Structure confirmation and thermal kinetics of the inclusion of cis-jasmone in β-cyclodextrin

In this study, inclusion complex of cis-jasmone in β-CD (β-CD-CJ) was synthesized to improve cis-jasmone stability. The structure and thermal kinetics of the inclusion complex was investigated by Fourier transform infrared spectroscopy (FTIR), thermogravimetric analysis (TG) and differential scannin...

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Detalles Bibliográficos
Autores principales: Ai, Lvye, Hu, Jingyan, Ji, Xiaoming, Zhao, Huaxin
Formato: Online Artículo Texto
Lenguaje:English
Publicado: The Royal Society of Chemistry 2019
Materias:
Chemistry
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9070386/
https://www.ncbi.nlm.nih.gov/pubmed/35531039
http://dx.doi.org/10.1039/c9ra03343b
Descripción
Sumario:In this study, inclusion complex of cis-jasmone in β-CD (β-CD-CJ) was synthesized to improve cis-jasmone stability. The structure and thermal kinetics of the inclusion complex was investigated by Fourier transform infrared spectroscopy (FTIR), thermogravimetric analysis (TG) and differential scanning calorimetry (DSC). DSC studies showed that the stability of cis-jasmone after β-cyclodextrin encapsulation was improved. The dissociation kinetics of β-CD-CJ at different heating rates was studied by TG, and the activation energy E of β-CD-CJ thermal decomposition kinetic parameters was defined by Flynn–Wall–Ozawa method. The results showed that the average activation energy E was 121.16 kJ mol(−1).

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