A novel and efficient synthetic route to perfluoroisobutyronitrile from perfluoroisobutyryl acid

A novel synthetic route to perfluoroisobutyronitrile from perfluoroisobutyryl acid which has mild conditions and low toxicity is described. This study introduces detailed synthetic protocols and characterization including GC-MS, (13)C NMR and (19)F NMR spectroscopy of perfluoroisobutyryl acid, perfl...

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Detalles Bibliográficos
Autores principales: Wang, Yi, Sun, Mengting, Gao, Zhanyang, Zou, Lilin, Zhong, Lingyu, Peng, Ruichao, Yu, Ping, Luo, Yunbai
Formato: Online Artículo Texto
Lenguaje:English
Publicado: The Royal Society of Chemistry 2018
Materias:
Chemistry
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9088968/
https://www.ncbi.nlm.nih.gov/pubmed/35557811
http://dx.doi.org/10.1039/c8ra07821a
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author Wang, Yi
Sun, Mengting
Gao, Zhanyang
Zou, Lilin
Zhong, Lingyu
Peng, Ruichao
Yu, Ping
Luo, Yunbai
author_facet Wang, Yi
Sun, Mengting
Gao, Zhanyang
Zou, Lilin
Zhong, Lingyu
Peng, Ruichao
Yu, Ping
Luo, Yunbai
author_sort Wang, Yi
collection PubMed
description A novel synthetic route to perfluoroisobutyronitrile from perfluoroisobutyryl acid which has mild conditions and low toxicity is described. This study introduces detailed synthetic protocols and characterization including GC-MS, (13)C NMR and (19)F NMR spectroscopy of perfluoroisobutyryl acid, perfluoroisobutyryl chloride, perfluoroisobutyl amide and perfluoroisobutyronitrile. Besides, this route is superior to the established patent and shows potential application in high voltage electrical equipment.
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spelling pubmed-90889682022-05-11 A novel and efficient synthetic route to perfluoroisobutyronitrile from perfluoroisobutyryl acid Wang, Yi Sun, Mengting Gao, Zhanyang Zou, Lilin Zhong, Lingyu Peng, Ruichao Yu, Ping Luo, Yunbai RSC Adv Chemistry A novel synthetic route to perfluoroisobutyronitrile from perfluoroisobutyryl acid which has mild conditions and low toxicity is described. This study introduces detailed synthetic protocols and characterization including GC-MS, (13)C NMR and (19)F NMR spectroscopy of perfluoroisobutyryl acid, perfluoroisobutyryl chloride, perfluoroisobutyl amide and perfluoroisobutyronitrile. Besides, this route is superior to the established patent and shows potential application in high voltage electrical equipment. The Royal Society of Chemistry 2018-11-05 /pmc/articles/PMC9088968/ /pubmed/35557811 http://dx.doi.org/10.1039/c8ra07821a Text en This journal is © The Royal Society of Chemistry https://creativecommons.org/licenses/by/3.0/
spellingShingle Chemistry
Wang, Yi
Sun, Mengting
Gao, Zhanyang
Zou, Lilin
Zhong, Lingyu
Peng, Ruichao
Yu, Ping
Luo, Yunbai
A novel and efficient synthetic route to perfluoroisobutyronitrile from perfluoroisobutyryl acid
title A novel and efficient synthetic route to perfluoroisobutyronitrile from perfluoroisobutyryl acid
title_full A novel and efficient synthetic route to perfluoroisobutyronitrile from perfluoroisobutyryl acid
title_fullStr A novel and efficient synthetic route to perfluoroisobutyronitrile from perfluoroisobutyryl acid
title_full_unstemmed A novel and efficient synthetic route to perfluoroisobutyronitrile from perfluoroisobutyryl acid
title_short A novel and efficient synthetic route to perfluoroisobutyronitrile from perfluoroisobutyryl acid
title_sort novel and efficient synthetic route to perfluoroisobutyronitrile from perfluoroisobutyryl acid
topic Chemistry
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9088968/
https://www.ncbi.nlm.nih.gov/pubmed/35557811
http://dx.doi.org/10.1039/c8ra07821a
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