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Drying Regimes on Regenerated Cellulose Films Characteristics and Properties

Abundant water content and its interaction with cellulose macromolecules through hydrogen bonding engenders a complex drying process, the circumstances of which have not yet been unveiled. For instance, excessive drying on regenerated cellulose membranes (RCM) causes cracking and severe shrinking, a...

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Autores principales: Ibrahim, Nur Ain, Salleh, Kushairi Mohd, Fudholi, Ahmad, Zakaria, Sarani
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9145432/
https://www.ncbi.nlm.nih.gov/pubmed/35629771
http://dx.doi.org/10.3390/membranes12050445
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author Ibrahim, Nur Ain
Salleh, Kushairi Mohd
Fudholi, Ahmad
Zakaria, Sarani
author_facet Ibrahim, Nur Ain
Salleh, Kushairi Mohd
Fudholi, Ahmad
Zakaria, Sarani
author_sort Ibrahim, Nur Ain
collection PubMed
description Abundant water content and its interaction with cellulose macromolecules through hydrogen bonding engenders a complex drying process, the circumstances of which have not yet been unveiled. For instance, excessive drying on regenerated cellulose membranes (RCM) causes cracking and severe shrinking, affecting the produced regenerated cellulose film (RCF). Thus, mathematical models in estimating the drying kinetics and required energy to dry RCM are necessary. This study evaluated two drying techniques of oven drying and infrared (IR) drying on RCM at different temperatures of 50–80 °C. Five mathematical models were used, namely Newton, Page, Handreson–Pabis, logarithmic, and Wang–Singh, to adjust the obtained experimental data and were statistically validated using ANOVA to review their effect on the quality of the produced RCF. A logarithmic model and a Wang–Singh model were the best models for oven drying and IR drying of RCM, respectively. It was found that the physical property of the RCF was similar to all drying types. Meanwhile, for mechanical properties, the high temperature of oven drying affected the tensile properties of RCF compared with IR drying. This study is beneficial by approximating the drying kinetics of RCM and defining appropriate drying conditions, which controls the quality of its predictive physical and mechanical properties.
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spelling pubmed-91454322022-05-29 Drying Regimes on Regenerated Cellulose Films Characteristics and Properties Ibrahim, Nur Ain Salleh, Kushairi Mohd Fudholi, Ahmad Zakaria, Sarani Membranes (Basel) Article Abundant water content and its interaction with cellulose macromolecules through hydrogen bonding engenders a complex drying process, the circumstances of which have not yet been unveiled. For instance, excessive drying on regenerated cellulose membranes (RCM) causes cracking and severe shrinking, affecting the produced regenerated cellulose film (RCF). Thus, mathematical models in estimating the drying kinetics and required energy to dry RCM are necessary. This study evaluated two drying techniques of oven drying and infrared (IR) drying on RCM at different temperatures of 50–80 °C. Five mathematical models were used, namely Newton, Page, Handreson–Pabis, logarithmic, and Wang–Singh, to adjust the obtained experimental data and were statistically validated using ANOVA to review their effect on the quality of the produced RCF. A logarithmic model and a Wang–Singh model were the best models for oven drying and IR drying of RCM, respectively. It was found that the physical property of the RCF was similar to all drying types. Meanwhile, for mechanical properties, the high temperature of oven drying affected the tensile properties of RCF compared with IR drying. This study is beneficial by approximating the drying kinetics of RCM and defining appropriate drying conditions, which controls the quality of its predictive physical and mechanical properties. MDPI 2022-04-20 /pmc/articles/PMC9145432/ /pubmed/35629771 http://dx.doi.org/10.3390/membranes12050445 Text en © 2022 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Ibrahim, Nur Ain
Salleh, Kushairi Mohd
Fudholi, Ahmad
Zakaria, Sarani
Drying Regimes on Regenerated Cellulose Films Characteristics and Properties
title Drying Regimes on Regenerated Cellulose Films Characteristics and Properties
title_full Drying Regimes on Regenerated Cellulose Films Characteristics and Properties
title_fullStr Drying Regimes on Regenerated Cellulose Films Characteristics and Properties
title_full_unstemmed Drying Regimes on Regenerated Cellulose Films Characteristics and Properties
title_short Drying Regimes on Regenerated Cellulose Films Characteristics and Properties
title_sort drying regimes on regenerated cellulose films characteristics and properties
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9145432/
https://www.ncbi.nlm.nih.gov/pubmed/35629771
http://dx.doi.org/10.3390/membranes12050445
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