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Optimization of Typha Fibre Extraction and Properties for Bio-Composite Applications Using Desirability Function Analysis

The effect of extraction time, temperature, and alkali concentration on the physical and mechanical properties of cattail (Typha latifolia L.) fibres were investigated using five levels of time (4, 6, 8, 10, and 12 h), four levels of temperature (70, 80, 90, and 95 °C), and three levels of NaOH conc...

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Detalles Bibliográficos
Autores principales: Hasan, Mahmudul, Rahman, Mashiur, Chen, Ying, Cicek, Nazim
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9100250/
https://www.ncbi.nlm.nih.gov/pubmed/35566855
http://dx.doi.org/10.3390/polym14091685
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author Hasan, Mahmudul
Rahman, Mashiur
Chen, Ying
Cicek, Nazim
author_facet Hasan, Mahmudul
Rahman, Mashiur
Chen, Ying
Cicek, Nazim
author_sort Hasan, Mahmudul
collection PubMed
description The effect of extraction time, temperature, and alkali concentration on the physical and mechanical properties of cattail (Typha latifolia L.) fibres were investigated using five levels of time (4, 6, 8, 10, and 12 h), four levels of temperature (70, 80, 90, and 95 °C), and three levels of NaOH concentration (4, 7, 10%, w/v) in a 3 × 4 × 5 factorial experimental design. The extraction parameters were optimized for bio-composite application using a desirability function analysis (DFA), which determined that the optimum extraction time, temperature and NaOH concentration were 10 h, 90 °C, and 7%, respectively. A sensitivity analysis for optimal treatment conditions confirmed that the higher overall desirability does not necessarily mean a better solution. However, the analysis showed that the majority of optimum settings for time, temperature, and concentration of NaOH found in the sensitivity analysis matched with the optimum conditions determined by DFA, which confirmed the validity of the optimum treatment conditions.
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spelling pubmed-91002502022-05-14 Optimization of Typha Fibre Extraction and Properties for Bio-Composite Applications Using Desirability Function Analysis Hasan, Mahmudul Rahman, Mashiur Chen, Ying Cicek, Nazim Polymers (Basel) Article The effect of extraction time, temperature, and alkali concentration on the physical and mechanical properties of cattail (Typha latifolia L.) fibres were investigated using five levels of time (4, 6, 8, 10, and 12 h), four levels of temperature (70, 80, 90, and 95 °C), and three levels of NaOH concentration (4, 7, 10%, w/v) in a 3 × 4 × 5 factorial experimental design. The extraction parameters were optimized for bio-composite application using a desirability function analysis (DFA), which determined that the optimum extraction time, temperature and NaOH concentration were 10 h, 90 °C, and 7%, respectively. A sensitivity analysis for optimal treatment conditions confirmed that the higher overall desirability does not necessarily mean a better solution. However, the analysis showed that the majority of optimum settings for time, temperature, and concentration of NaOH found in the sensitivity analysis matched with the optimum conditions determined by DFA, which confirmed the validity of the optimum treatment conditions. MDPI 2022-04-21 /pmc/articles/PMC9100250/ /pubmed/35566855 http://dx.doi.org/10.3390/polym14091685 Text en © 2022 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Hasan, Mahmudul
Rahman, Mashiur
Chen, Ying
Cicek, Nazim
Optimization of Typha Fibre Extraction and Properties for Bio-Composite Applications Using Desirability Function Analysis
title Optimization of Typha Fibre Extraction and Properties for Bio-Composite Applications Using Desirability Function Analysis
title_full Optimization of Typha Fibre Extraction and Properties for Bio-Composite Applications Using Desirability Function Analysis
title_fullStr Optimization of Typha Fibre Extraction and Properties for Bio-Composite Applications Using Desirability Function Analysis
title_full_unstemmed Optimization of Typha Fibre Extraction and Properties for Bio-Composite Applications Using Desirability Function Analysis
title_short Optimization of Typha Fibre Extraction and Properties for Bio-Composite Applications Using Desirability Function Analysis
title_sort optimization of typha fibre extraction and properties for bio-composite applications using desirability function analysis
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9100250/
https://www.ncbi.nlm.nih.gov/pubmed/35566855
http://dx.doi.org/10.3390/polym14091685
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