemistry https://creativecommons.org/licenses/by-nc/3.0/ |
spellingShingle | Chemistry Zahedifar, Mahboobeh Es-haghi, Ali Zhiani, Rahele Sadeghzadeh, Seyed Mohsen Synthesis of benzimidazolones by immobilized gold nanoparticles on chitosan extracted from shrimp shells supported on fibrous phosphosilicate |
title | Synthesis of benzimidazolones by immobilized gold nanoparticles on chitosan extracted from shrimp shells supported on fibrous phosphosilicate |
title_full | Synthesis of benzimidazolones by immobilized gold nanoparticles on chitosan extracted from shrimp shells supported on fibrous phosphosilicate |
title_fullStr | Synthesis of benzimidazolones by immobilized gold nanoparticles on chitosan extracted from shrimp shells supported on fibrous phosphosilicate |
title_full_unstemmed | Synthesis of benzimidazolones by immobilized gold nanoparticles on chitosan extracted from shrimp shells supported on fibrous phosphosilicate |
title_short | Synthesis of benzimidazolones by immobilized gold nanoparticles on chitosan extracted from shrimp shells supported on fibrous phosphosilicate |
title_sort | synthesis of benzimidazolones by immobilized gold nanoparticles on chitosan extracted from shrimp shells supported on fibrous phosphosilicate |
topic | Chemistry |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9060964/ https://www.ncbi.nlm.nih.gov/pubmed/35518508 http://dx.doi.org/10.1039/c9ra00481e |
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