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Structure confirmation and thermal kinetics of the inclusion of cis-jasmone in β-cyclodextrin
In this study, inclusion complex of cis-jasmone in β-CD (β-CD-CJ) was synthesized to improve cis-jasmone stability. The structure and thermal kinetics of the inclusion complex was investigated by Fourier transform infrared spectroscopy (FTIR), thermogravimetric analysis (TG) and differential scannin...
Autores principales: | , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
The Royal Society of Chemistry
2019
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9070386/ https://www.ncbi.nlm.nih.gov/pubmed/35531039 http://dx.doi.org/10.1039/c9ra03343b |
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author | Ai, Lvye Hu, Jingyan Ji, Xiaoming Zhao, Huaxin |
author_facet | Ai, Lvye Hu, Jingyan Ji, Xiaoming Zhao, Huaxin |
author_sort | Ai, Lvye |
collection | PubMed |
description | In this study, inclusion complex of cis-jasmone in β-CD (β-CD-CJ) was synthesized to improve cis-jasmone stability. The structure and thermal kinetics of the inclusion complex was investigated by Fourier transform infrared spectroscopy (FTIR), thermogravimetric analysis (TG) and differential scanning calorimetry (DSC). DSC studies showed that the stability of cis-jasmone after β-cyclodextrin encapsulation was improved. The dissociation kinetics of β-CD-CJ at different heating rates was studied by TG, and the activation energy E of β-CD-CJ thermal decomposition kinetic parameters was defined by Flynn–Wall–Ozawa method. The results showed that the average activation energy E was 121.16 kJ mol(−1). |
format | Online Article Text |
id | pubmed-9070386 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2019 |
publisher | The Royal Society of Chemistry |
record_format | MEDLINE/PubMed |
spelling | pubmed-90703862022-05-05 Structure confirmation and thermal kinetics of the inclusion of cis-jasmone in β-cyclodextrin Ai, Lvye Hu, Jingyan Ji, Xiaoming Zhao, Huaxin RSC Adv Chemistry In this study, inclusion complex of cis-jasmone in β-CD (β-CD-CJ) was synthesized to improve cis-jasmone stability. The structure and thermal kinetics of the inclusion complex was investigated by Fourier transform infrared spectroscopy (FTIR), thermogravimetric analysis (TG) and differential scanning calorimetry (DSC). DSC studies showed that the stability of cis-jasmone after β-cyclodextrin encapsulation was improved. The dissociation kinetics of β-CD-CJ at different heating rates was studied by TG, and the activation energy E of β-CD-CJ thermal decomposition kinetic parameters was defined by Flynn–Wall–Ozawa method. The results showed that the average activation energy E was 121.16 kJ mol(−1). The Royal Society of Chemistry 2019-08-21 /pmc/articles/PMC9070386/ /pubmed/35531039 http://dx.doi.org/10.1039/c9ra03343b Text en This journal is © The Royal Society of Chemistry https://creativecommons.org/licenses/by-nc/3.0/ |
spellingShingle | Chemistry Ai, Lvye Hu, Jingyan Ji, Xiaoming Zhao, Huaxin Structure confirmation and thermal kinetics of the inclusion of cis-jasmone in β-cyclodextrin |
title | Structure confirmation and thermal kinetics of the inclusion of cis-jasmone in β-cyclodextrin |
title_full | Structure confirmation and thermal kinetics of the inclusion of cis-jasmone in β-cyclodextrin |
title_fullStr | Structure confirmation and thermal kinetics of the inclusion of cis-jasmone in β-cyclodextrin |
title_full_unstemmed | Structure confirmation and thermal kinetics of the inclusion of cis-jasmone in β-cyclodextrin |
title_short | Structure confirmation and thermal kinetics of the inclusion of cis-jasmone in β-cyclodextrin |
title_sort | structure confirmation and thermal kinetics of the inclusion of cis-jasmone in β-cyclodextrin |
topic | Chemistry |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9070386/ https://www.ncbi.nlm.nih.gov/pubmed/35531039 http://dx.doi.org/10.1039/c9ra03343b |
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