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Evaluation of Blend Uniformity and Terminal Point during Continuous Mixing in Water for Modified Double-Base Propellant Components Using a Near-Infrared Method

[Image: see text] A near-infrared (NIR) spectrometer was used to test the double-base absorbent powder sample and to quantitatively analyze the contents of each component as well as their dispersion uniformity to establish a rapid quantitative test method for blending uniformity of modified double-b...

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Autores principales: Liu, Ben, Xiao, Lei, Wu, Zongkai, Li, Duo, Hu, Yubing, Zhang, Guangpu, Zhao, Fengqi, Song, Xiuduo, Jiang, Wei, Hao, Gazi
Formato: Online Artículo Texto
Lenguaje:English
Publicado: American Chemical Society 2022
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9134419/
https://www.ncbi.nlm.nih.gov/pubmed/35647447
http://dx.doi.org/10.1021/acsomega.2c00532
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author Liu, Ben
Xiao, Lei
Wu, Zongkai
Li, Duo
Hu, Yubing
Zhang, Guangpu
Zhao, Fengqi
Song, Xiuduo
Jiang, Wei
Hao, Gazi
author_facet Liu, Ben
Xiao, Lei
Wu, Zongkai
Li, Duo
Hu, Yubing
Zhang, Guangpu
Zhao, Fengqi
Song, Xiuduo
Jiang, Wei
Hao, Gazi
author_sort Liu, Ben
collection PubMed
description [Image: see text] A near-infrared (NIR) spectrometer was used to test the double-base absorbent powder sample and to quantitatively analyze the contents of each component as well as their dispersion uniformity to establish a rapid quantitative test method for blending uniformity of modified double-base (MDB) propellant components. First, the quantitative calibration models of hexahydro-1,3,5-trinitro-1,3,5-triazine (RDX) were constructed based on sample testing, and the RDX model’s correlation coefficient was 0.9929. Then, during the blending process, NIR spectra were continually collected. For the original spectra of samples, the blend uniformity was assessed using the coefficient of moving block standard deviation (MBSD). After 160 min, the sample’s MBSD value had reached a steady state of less than 0.003, indicating that the sample’s components were distributed uniformly. The findings reveal that NIR spectroscopy can be used to verify the blending uniformity of MDB propellant components.
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spelling pubmed-91344192022-05-27 Evaluation of Blend Uniformity and Terminal Point during Continuous Mixing in Water for Modified Double-Base Propellant Components Using a Near-Infrared Method Liu, Ben Xiao, Lei Wu, Zongkai Li, Duo Hu, Yubing Zhang, Guangpu Zhao, Fengqi Song, Xiuduo Jiang, Wei Hao, Gazi ACS Omega [Image: see text] A near-infrared (NIR) spectrometer was used to test the double-base absorbent powder sample and to quantitatively analyze the contents of each component as well as their dispersion uniformity to establish a rapid quantitative test method for blending uniformity of modified double-base (MDB) propellant components. First, the quantitative calibration models of hexahydro-1,3,5-trinitro-1,3,5-triazine (RDX) were constructed based on sample testing, and the RDX model’s correlation coefficient was 0.9929. Then, during the blending process, NIR spectra were continually collected. For the original spectra of samples, the blend uniformity was assessed using the coefficient of moving block standard deviation (MBSD). After 160 min, the sample’s MBSD value had reached a steady state of less than 0.003, indicating that the sample’s components were distributed uniformly. The findings reveal that NIR spectroscopy can be used to verify the blending uniformity of MDB propellant components. American Chemical Society 2022-05-13 /pmc/articles/PMC9134419/ /pubmed/35647447 http://dx.doi.org/10.1021/acsomega.2c00532 Text en © 2022 The Authors. Published by American Chemical Society https://creativecommons.org/licenses/by-nc-nd/4.0/Permits non-commercial access and re-use, provided that author attribution and integrity are maintained; but does not permit creation of adaptations or other derivative works (https://creativecommons.org/licenses/by-nc-nd/4.0/).
spellingShingle Liu, Ben
Xiao, Lei
Wu, Zongkai
Li, Duo
Hu, Yubing
Zhang, Guangpu
Zhao, Fengqi
Song, Xiuduo
Jiang, Wei
Hao, Gazi
Evaluation of Blend Uniformity and Terminal Point during Continuous Mixing in Water for Modified Double-Base Propellant Components Using a Near-Infrared Method
title Evaluation of Blend Uniformity and Terminal Point during Continuous Mixing in Water for Modified Double-Base Propellant Components Using a Near-Infrared Method
title_full Evaluation of Blend Uniformity and Terminal Point during Continuous Mixing in Water for Modified Double-Base Propellant Components Using a Near-Infrared Method
title_fullStr Evaluation of Blend Uniformity and Terminal Point during Continuous Mixing in Water for Modified Double-Base Propellant Components Using a Near-Infrared Method
title_full_unstemmed Evaluation of Blend Uniformity and Terminal Point during Continuous Mixing in Water for Modified Double-Base Propellant Components Using a Near-Infrared Method
title_short Evaluation of Blend Uniformity and Terminal Point during Continuous Mixing in Water for Modified Double-Base Propellant Components Using a Near-Infrared Method
title_sort evaluation of blend uniformity and terminal point during continuous mixing in water for modified double-base propellant components using a near-infrared method
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9134419/
https://www.ncbi.nlm.nih.gov/pubmed/35647447
http://dx.doi.org/10.1021/acsomega.2c00532
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