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Test and Microstructural Analysis of a Steel Slag Cement-Based Material Using the Response Surface Method

In this study, the silica fume replacement rate, fly ash replacement rate, and curing temperature were regarded as the independent variables, and the compressive and flexural strengths were regarded as the response values. The response surface method was used to construct the response surface polyno...

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Autores principales: Zhang, Xuanshuo, Li, Hongbo, Li, Sheng, Ding, Yongfa, Zhang, Hubiao, Tong, Yufei, Hua, Shudong
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9105800/
https://www.ncbi.nlm.nih.gov/pubmed/35591448
http://dx.doi.org/10.3390/ma15093114
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author Zhang, Xuanshuo
Li, Hongbo
Li, Sheng
Ding, Yongfa
Zhang, Hubiao
Tong, Yufei
Hua, Shudong
author_facet Zhang, Xuanshuo
Li, Hongbo
Li, Sheng
Ding, Yongfa
Zhang, Hubiao
Tong, Yufei
Hua, Shudong
author_sort Zhang, Xuanshuo
collection PubMed
description In this study, the silica fume replacement rate, fly ash replacement rate, and curing temperature were regarded as the independent variables, and the compressive and flexural strengths were regarded as the response values. The response surface method was used to construct the response surface polynomial regression model and obtain the optimal preparation parameters of a steel slag cement-based gel slurry (SCGS). The univariate and multivariate effects on the SCGS’s strength were investigated via analysis of variance and a three-dimensional surface model, and the hydration products and strength development law were characterized via scanning electron microscopy and X-ray diffraction. The actual compressive strengths at 3 and 28 d of age were 31.78 and 53.94 MPa, respectively, which were close to the predicted values (32.59 and 55.81 MPa, respectively), demonstrating that the optimized strengths were accurate and reliable. Further, the hydration reaction rate of SiO(2) in the silica fume and the physical filling effect of the inert components of fly ash and steel slag under the optimal parameters were the key factors for the early strength of the material. Moreover, continuous C(3)S hydration in steel slag and the continuous excitation of the volcanic ash properties of fly ash were important factors for the later strength.
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spelling pubmed-91058002022-05-14 Test and Microstructural Analysis of a Steel Slag Cement-Based Material Using the Response Surface Method Zhang, Xuanshuo Li, Hongbo Li, Sheng Ding, Yongfa Zhang, Hubiao Tong, Yufei Hua, Shudong Materials (Basel) Article In this study, the silica fume replacement rate, fly ash replacement rate, and curing temperature were regarded as the independent variables, and the compressive and flexural strengths were regarded as the response values. The response surface method was used to construct the response surface polynomial regression model and obtain the optimal preparation parameters of a steel slag cement-based gel slurry (SCGS). The univariate and multivariate effects on the SCGS’s strength were investigated via analysis of variance and a three-dimensional surface model, and the hydration products and strength development law were characterized via scanning electron microscopy and X-ray diffraction. The actual compressive strengths at 3 and 28 d of age were 31.78 and 53.94 MPa, respectively, which were close to the predicted values (32.59 and 55.81 MPa, respectively), demonstrating that the optimized strengths were accurate and reliable. Further, the hydration reaction rate of SiO(2) in the silica fume and the physical filling effect of the inert components of fly ash and steel slag under the optimal parameters were the key factors for the early strength of the material. Moreover, continuous C(3)S hydration in steel slag and the continuous excitation of the volcanic ash properties of fly ash were important factors for the later strength. MDPI 2022-04-25 /pmc/articles/PMC9105800/ /pubmed/35591448 http://dx.doi.org/10.3390/ma15093114 Text en © 2022 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Zhang, Xuanshuo
Li, Hongbo
Li, Sheng
Ding, Yongfa
Zhang, Hubiao
Tong, Yufei
Hua, Shudong
Test and Microstructural Analysis of a Steel Slag Cement-Based Material Using the Response Surface Method
title Test and Microstructural Analysis of a Steel Slag Cement-Based Material Using the Response Surface Method
title_full Test and Microstructural Analysis of a Steel Slag Cement-Based Material Using the Response Surface Method
title_fullStr Test and Microstructural Analysis of a Steel Slag Cement-Based Material Using the Response Surface Method
title_full_unstemmed Test and Microstructural Analysis of a Steel Slag Cement-Based Material Using the Response Surface Method
title_short Test and Microstructural Analysis of a Steel Slag Cement-Based Material Using the Response Surface Method
title_sort test and microstructural analysis of a steel slag cement-based material using the response surface method
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9105800/
https://www.ncbi.nlm.nih.gov/pubmed/35591448
http://dx.doi.org/10.3390/ma15093114
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