Microwave-assisted synthesis of mutually embedded Rh concave nanocubes with enhanced electrocatalytic activity

Novel mutually embedded Rh concave nanocubes were synthesized by reducing Rh(acac)(3) in tetraethylene glycol in the presence of benzyldimethylhexadecylammonium, KI and polyvinylpyrrolidone under microwave irradiation for 120 s. KI and HDBAC were crucial to the formation of mutually embedded nanostr...

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Detalles Bibliográficos
Autores principales: Xu, Junxuan, Tang, Hongbin, Ning, Baogui, Zhao, Yanxi, Huang, Tao
Formato: Online Artículo Texto
Lenguaje:English
Publicado: The Royal Society of Chemistry 2019
Materias:
Chemistry
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9065163/
https://www.ncbi.nlm.nih.gov/pubmed/35516875
http://dx.doi.org/10.1039/c9ra02650a
Descripción
Sumario:Novel mutually embedded Rh concave nanocubes were synthesized by reducing Rh(acac)(3) in tetraethylene glycol in the presence of benzyldimethylhexadecylammonium, KI and polyvinylpyrrolidone under microwave irradiation for 120 s. KI and HDBAC were crucial to the formation of mutually embedded nanostructures. The as-prepared Rh nanocrystals exhibited higher electrocatalytic activity and stability.

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