Synthesis of self-assembled mesoporous 3D In(2)O(3) hierarchical micro flowers composed of nanosheets and their electrochemical properties

This report describes the methodology for the fabrication of mesoporous In(2)O(3) microflowers by hydrothermal and calcination procedures in which In(OH)(3)/In(2)S(3) acts as an intermediate. Both In(2)O(3) and its precursor were analyzed with scanning electron microscopy, energy dispersive X-ray sp...

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Autores principales: Prakasam, Balasubramaniam Arul, Lahtinen, Manu, Peuronen, Anssi, Manikandan, Govindhasamy, Muruganandham, Manickavachagam, Sillanpää, Mika
Formato: Online Artículo Texto
Lenguaje:English
Publicado: The Royal Society of Chemistry 2018
Materias:
Chemistry
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9083079/
https://www.ncbi.nlm.nih.gov/pubmed/35539774
http://dx.doi.org/10.1039/c8ra03573c
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author Prakasam, Balasubramaniam Arul
Lahtinen, Manu
Peuronen, Anssi
Manikandan, Govindhasamy
Muruganandham, Manickavachagam
Sillanpää, Mika
author_facet Prakasam, Balasubramaniam Arul
Lahtinen, Manu
Peuronen, Anssi
Manikandan, Govindhasamy
Muruganandham, Manickavachagam
Sillanpää, Mika
author_sort Prakasam, Balasubramaniam Arul
collection PubMed
description This report describes the methodology for the fabrication of mesoporous In(2)O(3) microflowers by hydrothermal and calcination procedures in which In(OH)(3)/In(2)S(3) acts as an intermediate. Both In(2)O(3) and its precursor were analyzed with scanning electron microscopy, energy dispersive X-ray spectrophotometry, transmission electron microscopy and powder X-ray diffraction. BET surface area, pore size and pore volume analyses were also carried out. Electron microscopy images clearly evidence the self-assembly of 2D nanosheets into the micro flower structure. The mechanism of self-assembly and calcination is reported. Electrochemical properties of the synthesized In(2)O(3) micro flowers were studied.
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spelling pubmed-90830792022-05-09 Synthesis of self-assembled mesoporous 3D In(2)O(3) hierarchical micro flowers composed of nanosheets and their electrochemical properties Prakasam, Balasubramaniam Arul Lahtinen, Manu Peuronen, Anssi Manikandan, Govindhasamy Muruganandham, Manickavachagam Sillanpää, Mika RSC Adv Chemistry This report describes the methodology for the fabrication of mesoporous In(2)O(3) microflowers by hydrothermal and calcination procedures in which In(OH)(3)/In(2)S(3) acts as an intermediate. Both In(2)O(3) and its precursor were analyzed with scanning electron microscopy, energy dispersive X-ray spectrophotometry, transmission electron microscopy and powder X-ray diffraction. BET surface area, pore size and pore volume analyses were also carried out. Electron microscopy images clearly evidence the self-assembly of 2D nanosheets into the micro flower structure. The mechanism of self-assembly and calcination is reported. Electrochemical properties of the synthesized In(2)O(3) micro flowers were studied. The Royal Society of Chemistry 2018-07-18 /pmc/articles/PMC9083079/ /pubmed/35539774 http://dx.doi.org/10.1039/c8ra03573c Text en This journal is © The Royal Society of Chemistry https://creativecommons.org/licenses/by-nc/3.0/
spellingShingle Chemistry
Prakasam, Balasubramaniam Arul
Lahtinen, Manu
Peuronen, Anssi
Manikandan, Govindhasamy
Muruganandham, Manickavachagam
Sillanpää, Mika
Synthesis of self-assembled mesoporous 3D In(2)O(3) hierarchical micro flowers composed of nanosheets and their electrochemical properties
title Synthesis of self-assembled mesoporous 3D In(2)O(3) hierarchical micro flowers composed of nanosheets and their electrochemical properties
title_full Synthesis of self-assembled mesoporous 3D In(2)O(3) hierarchical micro flowers composed of nanosheets and their electrochemical properties
title_fullStr Synthesis of self-assembled mesoporous 3D In(2)O(3) hierarchical micro flowers composed of nanosheets and their electrochemical properties
title_full_unstemmed Synthesis of self-assembled mesoporous 3D In(2)O(3) hierarchical micro flowers composed of nanosheets and their electrochemical properties
title_short Synthesis of self-assembled mesoporous 3D In(2)O(3) hierarchical micro flowers composed of nanosheets and their electrochemical properties
title_sort synthesis of self-assembled mesoporous 3d in(2)o(3) hierarchical micro flowers composed of nanosheets and their electrochemical properties
topic Chemistry
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9083079/
https://www.ncbi.nlm.nih.gov/pubmed/35539774
http://dx.doi.org/10.1039/c8ra03573c
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