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Polished diamond X-ray lenses
High-quality bi-concave 2D focusing diamond X-ray lenses of apex-radius R = 100 µm produced via laser-ablation and improved via mechanical polishing are presented here. Both for polished and unpolished individual lenses and for stacks of ten lenses, the remaining figure errors determined using X-ray...
Autores principales: | , , , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
International Union of Crystallography
2022
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9070707/ https://www.ncbi.nlm.nih.gov/pubmed/35510996 http://dx.doi.org/10.1107/S1600577522001795 |
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author | Celestre, Rafael Antipov, Sergey Gomez, Edgar Zinn, Thomas Barrett, Raymond Roth, Thomas |
author_facet | Celestre, Rafael Antipov, Sergey Gomez, Edgar Zinn, Thomas Barrett, Raymond Roth, Thomas |
author_sort | Celestre, Rafael |
collection | PubMed |
description | High-quality bi-concave 2D focusing diamond X-ray lenses of apex-radius R = 100 µm produced via laser-ablation and improved via mechanical polishing are presented here. Both for polished and unpolished individual lenses and for stacks of ten lenses, the remaining figure errors determined using X-ray speckle tracking are shown and these results are compared with those of commercial R = 50 µm beryllium lenses that have similar focusing strength and physical aperture. For two stacks of ten diamond lenses (polished and unpolished) and a stack of eleven beryllium lenses, this paper presents measured 2D beam profiles out of focus and wire scans to obtain the beam size in the focal plane. These results are complemented with small-angle X-ray scattering (SAXS) measurements of a polished and an unpolished diamond lens. Again, this is compared with the SAXS of a beryllium lens. The polished X-ray lenses show similar figure errors to commercially available beryllium lenses. While the beam size in the focal plane is comparable to that of the beryllium lenses, the SAXS signal of the polished diamond lenses is considerably lower. |
format | Online Article Text |
id | pubmed-9070707 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2022 |
publisher | International Union of Crystallography |
record_format | MEDLINE/PubMed |
spelling | pubmed-90707072022-05-10 Polished diamond X-ray lenses Celestre, Rafael Antipov, Sergey Gomez, Edgar Zinn, Thomas Barrett, Raymond Roth, Thomas J Synchrotron Radiat Research Papers High-quality bi-concave 2D focusing diamond X-ray lenses of apex-radius R = 100 µm produced via laser-ablation and improved via mechanical polishing are presented here. Both for polished and unpolished individual lenses and for stacks of ten lenses, the remaining figure errors determined using X-ray speckle tracking are shown and these results are compared with those of commercial R = 50 µm beryllium lenses that have similar focusing strength and physical aperture. For two stacks of ten diamond lenses (polished and unpolished) and a stack of eleven beryllium lenses, this paper presents measured 2D beam profiles out of focus and wire scans to obtain the beam size in the focal plane. These results are complemented with small-angle X-ray scattering (SAXS) measurements of a polished and an unpolished diamond lens. Again, this is compared with the SAXS of a beryllium lens. The polished X-ray lenses show similar figure errors to commercially available beryllium lenses. While the beam size in the focal plane is comparable to that of the beryllium lenses, the SAXS signal of the polished diamond lenses is considerably lower. International Union of Crystallography 2022-03-15 /pmc/articles/PMC9070707/ /pubmed/35510996 http://dx.doi.org/10.1107/S1600577522001795 Text en © Rafael Celestre et al. 2022 https://creativecommons.org/licenses/by/4.0/This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
spellingShingle | Research Papers Celestre, Rafael Antipov, Sergey Gomez, Edgar Zinn, Thomas Barrett, Raymond Roth, Thomas Polished diamond X-ray lenses |
title | Polished diamond X-ray lenses |
title_full | Polished diamond X-ray lenses |
title_fullStr | Polished diamond X-ray lenses |
title_full_unstemmed | Polished diamond X-ray lenses |
title_short | Polished diamond X-ray lenses |
title_sort | polished diamond x-ray lenses |
topic | Research Papers |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9070707/ https://www.ncbi.nlm.nih.gov/pubmed/35510996 http://dx.doi.org/10.1107/S1600577522001795 |
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